α-Cubebene


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5HP-5HP-5
Column length (m) 30.30.25.25.25.
Carrier gas HeliumHeliumHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.520.520.52
Tstart (C) 60.40.40.40.40.
Tend (C) 240.250.280.280.280.
Heat rate (K/min) 3.3.4.4.4.
Initial hold (min)  1.   
Final hold (min)  3.10.10.10.
I 1349.1343.1344.1344.1344.
ReferenceRodriques, Amorim, et al., 2013Jian-Yu, Zhu, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DP-5HP-5 MSHP-5 MSDB-5CP-Sil 5 CB
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.26
Tstart (C) 80.60.50.60.45.
Tend (C) 300.220.180.240.280.
Heat rate (K/min) 4.4.2.3.3.
Initial hold (min) 1.20.   
Final hold (min) 40.20.  22.
I 1344.1360.1337.1351.1352.
ReferenceVijayakumar, Duraipandiyan, et al., 2012Feizbakhsh and Naeemy, 2011Hammami, Kamoun, et al., 2011Karimi, Farmani, et al., 2011Mothana, Hasson, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5DB-5Elite-5 MSDB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.60.40.50.60.
Tend (C) 200.250.220.250.240.
Heat rate (K/min) 5.4.4.2.3.
Initial hold (min) 5.1.  2.
Final hold (min) 5.10.   
I 1360.1356.1376.1351.1351.
ReferenceVazquez, Demmel, et al., 2011Yousefzadi, Heidari, et al., 2011Baharum, Bunawan, et al., 2010Ho, Wang, et al., 2010Kahriman, Tosun, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5 MSHP-5HP-5 MSDB-5
Column length (m)  30.30.30.30.
Carrier gas NitrogenHeliumHydrogenHeliumHelium
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.100.70.70.60.
Tend (C) 220.220.290.290.240.
Heat rate (K/min) 5.2.5.5.3.
Initial hold (min) 10.    
Final hold (min) 30.  10. 
I 1351.1344.1355.1350.1353.
ReferenceMishra, Chaudhary, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2Scherer, Wagner, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5DB-1-MSDB-5SE-54
Column length (m) 30.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.30.40.60.
Tend (C) 240.240.200.250.260.
Heat rate (K/min) 3.3.2.10.2.
Initial hold (min)  1.4.1.5.
Final hold (min)   35.3.999.
I 1347.1345.1343.1390.1347.
ReferenceSilva, Pott, et al., 2010de Souza, Lopes, et al., 2010Takeoka, Hobbs, et al., 2010Yang, Zhang, et al., 2010Dayisoylu and Alma, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5 MSRTX-1RTX-1
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHydrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.50.30.60.60.
Tend (C) 220.250.230.230.230.
Heat rate (K/min) 3.5.8.2.2.
Initial hold (min)  2.5.  
Final hold (min) 40. 10.30.30.
I 1354.1351.1361.1346.1355.
ReferenceEl-Massry, El-Ghorab, et al., 2009Ho, Wang, et al., 2009Karlsson, Birgersson, et al., 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSSE-52SLB-5 MSDB-5 MS
Column length (m) 30.30.50.30.30.
Carrier gas HeliumHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.60.50.50.
Tend (C) 240.250.280.250.300.
Heat rate (K/min) 3.2.3.3.5.
Initial hold (min) 1.5. 2.5.
Final hold (min)   20.10.5.
I 1345.1382.1353.1348.1340.
Referencede Souza, Lopes, et al., 2009Cheng, Liu, et al., 2008Djarri, Medjroubi, et al., 2008Lo Presti, Sciarrone, et al., 2008Noudogbessi, Yedomonhan, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5 MSBPX-5HP-5HP-5 MS
Column length (m) 60.30.7.530.30.
Carrier gas HeHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.250.100.250.25
Phase thickness (μm) 0.250.2510.0.320.25
Tstart (C) 60.50.60.60.50.
Tend (C) 230.240.240.250.230.
Heat rate (K/min) 2.3.3.5.3.
Initial hold (min)    30.10.
Final hold (min) 35.   10.
I 1350.1371.1349.1350.1351.
ReferencePaolini, Tomi, et al., 2008Sarikurkcu, Tepe, et al., 2008Shellie, 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.260.260.25
Phase thickness (μm) 0.250.250.250.250.26
Tstart (C) 60.60.60.60.60.
Tend (C) 240.280.240.290.240.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)     2.
Final hold (min)     20.
I 1345.1350.1351.1351.1350.
ReferenceArgyropoulou, Daferera, et al., 2007Basta, Pavlovic, et al., 2007Bos, Woerdenbag, et al., 2007Elfami, Bos, et al., 2007Farsam, Amanlou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-101SE-30HP-5ZB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 60.70.40.40.60.
Tend (C) 240.200.250.250.220.
Heat rate (K/min) 2.3.5.5.4.
Initial hold (min)  2.5.5.5.
Final hold (min) 20. 10.10.20.
I 1340.1319.1351.1340.1349.
ReferenceHachicha, Skanji, et al., 2007Jerkovic, Mastelic, et al., 2007Loizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1BPX-5DB-5Elite-5MSHP-5MS
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.220.250.320.25
Phase thickness (μm) 0.2 0.250.50.25
Tstart (C) 70.50.60.40.40.
Tend (C) 220.300.320.280.250.
Heat rate (K/min) 3.4.10.4.3.
Initial hold (min)  1. 5.5.
Final hold (min) 15.10.4.10.10.
I 1344.1375.1350.1349.1340.
ReferencePinto, Salgueiro, et al., 2007Rali, Wossa, et al., 2007Smelcerovic, Spiteller, et al., 2007Tava, Pecetti, et al., 2007Vichi, Riu-Aumatell, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5AT-5BP-1
Column length (m) 30.30.30.60.50.
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.50.50.60.60.
Tend (C) 250.280.280.200.220.
Heat rate (K/min) 5.9.9.4.2.
Initial hold (min) 30.3.3.  
Final hold (min)  3.3.20.20.
I 1350.1349.1365.1351.1350.
ReferenceYassa and Akhani, 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Borges, Rojas, et al., 2006Boti, Yao, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5DB-5DB-5HP-5
Column length (m) 30.25.30.30.30.
Carrier gas HeliumHe HeliumHe
Substrate      
Column diameter (mm) 0.200.250.320.260.25
Phase thickness (μm) 0.200.250.250.250.25
Tstart (C) 70.50.60.60.50.
Tend (C) 220.300.230.290.300.
Heat rate (K/min) 3.5.3.3.5.
Initial hold (min)  5.  5.
Final hold (min) 15. 15. 5.
I 1342.1351.1351.1351.1347.
ReferenceCavaleiro, Pinto, et al., 2006Champagnat, Figueredo, et al., 2006Damjanovic, Skala, et al., 2006Elfami, Komar, et al., 2006Figuérédo, Cabassu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5BP-1DB-5
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.100.60.60.
Tend (C) 260.260.240.220.220.
Heat rate (K/min) 3.5.5.2.4.
Initial hold (min)  2.2. 5.
Final hold (min)  13.5.20. 
I 1386.1353.1351.1348.1353.
ReferenceJavidnia, Miri, et al., 2006Kucuk, Gulec, et al., 2006Lago, Soares, et al., 2006Lesueur, Ban, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-5HP-5MS
Column length (m) 25.50.30.30.30.
Carrier gas N2N2HydrogenHydrogenHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.150.250.250.250.25
Tstart (C) 50.95.70.70.60.
Tend (C) 200.240.280.280.280.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min) 3. 4.4. 
Final hold (min)      
I 1345.1349.1352.1351.1314.
ReferenceOuamba, Ouabonzi, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FSOT-RSL-200HP-5Methyl SiliconeDB-5DB-1
Column length (m) 30.25.25.30.50.
Carrier gas HydrogenN2N2N2N2
Substrate      
Column diameter (mm) 0.320.20.30.250.25
Phase thickness (μm) 0.250.330.150.250.25
Tstart (C) 40.30.50.60.90.
Tend (C) 280.280.210.240.240.
Heat rate (K/min) 6.3.2.4.4.
Initial hold (min) 5. 5.  
Final hold (min) 5.    
I 1350.1359.1361.1351.1341.
ReferenceSchmidt, Jirovetz, et al., 2006Shafi, Jose, et al., 2006Tonzibo, Coffy, et al., 2006Trilles, Bombarda, et al., 2006Velasco-Negueruela, Pérez-Alonso, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1DB-5DB-5DB-5
Column length (m) 25.50.25.30.30.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (μm) 0.520.330.150.250.25
Tstart (C) 50.50.40.60.60.
Tend (C) 280.220.220.240.240.
Heat rate (K/min) 2.54.3.3.3.
Initial hold (min) 5.1.5.  
Final hold (min)  10.   
I 1350.1345.1345.1350.1351.
ReferenceWang, Kong, et al., 2006Wong, Lim, et al., 2006Chagonda and Chalchat, 2005Chaverri and Cicció, 2005Chaverri and Cicció, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-1HP-5DB-1DB-5MS
Column length (m) 60.50.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 40.60.50.50.60.
Tend (C) 230.250.300.265.280.
Heat rate (K/min) 3.2.5.2.53.
Initial hold (min) 5.60.5.1.30.
Final hold (min)   5.20. 
I 1385.1356.1347.1348.1325.
ReferenceCornu, Kondjoyan, et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005Figuérédo, Cabassu, et al., 2005Khanavi, Ghasemian, et al., 2005Marongiu, Piras, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBDB-1RTX-5 MSDB-5
Column length (m) 30.25.50.30.25.
Carrier gas He N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.150.250.250.25
Tstart (C) 60.50.95.50.60.
Tend (C) 220.230.240.280.200.
Heat rate (K/min) 4.3.4.8.2.
Initial hold (min) 4.  2. 
Final hold (min)    2.80.
I 1353.1351.1345.1356.1346.
ReferenceMorteza-Semnani and Saeedi, 2005Olawore, Ogunwande, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005Pellati, Benvenuti, et al., 2005Rout, Misra, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSBP-1CP Sil 8 CB
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.40.60.60.60.
Tend (C) 275.260.280.220.290.
Heat rate (K/min) 4.2.3.5.3.
Initial hold (min)  5.  5.
Final hold (min)  20. 15. 
I 1348.1353.1351.1359.1382.
ReferenceSajjadi and Ghannadi, 2005Senatore, Apostolides Arnold, et al., 2005Slavkovska, Couladis, et al., 2005Srivastava, Srivastava, et al., 2005Suárez, Vásquez, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5MSHP-5 MSDB-5DB-1
Column length (m) 30.30.30.30.50.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.500.250.25
Tstart (C) 60.50.60.60.90.
Tend (C) 220.240.260.280.240.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)  3.   
Final hold (min)   20.  
I 1349.1400.1391.1318.1341.
ReferenceSzafranek, Chrapkowska, et al., 2005Tepe B., Sokmen M., et al., 2005Topçu, Barla, et al., 2005Tzakou and Constantinidis, 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSCP Sil 5 CBDB-1DB-1
Column length (m) 50.30.30.60.30.
Carrier gas   N2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.50.70.50.
Tend (C) 240.220.200.230.200.
Heat rate (K/min) 3.3.5.2.5.
Initial hold (min)  5. 2. 
Final hold (min)  10. 20. 
I 1331.1340.1333.1360.1369.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2005, 2Vichi, Riu-Aumatell, et al., 2005Agnaniet, Menut, et al., 2004Choi, 2004Fekam Boyom, Fotio, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5RTX-1DB-5DB-5
Column length (m) 60.25.30.30.30.
Carrier gas HeNitrogenN2HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 200.240.300.300.300.
Heat rate (K/min) 4.3.4.3.3.
Initial hold (min)      
Final hold (min) 30.    
I 1354.1348.1354.1336.1330.
ReferenceGauvin, Ravaomanarivo, et al., 2004JAvidnia, Mojab, et al., 2004Kalemba and Thiem, 2004Lago, de Ávila, et al., 2004Limberger, Sobral, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1NB-30NB-30HP-5MSHP-5
Column length (m) 30.50.50.30.25.
Carrier gas N2HeHeHeH2
Substrate      
Column diameter (mm) 0.320.20.20.250.32
Phase thickness (μm) 0.250.250.250.250.52
Tstart (C) 60.50.50.60.40.
Tend (C) 300.250.250.280.240.
Heat rate (K/min) 4.2.2.4.4.
Initial hold (min)      
Final hold (min)      
I 1348.1377.1346.1350.1351.
ReferenceLis, Boczek, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004Sajjadi and Shahpiri, 2004Simic, Sokovic, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5HP-5HP-5DB-1
Column length (m) 20.30.30.30.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 100.60.60.100.70.
Tend (C) 270.300.220.240.230.
Heat rate (K/min) 8.3.5.5.2.
Initial hold (min) 2. 10.2.2.
Final hold (min)    5.20.
I 1362.1351.1364.1351.1360.
ReferenceThappa, Bakshi, et al., 2004Tirillini, Pellegrino, et al., 2004Bertoli, Menichini, et al., 2003Chaves, Lago, et al., 2003Choi, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-1DB-1HP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.70.50.60.60.
Tend (C) 280.200.200.280.275.
Heat rate (K/min) 3.10.5.4.4.
Initial hold (min)      
Final hold (min)      
I 1349.1369.1347.1351.1354.
ReferenceCouladis, Özcan, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003Fekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003Ghannadi and Zolfaghari, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200CP Sil 5 CBDB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas H2H2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.390.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 280.280.220.250.280.
Heat rate (K/min) 6.6.5.3.3.
Initial hold (min) 5.5.   
Final hold (min) 5.5.  30.
I 1351.1360.1354.1340.1343.
ReferenceJirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Khanavi, Hadjiakhoondi, et al., 2003Limberger, Simões-Pires, et al., 2003Marongiu, Porcedda, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1CP Sil 5 CBDB-5HP-5
Column length (m) 30.60.25.30.30.
Carrier gas HeHeH2H2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.150.250.25
Tstart (C) 60.50.50.60.60.
Tend (C) 280.270.230.280.280.
Heat rate (K/min) 3.4.3.4.3.
Initial hold (min)    10. 
Final hold (min) 30.  40. 
I 1340.1350.1354.1352.1341.
ReferenceMarongiu, Porcedda, et al., 2003Mirza, Nik, et al., 2003Oyedeji, Ekundayo, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSCross-Linked MethylsiliconeHP-5HP-5
Column length (m) 30.30.25.25.25.
Carrier gas  HeHeH2H2
Substrate      
Column diameter (mm) 0.250.250.20.320.32
Phase thickness (μm) 0.250.250.330.530.53
Tstart (C) 40.60.70.40.40.
Tend (C) 260.240.250.280.280.
Heat rate (K/min) 2.3.4.4.4.
Initial hold (min) 5.    
Final hold (min)      
I 1358.1350.1341.1348.1351.
ReferenceSenatore and Bruno, 2003Taveira, de Lima, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5DB-5
Column length (m) 25.25.25.30.30.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.530.530.530.320.25
Tstart (C) 40.40.40.60.60.
Tend (C) 280.280.280.250.240.
Heat rate (K/min) 4.4.4.5.3.
Initial hold (min)    30. 
Final hold (min)      
I 1346.1347.1351.1357.1348.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Yassa, Akhani, et al., 2003Zoghbi, Andrade, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101HP-15 % Phenyl methyl siloxaneDB-5MSDB-5MS
Column length (m) 25.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.70.75.60.60.
Tend (C) 200.220.200.280.280.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min)   4.  
Final hold (min)  15.8.  
I 1369.1342.1351.1350.1350.
ReferenceBoyom, Keumedjio, et al., 2002Cavaleiro, Salgueiro, et al., 2002Cicció and Gómez-Laurito, 2002Congiu, Falconieri, et al., 2002Congiu, Falconieri, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5PTE-5SE-30RSL-200DB-1
Column length (m) 30.60.50.30.25.
Carrier gas HeH2HeH2He
Substrate      
Column diameter (mm) 0.250.320.250.320.23
Phase thickness (μm) 0.250.300.250.250.20
Tstart (C) 60.60.70.40.50.
Tend (C) 240.285.240.280.200.
Heat rate (K/min) 3.4.34.6.3.
Initial hold (min)    5.3.
Final hold (min)    5.30.
I 1353.1351.1349.1351.1354.
ReferenceFlamini, Ertugrul, et al., 2002Gudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002Khallouki, Younos, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5MSOV-101DB-1
Column length (m) 30.30.30.25.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 100.60.60.50.60.
Tend (C) 240.240.240.200.250.
Heat rate (K/min) 5.3.3.5.4.
Initial hold (min) 2.   10.
Final hold (min) 5.    
I 1343.1354.1350.1349.1381.
ReferenceLago, Reis, et al., 2002Maia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002Menut, Bessière, et al., 2002Norouzi-Arasi, Yavari, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5DB-5MSDB-5
Column length (m) 25.50.30.30.30.
Carrier gas HeN2H2HeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 220.240.280.270.240.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min)      
Final hold (min)      
I 1351.1331.1351.1349.1350.
ReferenceSchwob, Bessière, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Velickovic, Randjelovic, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5OV-1HP-5
Column length (m) 60.60.30.30.30.
Carrier gas HeHeN2H2N2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.30.25
Tstart (C) 40.40.60.50.60.
Tend (C) 280.280.220.250.220.
Heat rate (K/min) 4.4.5.3.5.
Initial hold (min) 5.5.10.1.10.
Final hold (min)    20. 
I 1349.1352.1351.1363.1353.
ReferenceDabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001Flamini, Cioni, et al., 2001Gallori, Bilia, et al., 2001Gallori, Flamini, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1Optima-5RTX-1DB-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas N2HeN2HeN2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.50.60.60.80.
Tend (C) 220.250.300.240.225.
Heat rate (K/min) 5.3.4.3.4.
Initial hold (min)  3.   
Final hold (min)    30. 
I 1352.1354.1355.1331.1338.
ReferenceGupta, Mallavarapu, et al., 2001Jacquemond-Collet, Bessière, et al., 2001Kalemba, Marschall, et al., 2001Marongiu, Porcedda, et al., 2001Palá-Paúl, Pérez-Alonso, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBCP-Sil 5 CBHP-5 MSDB-5
Column length (m) 30.25.25.30.30.
Carrier gas HeHeNitrogenHeliumHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm)  0.390.390.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.220.220.250.240.
Heat rate (K/min) 3.5.5.5.3.
Initial hold (min)    2. 
Final hold (min)    5. 
I 1344.01333.1333.1360.1352.
ReferenceSantos, Moreira, et al., 2001Sayyah, Kamalinejad, et al., 2001Sayyah, Kamalinejad, et al., 2001, 2Shang, Hu, et al., 2001Tellez M., Estell R., et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RSL-200DB-5OV-101SE-30
Column length (m) 30.60.30.50.25.
Carrier gas H2H2N2NitrogenHe
Substrate      
Column diameter (mm) 0.250.320.220.250.2
Phase thickness (μm) 0.250.250.25  
Tstart (C) 40.40.70.40.60.
Tend (C) 280.250.230.200.230.
Heat rate (K/min) 3.6.4.2.3.
Initial hold (min) 10. 2.10. 
Final hold (min) 10. 20.  
I 1348.1370.1351.1381.1365.
ReferenceBicalho, Pereira, et al., 2000Jirovetz, Puschmann, et al., 2000Mitiku, Sawamura, et al., 2000Tamura, Boonbumrung, et al., 2000Ali N.A.M. and Jantan, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBOV-101SE-30OV-1DB-1
Column length (m) 25.25.25.25.50.
Carrier gas H2N2HeH2He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.15  0.250.25
Tstart (C) 50.50.60.40.70.
Tend (C) 320.200.230.220.240.
Heat rate (K/min) 3.5.3.3.4.
Initial hold (min)   10.5. 
Final hold (min)    5. 
I 1343.1352.1365.1369.1338.
ReferenceAsekun and Ekundayo, 1999Ayedoun, Adéoti, et al., 1999Mohd and Jantan, 1999Oberhofer, Nikiforov, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-30Ultra-2CP Sil 5 CBDB-1
Column length (m) 30.30.25.25.60.
Carrier gas HeHelium HeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.20 0.390.25
Tstart (C) 40.60.40.60.40.
Tend (C) 250.200.300.220.280.
Heat rate (K/min) 2.3.5.5.4.
Initial hold (min) 5.4.4.5.5.
Final hold (min) 60.  20. 
I 1367.1392.1356.1361.1381.
ReferencePorta, Porcedda, et al., 1999Prikhod'ko, Klyuev, et al., 1999Quiroz, Fuentes-Contreras, et al., 1999Rustaiyan, Masoudi, et al., 1999Sefidkon, Dabiri, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-5MSSPB-5
Column length (m) 30.60.30.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.60.60.60.
Tend (C) 220.220.240.240.240.
Heat rate (K/min) 4.4.3.3.3.
Initial hold (min) 5.    
Final hold (min)     20.
I 1347.1357.1351.1348.1355.
ReferenceSefidkon and Khajavi, 1999Sefidkon and Mirza, 1999Tellez, Canel, et al., 1999Zoghbi, Andrade, et al., 1999Doneanu and Anitescu, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-1OV-101DB-5OV-1
Column length (m) 25.60.25.30.30.
Carrier gas HeHe He 
Substrate      
Column diameter (mm) 0.20.250.320.250.32
Phase thickness (μm) 0.20.25 0.250.25
Tstart (C) 70.50.50.65.40.
Tend (C) 200.280.200.300.270.
Heat rate (K/min) 3.4.5.4.2.
Initial hold (min) 2.5. 2.4.
Final hold (min) 10.    
I 1342.1381.1352.1355.1336.
ReferenceMilso, Mastelic, et al., 1998Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998Elias, Simoneit, et al., 1997Kökdil, Tanker, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-SulfurSPB-SulfurDB-1DB-5DB-5
Column length (m) 30.30. 30.30.
Carrier gas HeHe HeliumHe
Substrate      
Column diameter (mm) 0.320.32 0.250.25
Phase thickness (μm) 4.4. 0.25 
Tstart (C) 45.45.80.60.60.
Tend (C) 240.240.220.240.240.
Heat rate (K/min) 5.5.6.3.4.
Initial hold (min) 13.13.   
Final hold (min) 5.5.   
I 1381.1382.1345.1352.1353.
ReferenceMariaca, Berger, et al., 1997Mariaca, Berger, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Zunino, Novillo-Newton, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1OV-101DB-5OV-101DB-1
Column length (m) 25.50.30.50.60.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.32
Phase thickness (μm)  0.170.25 0.50
Tstart (C) 60.50.60.50.50.
Tend (C) 240.220.300.250.250.
Heat rate (K/min) 5.5.4.2.8.
Initial hold (min)   2. 1.
Final hold (min)   5. 6.
I 1365.1366.1348.21345.1383.
ReferenceZygadlo, Ariza-Espinar, et al., 1997Chacko, Jayalekshmy, et al., 1996Gawdzik, Mardarowicz, et al., 1996Orav, Kailas, et al., 1996Sagrero-Nieves and Bartley, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1Methyl SiliconeMethyl SiliconeSPB-5SE-54
Column length (m) 25.50.50.30.30.
Carrier gas HeliumN2N2 Hydrogen
Substrate      
Column diameter (mm) 0.320.250.25 0.25
Phase thickness (μm) 0.250.170.171.00.25
Tstart (C) 60.80.80.50.60.
Tend (C) 220.200.200.250.250.
Heat rate (K/min) 4.2.3.8.2.
Initial hold (min) 2.   5.
Final hold (min) 20.   2.
I 1344.1381.1376.1354.1344.
ReferenceThanh, Dung, et al., 1996Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993King and Knight, 1992Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1OV-101OV-101DB-1
Column length (m) 60.25.50.50.60.
Carrier gas   N2N2 
Substrate      
Column diameter (mm) 0.320.330.250.250.32
Phase thickness (μm)      
Tstart (C) 50.45.80.80.50.
Tend (C) 230.180.200.200.250.
Heat rate (K/min) 4.3.2.2.4.
Initial hold (min)  3.  0.1
Final hold (min) 10.   5.
I 1347.1346.1354.1359.1346.
ReferenceBinder, Turner, et al., 1990Wyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Binder and Flath, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase SE-30OV-101SE-30OV-3
Column length (m) 30.50.30.150.
Carrier gas     
Substrate     
Column diameter (mm)  0.30 0.66
Phase thickness (μm)     
Tstart (C) 50.40.50.20.
Tend (C) 240.230.240.170.
Heat rate (K/min) 4.3.54.1.
Initial hold (min) 2.5.2. 
Final hold (min) 10. 10. 
I 1344.1347.1344.1360.
ReferenceRamaswami, Briscese, et al., 1988Nykanen, 1986Ramaswami, Briscese, et al., 1986Buttery, Xu, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Gupta, Mallavarapu, et al., 2001
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Notes

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