Bicyclo[3.1.1]hept-2-ene, 2,6-dimethyl-6-(4-methyl-3-pentenyl)-


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase  HP-5 MSHP-5 MSHP-5 MSHP-5 MS
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Program not specifiednot specifiednot specifiednot specifiednot specified
I 1436.1433.1435.1438.1439.
ReferenceKarimi, Farmany, et al., 2011Payo, Colo, et al., 2011Payo, Colo, et al., 2011Payo, Colo, et al., 2011Payo, Colo, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-1 MSCBP-5HP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C 3 0C/min -> 150 0C (10 min) 10 0C/min -> 250 0C60C(2min) => 3C/min => 240C => 10C/min => 300C40C => 3C/min => 100C => 5C/min => 230C(2min)40C(10min) => 3C/min => 200C => 2C/min => 220C35C => 4C/min => 180C => 10C/min => 250C
I 1430.1411.1427.1435.1433.
ReferenceBajpai, Al-Reza, et al., 2009Cheriti, Saad, et al., 2007Chokeprasert P., Charles A.L., et al., 2007Cole, Haber, et al., 2007Santos, Nunes, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54SE-54SE-30SE-54DB-1
Column length (m) 25.25. 25.30.
Carrier gas HeliumHelium H2He
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.1
Program 110 0C 2 0C/min -> 160 0C 5 0C/min -> 290 0C (5 min)not specifiednot specified110C(2min) => 3C/min => 130C => 8.5C => 290C35C => 4C/min => 180C => 10C/min => 250C
I 1408.1436.1429.1436.1453.
ReferenceSouza, Souza, et al., 2006Souza, Souza, et al., 2006Vinogradov, 2004Lima, Veiga, et al., 2003Silva, Santos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5MSCBP-1CP Sil 5 CBMethyl Silicone
Column length (m) 25.30.25.25. 
Carrier gas  HeNitrogenN2 
Substrate      
Column diameter (mm) 0.20.250.25  
Phase thickness (μm) 0.110.250.25  
Program 60C (3min) => 2.5C/min => 190C (1min) => 70C/min => 240V (11min)40C (10min) => 3C/min => 120C => 10C/min => 250C (5min)not specifiednot specifiednot specified
I 1428.1440.1436.1434.1429.
ReferenceKovacevic and Kac, 2002Ansorena, Gimeno, et al., 2001Ly, Yamauchi, et al., 2001Weyerstahl, Marschall, et al., 1997Zenkevich, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Karimi, Farmany, et al., 2011
Karimi, H.; Farmany, A.; Noorizadeh, H., Prediction of linear retention index of Teucrium chamaedrys volatiles in GCxGC-TOF/MS by linear model, World Appl. Sci. J., 2011, 15, 8, 1086-1088. [all data]

Payo, Colo, et al., 2011
Payo, D.A.; Colo, J.; Calumpong, H.; de Clerck, O., Variability of non-polar secondary metabolites in the Red Alga Portieria, Mar Drugs, 2011, 9, 11, 2438-2468, https://doi.org/10.3390/md9112438 . [all data]

Bajpai, Al-Reza, et al., 2009
Bajpai, V.K.; Al-Reza, S.M.; Choi, U.L.; Lee, J.H.; Kang, S.C., Chemical composition, antibacterial and antioxidant activities of leaf essential oil and extracts of Metasequioa glyptostroboides Miki ex Hu, Food Chem. Toxicol., 2009, 47, 8, 1876-1883, https://doi.org/10.1016/j.fct.2009.04.043 . [all data]

Cheriti, Saad, et al., 2007
Cheriti, A.; Saad, A.; Belboukhari, N.; Ghezali, S., The essential oil composition of Bubonium graveolens (Forssk.) Maire from the algerian Sahara, Flavour Fragr. J., 2007, 22, 4, 286-288, https://doi.org/10.1002/ffj.1794 . [all data]

Chokeprasert P., Charles A.L., et al., 2007
Chokeprasert P.; Charles A.L.; Sue K.H.; Huang T.C., Volatile components of the leaves, fruits and seeds of wampee [Clausena lansium (Lour.) Skeels], J. Food Comp. Anal., 2007, 20, 1, 52-56, https://doi.org/10.1016/j.jfca.2006.07.002 . [all data]

Cole, Haber, et al., 2007
Cole, R.A.; Haber, W.A.; Setzer, W.N., Chemical composition of essential oils of seven species of Eugenia from Monteverde, Costa Rica, Biochem. Syst. Ecol., 2007, 35, 12, 877-886, https://doi.org/10.1016/j.bse.2007.06.013 . [all data]

Santos, Nunes, et al., 2006
Santos, R.P.; Nunes, E.P.; Nascimento, R.F.; Santiago, G.M.P.; Menezes, G.H.A.; Silveira, E.R.; Pessoa, O.D.L., Chemical Composition and Larvicidal Activity of the Essential Oils of Cordia leucomalloides and Cordia curassavica from the Northeast of Brazil, J. Braz. Chem. Soc., 2006, 17, 5, 1027-1030, https://doi.org/10.1590/S0103-50532006000500030 . [all data]

Souza, Souza, et al., 2006
Souza, M.A.A.; Souza, S.R.; Veiga, V.F., Jr.; Cortez, J.K.P.C.; Leal, R. de.S.; Dantas, T.N.C.; Maciel, M.A.M., Composicao quimica do oleo fixo de Croton cajucara e determinacao das suas propridades fungicidas, Braz. J. Pharmacognosy, 2006, 16, 599-610. [all data]

Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Lima, Veiga, et al., 2003
Lima, S.R.M.; Veiga, V.F., Jr.; Christo, H.B.; Pinto, A.C.; Fernandes, P.D., In vivo and in vitro studies on the anticancer activity of Copaifera multijuga Hayne and its fractions, Phytother. Res., 2003, 17, 9, 1048-1053, https://doi.org/10.1002/ptr.1295 . [all data]

Silva, Santos, et al., 2003
Silva, M.G.V.; Santos, R.N.D.; Matos, F.J.A.; Machado, M.I.L., Volatile constituents from leaf, inflorescence and root oils of Ocimum americanum L. grown in north-eastern Brazil, Flavour Fragr. J., 2003, 18, 4, 303-304, https://doi.org/10.1002/ffj.1217 . [all data]

Kovacevic and Kac, 2002
Kovacevic, N.; Kac, M., Analytical, nutritional, and clinical methods section. Determination and verification of hop varieties by analysis of essential oils, Food Chem., 2002, 77, 4, 489-494, https://doi.org/10.1016/S0308-8146(02)00114-0 . [all data]

Ansorena, Gimeno, et al., 2001
Ansorena, D.; Gimeno, O.; Astiasarán, I.; Bello, J., Analysis of volatile compounds by GC-MS of a dry fermented sausage: chorizo de Pamplona, Food Res. Int., 2001, 34, 1, 67-75, https://doi.org/10.1016/S0963-9969(00)00133-2 . [all data]

Ly, Yamauchi, et al., 2001
Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

Weyerstahl, Marschall, et al., 1997
Weyerstahl, P.; Marschall, H.; Seelmann, I.; Kaul, V.K., Constituents of the flower essential oil of Ageratina adenophora (Spreng.) K. et R. from India, Flavour Fragr. J., 1997, 12, 6, 387-396, https://doi.org/10.1002/(SICI)1099-1026(199711/12)12:6<387::AID-FFJ677>3.0.CO;2-F . [all data]

Zenkevich, 1996
Zenkevich, I.G., Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Mass Spectral Identification. Mono- and Sesquiterpenes, Rastitelnye Resursy (Plant resources), 1996, 34, 1-2, 48-58. [all data]


Notes

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