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Flunitrazepam


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedCapillaryCapillaryPacked
Active phase SE-30BP-1DB-5SE-30
Column length (m) 2. 15.2.
Carrier gas Nitrogen HeHe
Substrate Chromosorb G AW DMCS (80-100 mesh)  Chromosorb W(100-120 mesh)
Column diameter (mm)   0.25 
Phase thickness (mum)   0.25 
Tstart (C) 100.100.150.200.
Tend (C) 300.300.260.285.
Heat rate (K/min)   10.4.
Initial hold (min)   1.2.
Final hold (min)    10.
I 2645.2633.2633.2607.
ReferenceMHA, 9999MHA, 9999Zamechnik, Ethier, et al., 1989Chiarotti, de Giovanni, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Zamechnik, Ethier, et al., 1989
Zamechnik, J.; Ethier, J.-C.; Neville, G.A., Benzodiazepines- an extensive collection of mass spectra, J. Can. Soc. Forensic Sci., 1989, 22, 3, 233-259, https://doi.org/10.1080/00085030.1989.10757437 . [all data]

Chiarotti, de Giovanni, et al., 1986
Chiarotti, M.; de Giovanni, N.; Fiori, A., Analysis of Benzodiazepines. I. Chromatographic Identification, J. Chromatogr., 1986, 358, 169-178, https://doi.org/10.1016/S0021-9673(01)90326-7 . [all data]


Notes

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