Bicyclo[3.1.0]hexan-2-ol, 2-methyl-5-(1-methylethyl)-, (1α,2α,5α)-


Kovats' RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.260.260.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 246.246.280.280. 
Heat rate (K/min) 3.3.2.2.3.
Initial hold (min)   8.8. 
Final hold (min)   30.30. 
I 1068.1097.1075.1101.1070.
ReferenceAdams, González Elizondo, et al., 2006Adams, González Elizondo, et al., 2006Hazzit, Baaliouamer, et al., 2006Hazzit, Baaliouamer, et al., 2006Lucero, Fredrickson, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1DB-5DB-5DB-5
Column length (m) 25.25.30.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.260.260.26
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.246.246.246.
Heat rate (K/min) 5.5.3.3.3.
Initial hold (min)      
Final hold (min) 13.13.   
I 1096.1070.1070.1068.1097.
ReferenceRaina, Verma, et al., 2006Raina, Verma, et al., 2006Adams, Morris, et al., 2005Adams and Nguyen, 2005Adams and Nguyen, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSBP-5BP-5DB-5
Column length (m) 30.30.50.50.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.50.50.60.
Tend (C) 250.250.260.260.255.
Heat rate (K/min) 3.3.5.5.3.
Initial hold (min) 10.10.2.2. 
Final hold (min) 5.5.5.5. 
I 1071.1097.1099.1070.1069.
ReferenceAsuming, Beauchamp, et al., 2005Asuming, Beauchamp, et al., 2005Baranauskiene, Venskutonis, et al., 2005Baranauskiene, Venskutonis, et al., 2005Medina, Lucero, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5BPX-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas HeH2H2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.40.60.60.
Tend (C) 240.280.280.240.260.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min)      
Final hold (min)  30.30.  
I 1043.1069.1107.1093.1070.
ReferenceTepe, Sokmen, et al., 2005Avato, Raffo, et al., 2004Avato, Raffo, et al., 2004El-Ghorab, Mansour, et al., 2004Lopes, Strobl, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.251.0.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 260.250.280.280.280.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min)  1.   
Final hold (min)      
I 1099.1076.1045.1058.1093.
ReferenceLopes, Strobl, et al., 2004Bouzouita, Kachouri, et al., 2003Gkinis, Tzakou, et al., 2003Özcan, Tzakou, et al., 2003Özcan, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30BP-1BP-1BP-1
Column length (m) 25.25.60.60.25.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.220.220.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.60.60.60.
Tend (C) 220.220.220.220.220.
Heat rate (K/min) 4.4.5.5.5.
Initial hold (min)      
Final hold (min)     15.
I 1083.1056.1094.1061.1091.
ReferencePalá-Paúl, Velasco-Negueruela, et al., 2002Palá-Paúl, Velasco-Negueruela, et al., 2002Raina, Lal, et al., 2002Raina, Lal, et al., 2002Raina, Srivastava, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1BP-1BP-1BP-1
Column length (m) 25.25.25.30.30.
Carrier gas N2N2 N2N2
Substrate      
Column diameter (mm) 0.320.50.50.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.220.220.220.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min)      
Final hold (min) 15.10.10.13.13.
I 1062.1060.1060.1086.1051.
ReferenceRaina, Srivastava, et al., 2002Rajeswara Rao, 2002Rao B.R.R., 2002Shawl, Srivastava, et al., 2002Shawl, Srivastava, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-1HP-5SE-54
Column length (m) 25.25.50.30.30.
Carrier gas H2H2N2HeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.26
Phase thickness (μm) 0.520.520.250.250.25
Tstart (C) 40.40.80.60.60.
Tend (C) 240.240.225.280.246.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min)      
Final hold (min)      
I 1068.1097.1073.1067.1068.
ReferenceKitic, Palic, et al., 2001Kitic, Palic, et al., 2001Palá-Paúl, Velasco-Negueruela, et al., 2001Tzakou and Couladis, 2001Adams, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5DB-5SE-54SE-54
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.260.260.260.260.26
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 246.240.240.246.246.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)      
Final hold (min)      
I 1097.1068.1097.1068.1097.
ReferenceAdams, 2000Adams, 2000, 2Adams, 2000, 2Adams, 2000, 3Adams, 2000, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5SE-30DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.260.260.220.260.26
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 246.246.220.246.246.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)      
Final hold (min)      
I 1068.1097.1052.1068.1097.
ReferenceAdams, 2000, 4Adams, 2000, 4Kardali, Velasco-Negueruela, et al., 2000Adams, 1999Adams, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5DB-5DB-5BP-1
Column length (m) 25.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.330.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 280.280.260.240.260.
Heat rate (K/min) 5.4.2.3.2.
Initial hold (min)   5.  
Final hold (min)   20.  
I 1059.1065.1116.1064.1091.
ReferenceKaul, Gujral, et al., 1999Sajjadi and Ghassemi, 1999Senatore and de Feo, 1999da Silva, Andrade, et al., 1999Vera and Chane-Ming, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1BP-1Methyl SiliconeMethyl Silicone
Column length (m) 50.50.50.30.30.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 260.260.260.250.250.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)    2.2.
Final hold (min)    5.5.
I 1092.1078.1085.1065.1096.
ReferenceVera and Chane-Ming, 1999Vera and Chane-Ming, 1999Vera and Chane-Ming, 1999Adegoke, Rao, et al., 1998Adegoke, Rao, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1DB-5DB-5OV-101
Column length (m) 50.50.30.30.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (μm) 1.1.0.250.250.2
Tstart (C) 50.50.60.60.80.
Tend (C) 220.220.240.240.200.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min)      
Final hold (min)     60.
I 1090.1060.1069.1096.1064.
ReferenceBreheret, Talou, et al., 1997Breheret, Talou, et al., 1997Tellez, Estell, et al., 1997Tellez, Estell, et al., 1997Padrayuttawat, Tamura, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SPB-1
Column length (m) 50.
Carrier gas He
Substrate  
Column diameter (mm) 0.20
Phase thickness (μm)  
Tstart (C) 35.
Tend (C) 200.
Heat rate (K/min) 3.
Initial hold (min) 5.
Final hold (min) 20.
I 1073.
ReferenceWong and Tie, 1993
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Adams, González Elizondo, et al., 2006
Adams, R.P.; González Elizondo, M.S.; González Elizondo, M.; Slinkman, E., DNA fingerprinting and terpenoid analysis of Juniperus blancoi var. huehuentensis (Cupressaceae), a new subalpine variety from Durango, Mexico, Biochem. Syst. Ecol., 2006, 34, 3, 205-211, https://doi.org/10.1016/j.bse.2005.11.004 . [all data]

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Tzakou and Couladis, 2001
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Adams, 2000
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Adams, 2000, 2
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Adams, 2000, 3
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Adams, 2000, 4
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Kardali, Velasco-Negueruela, et al., 2000
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Adams, 1999
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Sajjadi and Ghassemi, 1999
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Senatore and de Feo, 1999
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da Silva, Andrade, et al., 1999
da Silva, M.H.L.; Andrade, E.H.A.; Zoghbi, M.G.B.; Luz, A.I.R.; da Silva, J.D.; Maia, J.G.S., The essential oils of Lantana camara L. occurring in North Brazil, Flavour Fragr. J., 1999, 14, 4, 208-210, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<208::AID-FFJ811>3.0.CO;2-F . [all data]

Vera and Chane-Ming, 1999
Vera, R.R.; Chane-Ming, J., Chemical composition of the essential oil of marjoram (Origanum majorana L.) from Reunion Island, Food Chem., 1999, 66, 2, 143-145, https://doi.org/10.1016/S0308-8146(98)00018-1 . [all data]

Adegoke, Rao, et al., 1998
Adegoke, G.O.; Rao, L.J.M.; Shankaracharya, N.B., A comparison of the essential oils of Aframomum daniellii (Hook. f.) K. Schum. and Amomum subulatum Roxb, Flavour Fragr. J., 1998, 13, 5, 349-352, https://doi.org/10.1002/(SICI)1099-1026(1998090)13:5<349::AID-FFJ758>3.0.CO;2-O . [all data]

Breheret, Talou, et al., 1997
Breheret, S.; Talou, T.; Rapior, S.; Bessiére, J.-M., Monoterpenes in the aroma of fresh wild mushrooms (Basidiomycetes), J. Agric. Food Chem., 1997, 45, 3, 831-836, https://doi.org/10.1021/jf960417h . [all data]

Tellez, Estell, et al., 1997
Tellez, M.R.; Estell, R.E.; Fredrickson, E.L.; Havstad, K.M., Essential oil of Dyssodia acerosa DC., J. Agric. Food Chem., 1997, 45, 8, 3276-3278, https://doi.org/10.1021/jf9701502 . [all data]

Padrayuttawat, Tamura, et al., 1996
Padrayuttawat, A.; Tamura, H.; Yamao, M., A split injection system for the analysis of purge and trap headspace of the volatile components in Citrus sudachi, J. Hi. Res. Chromatogr., 1996, 19, 6, 365-369, https://doi.org/10.1002/jhrc.1240190613 . [all data]

Wong and Tie, 1993
Wong, K.C.; Tie, D.Y., The Essential Oil of the Leaves of Murraya koenigii Spreng., J. Essent. Oil Res., 1993, 5, 4, 371-374, https://doi.org/10.1080/10412905.1993.9698245 . [all data]


Notes

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