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Phenanthrene, 7-ethenyl-1,2,3,4,4a,4b,5,6,7,8,10,10a-dodecahydro-1,1,4a,7-tetramethyl-, [4aS-(4a«alpha»,4b«beta»,7«beta»,10a«beta»)]-


Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
NIST MS number 13160

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Gas Chromatography

Go To: Top, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-101190.1994.Kosyukova and Khorguani, 1989Chromaton N-AW-DMCS; Column length: 2.5 m
CapillarySE-30170.1968.Perry and Weavers, 1984 
CapillarySE-30190.1994.Perry and Weavers, 1984 

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedCarbowax 20M170.2335.Kosyukova and Khorguani, 1989Chromaton N-AW-DMCS; Column length: 2.5 m
PackedCarbowax 20M190.2375.Kosyukova and Khorguani, 1989Chromaton N-AW-DMCS; Column length: 2.5 m
CapillaryCarbowax 20M170.2295.Perry and Weavers, 1984 
CapillaryCarbowax 20M190.2332.Perry and Weavers, 1984 

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-11999.Duquesnoy, Castola, et al., 200750. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillarySPB-11969.Cavaleiro, Salgueiro, et al., 200330. m/0.2 mm/0.2 «mu»m, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryCP Sil 5 CB2013.Pfeifhofer, 200050. m/0.22 mm/0.13 «mu»m, H2, 4. K/min, 300. C @ 10. min; Tstart: 40. C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-202319.Duquesnoy, Castola, et al., 200750. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-11969.Cavaleiro, Salgueiro, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP Innowax FSP2346.Kaya, Baser, et al., 199960. m/0.25 mm/0.25 «mu»m, He, 60. C @ 10. min, 220. C @ 10. min
CapillaryHP-Innowax2349.Kaya, Baser, et al., 1999, 260. m/0.25 mm/0.25 «mu»m, He, 60. C @ 10. min; Tend: 220. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-Innowax FSC2349.Demirci, Demirci, et al., 200560. m/0.25 mm/0.25 «mu»m, N2; Program: 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C

References

Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kosyukova and Khorguani, 1989
Kosyukova, L.V.; Khorguani, T.V., Retention indices of diterpenes isolated from resins of coniferous trees, Zh. Anal. Khim., 1989, 44, 9, 1309-1313. [all data]

Perry and Weavers, 1984
Perry, N.B.; Weavers, R.T., Kovats indices of diterpene hydrocarbons on fused-silica capillary columns, J. Chromatogr., 1984, 284, 478-481, https://doi.org/10.1016/S0021-9673(01)87850-X . [all data]

Duquesnoy, Castola, et al., 2007
Duquesnoy, E.; Castola, V.; Casanova, J., Composition and chemical variability of the twig oil of Abies alba Miller from Corsica, Flavour Fragr. J., 2007, 22, 4, 293-299, https://doi.org/10.1002/ffj.1796 . [all data]

Cavaleiro, Salgueiro, et al., 2003
Cavaleiro, C.; Salgueiro, L.R.; da Cunha, A.P.; Figueiredo, A.C.; Barroso, J.G.; Bighelli, A.; Casanova, J., Composition and variability of the essential oils of the leaves and berries from Juniperus navicularis, Biochem. Syst. Ecol., 2003, 31, 2, 193-201, https://doi.org/10.1016/S0305-1978(02)00080-7 . [all data]

Pfeifhofer, 2000
Pfeifhofer, H.W., Composition of the essential oil of Pinus canariensis Sweet ex Sprengel, Flavour Fragr. J., 2000, 15, 4, 266-270, https://doi.org/10.1002/1099-1026(200007/08)15:4<266::AID-FFJ908>3.0.CO;2-E . [all data]

Cavaleiro, Salgueiro, et al., 2002
Cavaleiro, C.; Salgueiro, L.; Barroso, J.G.; Figueiredo, A.C.; Pedro, L.G.; Fontinha, S.S.; Bighelli, A.; Casanova, J.; Looman, A.; Scheffer, J.J.C., Composition of the essential oil of Juniperus cedrus Webb and Berth. grown on Madeira, Flavour Fragr. J., 2002, 17, 2, 111-114, https://doi.org/10.1002/ffj.1061 . [all data]

Kaya, Baser, et al., 1999
Kaya, A.; Baser, K.H.C.; Koca, F., Essential oils of Acinos troodi (Post) Leblebici subsp. vardaranus Leblebici and subsp. grandiflorus Hartvig Strid, Flavour Fragr. J., 1999, 14, 1, 50-54, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<50::AID-FFJ783>3.0.CO;2-7 . [all data]

Kaya, Baser, et al., 1999, 2
Kaya, A.; Baser, K.H.C.; Tümen, G.; Koca, F., The essential oil of Acinos suaveolens (Sm.) G. Don fil. Acinos arvensis (Lam.) Dandy and Acinos rotundifolius Pers. growing wild in Turkey, Flavour Fragr. J., 1999, 14, 1, 60-64, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<60::AID-FFJ785>3.0.CO;2-0 . [all data]

Demirci, Demirci, et al., 2005
Demirci, B.; Demirci, F.; Dönmez, A.A.; Franz, G.; Paper, D.H.; Baser, K.H.C., Effects of Salvia essential oils on the chorioallantoic membrane (CAM) assay, Pharm. Biol., 2005, 43, 8, 666-671, https://doi.org/10.1080/13880200500383397 . [all data]


Notes

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