2-Cyclohexen-1-ol, 3-methyl-6-(1-methylethyl)-, cis-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1-MSHP-5MSRTX-1RTX-1HP-5 MS
Column length (m) 60.30.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 30.50.60.60.50.
Tend (C) 200.250.230.230.230.
Heat rate (K/min) 2.7.2.2.3.
Initial hold (min) 4.1.  10.
Final hold (min) 35.5.30.30.10.
I 1178.1203.1181.1181.1193.
ReferenceTakeoka, Hobbs, et al., 2010Zouari, Zouari, et al., 2010Museli, Pau, et al., 2009Museli, Pau, et al., 2009Adams, Beauchamp, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeliumHe 
Substrate      
Column diameter (mm) 0.260.250.260.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 240.240.290.210.220.
Heat rate (K/min) 3.5.3.30.4.
Initial hold (min)  1. 3.5.
Final hold (min)  4.  20.
I 1195.1193.1195.1194.1193.
ReferenceBos, Woerdenbag, et al., 2007Cheraif, Ben Jannet, et al., 2007Elfami, Bos, et al., 2007Ghasemi, Yamini, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSAT-5SPB-1HP-5DB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.250.200.320.26
Phase thickness (μm) 0.250.250.200.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 280.200.220.246.290.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)      
Final hold (min)  20.15.  
I 1167.1196.1177.1196.1195.
ReferenceTzakou, Bazos, et al., 2007Borges, Rojas, et al., 2006Cavaleiro, Pinto, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Elfami, Komar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-1DB-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas N2HydrogenHeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.70.60.60.60.
Tend (C) 300.280.250.240.230.
Heat rate (K/min) 4.4.5.3.3.
Initial hold (min)  4.   
Final hold (min)   10. 20.
I 1186.1193.1182.1194.1196.
ReferenceLis and Milczarek, 2006Pino, Marbot, et al., 2006Sonboli, Mirjalili, et al., 2006Khayyat and Karimi, 2005Skoula and Grayer, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5DB-5DB-5
Column length (m) 30.30.60.60.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.2
Phase thickness (μm) 0.250.25  0.25
Tstart (C) 60.90.50.50.50.
Tend (C) 280.220.220.200.220.
Heat rate (K/min) 3.7.3.3.3.
Initial hold (min)  2.  2.
Final hold (min)  5.   
I 1169.1189.1200.1215.1198.
ReferenceTzakou, Bazos, et al., 2005Agnihotri, Thappa, et al., 2004Edris and Farrag, 2003Edris, Shalaby, et al., 2003Masotti, Juteau, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1DB-5HP-1
Column length (m) 30.30.60.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.2490.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.70.
Tend (C) 280.280.280.300.220.
Heat rate (K/min) 4.3.4.3.3.
Initial hold (min) 10.    
Final hold (min) 40.  5.15.
I 1193.1178.1183.1193.1177.
ReferencePino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Shahmir, Ahmadi, et al., 2003Bos, Koulman, et al., 2002Cavaleiro, Salgueiro, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1DB-1DB-5SE-54
Column length (m) 30.30.25.30.30.
Carrier gas  N2HeHeHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 240.300.290.240.250.
Heat rate (K/min) 3.4.4.3.2.
Initial hold (min)     5.
Final hold (min)     2.
I 1199.1185.1193.1194.1200.
ReferenceNovak, Langbehn, et al., 2002Kalemba, 1999Koulman, 1999Maia, Zohhbi, et al., 1998Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase BP-1
Column length (m) 50.
Carrier gas H2
Substrate  
Column diameter (mm) 0.30
Phase thickness (μm)  
Tstart (C) 40.
Tend (C) 250.
Heat rate (K/min) 10.
Initial hold (min) 1.
Final hold (min)  
I 1195.
ReferenceBrophy, Davies, et al., 1989
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Lis and Milczarek, 2006
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References