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«alpha»-Cubebene


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxDB-WaxBP-20DB-WaxRTX-Wax
Column length (m) 60.30. 30.60.
Carrier gas HeliumHeliumNitrogenHydrogenHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.22
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.40.60.30.60.
Tend (C) 220.230.200.230.230.
Heat rate (K/min) 5.4.5.8.2.
Initial hold (min) 1.2. 5. 
Final hold (min) 5.4.5 10.30.
I 1462.1480.1455.1460.1435.
ReferenceFeng, Cui, et al., 2011Zeng, Xie, et al., 2011Mishra, Chaudhary, et al., 2010Karlsson, Birgersson, et al., 2009Museli, Pau, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxRTX-WaxHP-InnowaxHP-20MTC-FFAP
Column length (m) 30.60.30.50. 
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.20.25
Phase thickness (mum) 0.250.250.250.20.25
Tstart (C) 50.60.60.70.60.
Tend (C) 240.230.240.180.220.
Heat rate (K/min) 15.2.2.4.3.
Initial hold (min) 10.  4. 
Final hold (min) 19.35.20. 30.
I 1463.1460.1461.1428.1460.
ReferenceCharoensiddhi and Anprung, 2008Paolini, Tomi, et al., 2008Hachicha, Skanji, et al., 2007Jerkovic, Mastelic, et al., 2007Kurose, Okamura, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-FFAPSupelcowax-10CP-Wax 52CBSupelcowax-10Innowax
Column length (m)  30.60.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.20.320.250.25
Phase thickness (mum) 0.250.20.50.250.25
Tstart (C) 60.70.40.40.50.
Tend (C) 220.220.220.250.280.
Heat rate (K/min) 3.3.4.3.9.
Initial hold (min)   8.5.3.
Final hold (min) 30.15.20.10.3.
I 1459.1457.1466.1446.1455.
ReferenceKurose, Okamura, et al., 2007Pinto, Salgueiro, et al., 2007Povolo, Contarini, et al., 2007Vichi, Riu-Aumatell, et al., 2007Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxAT-WaxBP-20Supelcowax 10BP-20
Column length (m) 30.60.50.30.50.
Carrier gas N2He HeliumHe
Substrate      
Column diameter (mm) 0.250.250.220.200.22
Phase thickness (mum) 0.250.250.250.200.25
Tstart (C) 50.60.60.70.60.
Tend (C) 280.200.220.220.220.
Heat rate (K/min) 9.4.2.3.2.
Initial hold (min) 3.    
Final hold (min) 3.20.20.15.20.
I 1458.1465.1456.1455.1454.
ReferenceAbdelwahed, Hayder, et al., 2006Borges, Rojas, et al., 2006Boti, Yao, et al., 2006Cavaleiro, Pinto, et al., 2006Lesueur, Ban, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Carbowax 20MStabilwaxStabilwaxCarbowax
Column length (m) 30.50.30.30.30.
Carrier gas He H2  
Substrate      
Column diameter (mm) 0.250.20.320.320.25
Phase thickness (mum) 0.250.250.50.50.25
Tstart (C) 50.60.40.40.40.
Tend (C) 220.250.280.280.200.
Heat rate (K/min) 4.2.6.6.4.
Initial hold (min) 1.60.5.5. 
Final hold (min) 10. 5.5. 
I 1451.1425.1481.1481.1480.
ReferenceWong, Lim, et al., 2006Fernandez, Lizzani-Cuvelier, et al., 2005Jirovetz, Buchbauer, et al., 2005Jirovetz, Buchbauer, et al., 2005, 2Szafranek, Chrapkowska, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10DB-WaxDB-WaxSupelcowax-10DB-Wax
Column length (m) 30.60.60.60.60.
Carrier gas  N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.250.2 
Tstart (C) 40.70.70.60.60.
Tend (C) 220.230.230.200.220.
Heat rate (K/min) 3.2.2.4.2.
Initial hold (min) 5.2.2. 4.
Final hold (min) 10.20.20.40. 
I 1446.1469.1467.1438.1469.
ReferenceVichi, Riu-Aumatell, et al., 2005Choi, 2004Choi, 2004, 2Gauvin, Ravaomanarivo, et al., 2004Jiang and Kubota, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MSupelcowax-10TC-WaxRTX-Wax
Column length (m) 60.30.50.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum)  0.250.25 0.5
Tstart (C) 60.60.70.80.40.
Tend (C) 220.250.230.240.180.
Heat rate (K/min) 2.3.2.3.5.
Initial hold (min) 4.   5.
Final hold (min)     20.
I 1469.1443.1453.1462.1483.
ReferenceJiang and Kubota, 2004Lago, de Ávila, et al., 2004Orav, Stulova, et al., 2004Miyazawa, Teranishi, et al., 2003Galindo-Cuspinera, Lubran, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.60.30.60.60.
Carrier gas N2HeHeHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (mum) 0.250.25 0.25 
Tstart (C) 70.45.50.50.40.
Tend (C) 230.240.180.230.200.
Heat rate (K/min) 2.3.3.5.2.
Initial hold (min)   8.2.10.
Final hold (min)      
I 1468.1460.1435.1456.1468.
ReferenceTu, Thanh, et al., 2002Christoph, 2001Franco and Shibamoto, 2000Paniandy, Chane-Ming, et al., 2000Tamura, Boonbumrung, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20HP Innowax FSPInnowaxHP-InnowaxDB-Wax
Column length (m) 25.60.60.60.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.330.250.250.250.25
Phase thickness (mum) 0.50.250.250.250.25
Tstart (C) 80.60.60.60.60.
Tend (C) 220.220.220.220.240.
Heat rate (K/min) 5.   4.
Initial hold (min)  10.10.10. 
Final hold (min)  10.   
I 1480.1466.1466.1466.1464.
ReferenceDunlop, Bignell, et al., 1999Kaya, Baser, et al., 1999Kaya, Baser, et al., 1999, 2Kaya, Baser, et al., 1999, 3Ngassoum, Yonkeu, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20HP-20MDB-WaxHP-InnowaxHP-Innowax FSC
Column length (m) 25.50.30.60.60.
Carrier gas H2HeN2HeHe
Substrate      
Column diameter (mm) 0.330.20.250.250.25
Phase thickness (mum) 0.50.20.250.250.25
Tstart (C) 80.70.45.50.60.
Tend (C) 220.180.220.220.220.
Heat rate (K/min) 5.4.3.5.4.
Initial hold (min)  4. 5.10.
Final hold (min)  10.  10.
I 1480.1433.1469.1458.1466.
ReferenceBignell, Dunlop, et al., 1998Milso, Mastelic, et al., 1998Molleken U., Sinnwell V., et al., 1998Stashenko, Cervantes, et al., 1998Tümen, Baser, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20BP-20BP-20BP-20
Column length (m) 25.25.25.25.25.
Carrier gas H2H2H2H2 
Substrate      
Column diameter (mm) 0.330.330.330.330.33
Phase thickness (mum) 0.50.50.50.50.5
Tstart (C) 80.80.80.80.80.
Tend (C) 220.220.220.220.220.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min)      
Final hold (min)      
I 1480.1480.1480.1480.1480.
ReferenceBignell, Dunlop, et al., 1997Bignell, Dunlop, et al., 1997, 2Bignell, Dunlop, et al., 1997, 3Bignell, Dunlop, et al., 1997, 4Bignell, Dunlop, et al., 1997, 5
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20Supelcowax-10Supelcowax-10SP-1000DB-Wax
Column length (m) 25.30.0.85.60.
Carrier gas H2 HeHeHe
Substrate      
Column diameter (mm) 0.330.250.250.500.32
Phase thickness (mum) 0.5   0.50
Tstart (C) 80.60.40.65.50.
Tend (C) 220.240.240.225.250.
Heat rate (K/min) 5.4.3.3.8.
Initial hold (min)     1.
Final hold (min)     6.
I 1480.1458.1475.1468.1455.
ReferenceBignell, Dunlop, et al., 1997, 6Zunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Brophy, Goldsack, et al., 1996Sagrero-Nieves and Bartley, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Carbowax 20MDB-WaxDB-WaxDB-Wax
Column length (m) 60.45.60.30.60.
Carrier gas HeHydrogen   
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (mum) 0.251.0   
Tstart (C) 40.60.50.70.50.
Tend (C) 200.200.230.200.250.
Heat rate (K/min) 3.2.4.4.4.
Initial hold (min) 3.5. 2.0.1
Final hold (min) 30. 10. 5.
I 1475.1453.1455.1464.1454.
ReferenceWong and Lai, 1996Kollmannsberger, Nitz, et al., 1992Binder, Turner, et al., 1990Wyllie, Brophy, et al., 1990Binder and Flath, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FFAPCarbowax 20MSupelcowax-10Supelcowax-10Carbowax 20M
Column length (m) 50.50.30.30.150.
Carrier gas  H2 He 
Substrate      
Column diameter (mm)  0.32  0.66
Phase thickness (mum)  0.15   
Tstart (C) 50.70.50.50.60.
Tend (C) 180.210.240.240.170.
Heat rate (K/min) 10.2.4.4.1.
Initial hold (min) 1. 2.2.40.
Final hold (min)   10.10. 
I 1479.1445.1458.1458.1420.
ReferenceBrophy, Davies, et al., 1989Gaydou, Faure, et al., 1989Ramaswami, Briscese, et al., 1988Ramaswami, Briscese, et al., 1986Buttery, Xu, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase Carbowax 20M
Column length (m) 50.
Carrier gas  
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum)  
Tstart (C) 70.
Tend (C) 180.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 1431.
ReferenceTressl, Engel, et al., 1983
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Feng, Cui, et al., 2011
Feng, T.; Cui, J.-J.; Xiao, Z.-B.; Tian, H.-X.; Yi, F.-P.; Ma, X., Chemical composition od essential oil from the peel of Chinese Torreya grandis Frt, Org. Chem. International, 2011, 2011, 1-5, https://doi.org/10.1155/2011/187372 . [all data]

Zeng, Xie, et al., 2011
Zeng, Z.; Xie, R.; Zhang, T.; Zhang, H.; Chen, J.Y., Analysis of volatile compositions of Magnolia biondii Pamp by steam distillation and Headspace solid phase micro-extraction, J. Oleo Sci., 2011, 60, 12, 591-596, https://doi.org/10.5650/jos.60.591 . [all data]

Mishra, Chaudhary, et al., 2010
Mishra, R.K.; Chaudhary, S.; Pandey, R.; Gupta, S.; Mallavarapu, G.R.; Kumar, S., Analysis of linalool content in the inflorescence (flower) essential oil and leaf oil of Lippia alba cultivar Kavach, J. Essen. Oil Res., 2010, 22, 1, 3-7, https://doi.org/10.1080/10412905.2010.9700253 . [all data]

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Karlsson, M.F.; Birgersson, G.; Prado, A.M.C.; Bosa, F.; Bengtsson, M.; Witzgall, P., Plant Odor Analysis of Potato: Responce of Guatemalan Moth to Above- and Background Potato Volatiles, J. Agric. Food Chem., 2009, 57, 13, 5903-5909, https://doi.org/10.1021/jf803730h . [all data]

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Charoensiddhi and Anprung, 2008
Charoensiddhi, S.; Anprung, P., Bioacrive compounds and volatile compounds of Thai bael fruit (Aegle marmelos (L.) Correa) as a valuable source for functional food ingredients, Internat. Food Res. J., 2008, 15, 3, 287-295. [all data]

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Hachicha, Skanji, et al., 2007
Hachicha, S.F.; Skanji, T.; Barrek, S.; Ghrabi, Z.G.; Zarrouk, H., Composition of the essential oil of Teucrium ramosissimum Desf. (Lamiaceae) from Tunisia, Flavour Fragr. J., 2007, 22, 2, 101-104, https://doi.org/10.1002/ffj.1764 . [all data]

Jerkovic, Mastelic, et al., 2007
Jerkovic, I.; Mastelic, J.; Marijanovic, Z., Bound volatile compounds and essential oil from the fruit of Maclura pomifera (Raf.) Schneid. (osage orange), Flavour Fragr. J., 2007, 22, 1, 84-88, https://doi.org/10.1002/ffj.1763 . [all data]

Kurose, Okamura, et al., 2007
Kurose, K.; Okamura, D.; Yatagai, M., Composition of the essential oils from the leaves of nine Pinus species and the cones of three of Pinus species, Flavour Fragr. J., 2007, 22, 1, 10-20, https://doi.org/10.1002/ffj.1609 . [all data]

Pinto, Salgueiro, et al., 2007
Pinto, E.; Salgueiro, L.R.; Cavaleiro, C.; Palmeira, A.; Goncalves, M.J., In vitro susceptibility of some species of yeasts and filamentous fungi to essential oils of Salvia of?cinalis, Ind. Crops Prod., 2007, 26, 2, 135-141, https://doi.org/10.1016/j.indcrop.2007.02.004 . [all data]

Povolo, Contarini, et al., 2007
Povolo, M.; Contarini, G.; Mele, M.; Secchiari, P., Study on the influence of pasture on volatile fraction of Ewes' dairy products by solid-phase microextraction and gas chromatography-mass spectrometry, J. Dairy Sci., 2007, 90, 2, 556-569, https://doi.org/10.3168/jds.S0022-0302(07)71539-4 . [all data]

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Abdelwahed, Hayder, et al., 2006
Abdelwahed, A.; Hayder, N.; Kilani, S.; Mahmoud, A.; Chibani, J.; Hammami, M.; Chekir-Ghedira, L.; Ghedira, K., Chemical composition and antimicrobial activity of essential oils from Tunisian Pituranthos tortuosus (Coss.) Maire, Flavour Fragr. J., 2006, 21, 1, 129-133, https://doi.org/10.1002/ffj.1542 . [all data]

Borges, Rojas, et al., 2006
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Boti, Yao, et al., 2006
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Cavaleiro, Pinto, et al., 2006
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Lesueur, Ban, et al., 2006
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Wong, Lim, et al., 2006
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Fernandez, Lizzani-Cuvelier, et al., 2005
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Jirovetz, Buchbauer, et al., 2005
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Jirovetz, Buchbauer, et al., 2005, 2
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Szafranek, Chrapkowska, et al., 2005
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Vichi, Riu-Aumatell, et al., 2005
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Choi, 2004
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Choi, 2004, 2
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Gauvin, Ravaomanarivo, et al., 2004
Gauvin, A.; Ravaomanarivo, H.; Smadja, J., Comparative analysis by gas chromatography?mass spectrometry of the essential oils from bark and leaves of Cedrelopsis grevei Baill, an aromatic and medicinal plant from Madagascar, J. Chromatogr. A, 2004, 1029, 1-2, 279-282, https://doi.org/10.1016/j.chroma.2003.12.012 . [all data]

Jiang and Kubota, 2004
Jiang, L.; Kubota, K., Differences in the volatile components and their odor characteristics of green and ripe fruits and dried pericarp of Japanese pepper (Xanthoxylum piperitum DC.), J. Agric. Food Chem., 2004, 52, 13, 4197-4203, https://doi.org/10.1021/jf030663a . [all data]

Lago, de Ávila, et al., 2004
Lago, J.H.G.; de Ávila, P., Jr.; de Aquino, E.M.; Moreno, P.R.H.; Ohara, M.T.; Limberger, R.P.; Apel, M.A.; Henriques, A.T., Volatile oils from leaves and stem barks of Cedrela fissilis (Meliaceae): chemical composition and antibacterial activities, Flavour Fragr. J., 2004, 19, 5, 448-451, https://doi.org/10.1002/ffj.1347 . [all data]

Orav, Stulova, et al., 2004
Orav, A.; Stulova, I.; Kailas, T.; Müürisepp, M., Effect of storage on the essential oil composition of piper nigrum L. fruits of different ripening states, J. Agric. Food Chem., 2004, 52, 9, 2582-2586, https://doi.org/10.1021/jf030635s . [all data]

Miyazawa, Teranishi, et al., 2003
Miyazawa, M.; Teranishi, A.; Ishikawa, Y., Components of the essential oil from Petasites japonicus, Flavour Fragr. J., 2003, 18, 3, 231-233, https://doi.org/10.1002/ffj.1203 . [all data]

Galindo-Cuspinera, Lubran, et al., 2002
Galindo-Cuspinera, V.; Lubran, M.B.; Rankin, S.A., Comparison of volatile compounds in water- and oil-soluble annatto (Bixa orellana L.) extracts, J. Agric. Food Chem., 2002, 50, 7, 2010-2015, https://doi.org/10.1021/jf011325h . [all data]

Tu, Thanh, et al., 2002
Tu, N.T.M.; Thanh, L.X.; Une, A.; Ukeda, H.; Sawamura, M., Volatile constituents of Vietnamese pummelo, orange, tangerine and lime peel oils, Flavour Fragr. J., 2002, 17, 3, 169-174, https://doi.org/10.1002/ffj.1076 . [all data]

Christoph, 2001
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Notes

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