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B-Cortol TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-13085.Ludwig-Koehn and Henning, 198630. m/0.25 mm/0.25 «mu»m, H2, 2. K/min; Tstart: 120. C; Tend: 280. C
PackedOV-1013102.Hurter and van Ree, 1979Gas-Chrom P (80-100 mesh), 1. K/min; Column length: 3.6 m; Tstart: 180. C
PackedSE-303070.Hurter and van Ree, 1979Gas-Chrom P (80-100 mesh), 1. K/min; Column length: 3.6 m; Tstart: 180. C
PackedOV-13079.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C
CapillarySE-303097.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 200. C
PackedSE-303080.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ludwig-Koehn and Henning, 1986
Ludwig-Koehn, H.; Henning, H.V., Some aspects of quantification of neutral steroid metabolites in body fluids of healthy and uremic subjects by capillary gas chromatography, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 1, 35-38, https://doi.org/10.1002/jhrc.1240090106 . [all data]

Hurter and van Ree, 1979
Hurter, P.; van Ree, T., Programmed-Temperature Gas Chromatography on Mixed Phases. Separation of Steroid Derivatives on Binary Mixtures, J. Chromatogr., 1979, 169, 93-100, https://doi.org/10.1016/0021-9673(75)85034-5 . [all data]

Luyten and Rutten, 1974
Luyten, J.A.; Rutten, G.A.F.M., Analysis of Steroids by High-Resolution Gas-Liquid Chromatography. II. Application to Urinary Samples, J. Chromatogr., 1974, 91, 393-406, https://doi.org/10.1016/S0021-9673(01)97918-X . [all data]


Notes

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