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cis-Muurola-4(15),5-diene


Gas Chromatography

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51461.Adams and Nguyen, 200530. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryHP-5MS1445.Gkinis, Tzakou, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillarySE-541461.Adams, 200030. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillarySE-541461.Adams, 2000, 230. m/0.26 mm/0.25 «mu»m, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51461.Adams, 2000, 330. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillarySE-301455.Kardali, Velasco-Negueruela, et al., 200025. m/0.22 mm/0.25 «mu»m, He, 5. K/min; Tstart: 70. C; Tend: 220. C
CapillaryDB-51461.Adams, 199930. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51462.Flamini, Cioni, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51463.Maccioni, Baldini, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51463.Flamini, Tebano, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-5MS1461.Silva-Brandão, Solferini, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillaryHP-51464.Flamini, Luigi Cioni, et al., 200530. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-5MS1478.Mumm, Tiemann, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 5. K/min; Tend: 300. C
CapillaryHP-5MS1448.Tzakou, Vagias, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1460.Demetzos, Angelopoulou, et al., 200230. m/0.25 mm/0.25 «mu»m, 50. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-51462.Flamini, Cioni, et al., 200230. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51460.Javidnia, Miri, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 60. C; Tend: 260. C
CapillaryHP-51432.Pitarokili, Couladis, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51459.Maia, de Paula, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryDB-51459.Maia, de Paula, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryDB-51460.Maia, de Paula, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 60. C @ 2. min, 3. K/min; Tend: 240. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-5MS1469.8Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryBPX-51478.Cardeal, da Silva, et al., 200630. m/0.25 mm/0.25 «mu»m; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51467.Bertoli, Lepnardi, et al., 201130. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5 MS1462.Ogunwande, Flamini, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-51472.Radulovic, Dordevic, et al., 201030. m/0.25 mm/0.25 «mu»m, Hydrogen, 5. K/min; Tstart: 70. C; Tend: 290. C
CapillaryDB-51484.Bos, Woerdenbag, et al., 200730. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51461.Cheraif, Ben Jannet, et al., 200730. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 1. min, 5. K/min, 240. C @ 4. min
CapillaryDB-51484.Elfami, Bos, et al., 200730. m/0.26 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryCol-Elite 5MS1473.Gudaityte and Venskutonis R.P., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 30. C; Tend: 246. C
CapillaryZB-51472.Mohottalage, Tabacchi, et al., 200730. m/0.25 mm/0.25 «mu»m, 60. C @ 5. min, 4. K/min, 220. C @ 20. min
CapillaryDB-11454.Pala-Paul, Brophy, et al., 200750. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryHP-5 MS1467.Vagionas, Graikou, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51484.Elfami, Komar, et al., 200630. m/0.26 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryDB-51469.Morteza-Semnani, Akbarzadeh, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 60. C; Tend: 220. C
CapillaryHP-51465.Pintore G., Chessa M., et al., 200630. m/0.25 mm/0.25 «mu»m, He, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51461.Pino, Marbot, et al., 200630. m/0.25 mm/0.25 «mu»m, Hydrogen, 70. C @ 4. min, 4. K/min; Tend: 280. C
CapillaryDB-51459.Pino, Marbot, et al., 200630. m/0.25 mm/0.25 «mu»m, Hydrogen, 70. C @ 4. min, 4. K/min; Tend: 280. C
CapillaryMethyl Silicone1480.Tonzibo, Coffy, et al., 200625. m/0.3 mm/0.15 «mu»m, N2, 50. C @ 5. min, 2. K/min; Tend: 210. C
CapillaryDB-51455.Chaverri and Cicció, 200530. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51462.Figuérédo, Cabassu, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 5. K/min, 300. C @ 5. min
CapillaryHP-5MS1477.Melkani, Dev, et al., 200530. m/0.25 mm/0.25 «mu»m, 50. C @ 10. min, 3. K/min, 250. C @ 5. min
CapillaryDB-51469.Morteza-Semnani and Saeedi, 200530. m/0.25 mm/0.25 «mu»m, He, 60. C @ 4. min, 4. K/min; Tend: 220. C
CapillaryDB-11454.Pala-Paul, Perez-Alonso, et al., 200550. m/0.25 mm/0.25 «mu»m, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryDB-11438.Velasco-Negueruela, Pérez-Alonso, et al., 200550. m/0.25 mm/0.25 «mu»m, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51450.Marongiu, Porcedda, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 280. C @ 30. min; Tstart: 60. C
CapillaryHP-51445.Pitarokili, Tzakou, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
Capillary5 % Phenyl methyl siloxane1467.Cicció and Gómez-Laurito, 200230. m/0.25 mm/0.25 «mu»m, He, 75. C @ 4. min, 3. K/min, 200. C @ 8. min
CapillaryDB-51466.Kabouss, Charrouf, et al., 200230. m/0.25 mm/0.25 «mu»m, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillaryDB-11438.Velasco-Negueruela, Pérez-Alonso, et al., 200250. m/0.25 mm/0.25 «mu»m, N2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-5MS1462.Zoghbi, Andrade, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 270. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCP Sil 8 CB1467.Kupcinskiene, Stikliene, et al., 200850. m/0.32 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryDB-5 MS1466.Silva, Doria, et al., 200830. m/0.25 mm/0.25 «mu»m; Program: 80 0C (1.5 min) 4 pC/min -> 180 0C 10 0C/min -> 300 0C (10 min)
CapillaryDB-5MS1470.Barra A., Coroneo V., et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 60C => 1C/min => 65C => 3C/min => 120C => 5C/min => 180C(5min) => 5C/min => 250C (20min)
CapillaryCP Sil 8 CB1467.Mockute, Bernotiene, et al., 200650. m/0.32 mm/0.25 «mu»m, He; Program: 60 0C (2 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C (5 min)
CapillaryCP Sil 8 CB1467.Butkienë, Nivinskienë, et al., 200550. m/0.32 mm/0.25 «mu»m, He; Program: 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
CapillaryCP Sil 8 CB1467.Butkienë, Nivinskienë, et al., 200450. m/0.32 mm/0.25 «mu»m, He; Program: 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
CapillaryOV-11448.El-Shazly and Hussein, 2004He; Column length: 15. m; Column diameter: 0.317 mm; Program: 50C(4min) => 4C/min => 90C => 10C/min => 300C(10min)
CapillaryCP-Sil 8CB-MS1460.Mockute, Bernotiene, et al., 2003Column length: 50. m; Column diameter: 0.32 mm; Program: 60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Adams and Nguyen, 2005
Adams, R.P.; Nguyen, S., Infra-specific variation in Juniperus deppeana and F. Sperryi in the Davis Mountains of Texas: variation in leaf essential oils and random amplified polymorphic DNAS (RAPDS), Phytologia, 2005, 87, 2, 96-108. [all data]

Gkinis, Tzakou, et al., 2003
Gkinis, G.; Tzakou, O.; Iliopoulou, D.; Roussis, V., Chemical Composition and Biological Activity of Nepeta parnassica Oils and Isolated Nepetalactones, Z. Naturforsch. C:, 2003, 58, 681-686. [all data]

Adams, 2000
Adams, R.P., Systematics of smooth leaf margin Juniperus of the western hemisphere based on leaf essential oils and RAPD DNA fingerprinting, Biochem. Syst. Ecol., 2000, 28, 2, 149-162, https://doi.org/10.1016/S0305-1978(99)00047-2 . [all data]

Adams, 2000, 2
Adams, R.P., Systematics of the one seeded Juniperus of the eastern hemisphere based on leaf essential oils and random amplified polymorphic DNAs (RAPDs), Biochem. Syst. Ecol., 2000, 28, 6, 529-543, https://doi.org/10.1016/S0305-1978(99)00096-4 . [all data]

Adams, 2000, 3
Adams, R.P., The serrate leaf margined Juniperus (Section Sabina) of the western hemisphere: systematics and evolution based on leaf essential oils and Random Amplified Polymorphic DNAs (RAPDs), Biochem. Syst. Ecol., 2000, 28, 10, 975-989, https://doi.org/10.1016/S0305-1978(00)00022-3 . [all data]

Kardali, Velasco-Negueruela, et al., 2000
Kardali, M.; Velasco-Negueruela, A.; Pérez-Alonso, M., Essential Oil Constituents of Sideritis ibanyezii Pau, Botanica Complutensis, 2000, 24, 101-106. [all data]

Adams, 1999
Adams, R.P., Systematics of multi-seeded eastern hemisphere Juniperus based on leaf essential oils and RAPD DNA fingerprinting, Biochem. Syst. Ecol., 1999, 27, 7, 709-725, https://doi.org/10.1016/S0305-1978(99)00016-2 . [all data]

Flamini, Cioni, et al., 2007
Flamini, G.; Cioni, P.L.; Morelli, I.; Bader, A., Essential oils of the aerial parts of three Salvia species from Jordan: Salvia lanigera, S. spinosa and S. syriaca, Food Chem., 2007, 100, 2, 732-735, https://doi.org/10.1016/j.foodchem.2005.10.032 . [all data]

Maccioni, Baldini, et al., 2007
Maccioni, S.; Baldini, R.; Luigi Cioni, P.; Tebano, M.; Flamini, G., In vivo volatiles emission and essential oils from different organs and pollen of Cistus albidus from Caprione (Eastern Liguria, Italy), Flavour Fragr. J., 2007, 22, 1, 61-65, https://doi.org/10.1002/ffj.1759 . [all data]

Flamini, Tebano, et al., 2006
Flamini, G.; Tebano, M.; Cioni, P.L.; Bagci, Y.; Dural, H.; Ertugrul, K.; Uysal, T.; Savran, A., A multivariate statistical approach to Centaurea classification using essential oil composition data of some species from Turkey, Pl. Syst. Evol., 2006, 261, 1-4, 217-228, https://doi.org/10.1007/s00606-006-0448-3 . [all data]

Silva-Brandão, Solferini, et al., 2006
Silva-Brandão, K.L.; Solferini, V.N.; Trigo, J.R., Chemical and phylogenetic relationships among Aristolochia L. (Aristolochiaceae) from southeastern Brazil, Biochem. Syst. Ecol., 2006, 34, 4, 291-302, https://doi.org/10.1016/j.bse.2005.10.011 . [all data]

Flamini, Luigi Cioni, et al., 2005
Flamini, G.; Luigi Cioni, P.; Morelli, I., Composition of the essential oils and in vivo emission of volatiles of four Lamium species from Italy: L. purpureum, L. hybridum, L. bifidum and L. amplexicaule, Food Chem., 2005, 91, 1, 63-68, https://doi.org/10.1016/j.foodchem.2004.05.047 . [all data]

Mumm, Tiemann, et al., 2004
Mumm, R.; Tiemann, T.; Schulz, S.; Hilker, M., Analysis of volatiles from black pine (Pinus nigra): significance of wounding and egg deposition by a herbivorous sawfly, Phytochemistry, 2004, 65, 24, 3221-3230, https://doi.org/10.1016/j.phytochem.2004.10.010 . [all data]

Tzakou, Vagias, et al., 2004
Tzakou, O.; Vagias, C.; Gani, A.; Yannitsaros, A., Volatile constituents of essential oils isolated at different growth stages from three Conyza species growing in Greece, Flavour Fragr. J., 2004, 19, 425-428. [all data]

Demetzos, Angelopoulou, et al., 2002
Demetzos, C.; Angelopoulou, D.; Perdetzoglou, D., A comparative study of the essential oils of Cistus salviifolius in several populations of Crete (Greece), Biochem. Syst. Ecol., 2002, 30, 7, 651-665, https://doi.org/10.1016/S0305-1978(01)00145-4 . [all data]

Flamini, Cioni, et al., 2002
Flamini, G.; Cioni, P.L.; Morelli, I., Differences in the fragrances of pollen and different floral parts of male and female flowers of Laurus nobilis, J. Agric. Food Chem., 2002, 50, 16, 4647-4652, https://doi.org/10.1021/jf020269x . [all data]

Javidnia, Miri, et al., 2002
Javidnia, K.; Miri, R.; Kamalinejad, M.; Nasiri, A., Composition of the essential oil of Salvia mirzayanii Rech. f. Esfand from Iran, Flavour Fragr. J., 2002, 17, 6, 465-467, https://doi.org/10.1002/ffj.1128 . [all data]

Pitarokili, Couladis, et al., 2002
Pitarokili, D.; Couladis, M.; Petsikos-Panayotarou, N.; Tzakou, O., Composition and antifungal activity on soil-borne pathogens of the essential oil of Salvia sclarea from Greece, J. Agric. Food Chem., 2002, 50, 23, 6688-6691, https://doi.org/10.1021/jf020422n . [all data]

Maia, de Paula, et al., 2000
Maia, B.H.L.N.S.; de Paula, J.R.; Sant'Ana, J.; da Silva, M.F.G.F.; Fernandes, J.B.; Vieira, P.C.; Costa, M.S.S.; Ohashi, O.S.; Silva, J.N.M., Essential oils of Toona and Cedrela species (Meliaceae): Taxonomic and ecological implications, J. Braz. Chem. Soc., 2000, 11, 6, 629-639, https://doi.org/10.1590/S0103-50532000000600012 . [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Cardeal, da Silva, et al., 2006
Cardeal, Z.L.; da Silva, M.D.R.G.; Marriott, P.J., Comprehensive two-dimensional gas chromatography/mass spectrometric analysis of pepper volatiles, Rapid Commun. Mass Spectrom., 2006, 20, 19, 2823-2836, https://doi.org/10.1002/rcm.2665 . [all data]

Bertoli, Lepnardi, et al., 2011
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Ogunwande, Flamini, et al., 2010
Ogunwande, I.A.; Flamini, G.; Cioni, P.L.; Omikorede, O.; Azeez, R.A.; Ayodele, A.A.; Kamil, Y.O., Aromatic plants growing in Nigeria: essential oil constituents of Cassia alata (Linn.) Roxb. and Helianthus annuus L., Rec. Nat. Prod., 2010, 4, 4, 211-217. [all data]

Radulovic, Dordevic, et al., 2010
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Bos, Woerdenbag, et al., 2007
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Elfami, Bos, et al., 2007
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Gudaityte and Venskutonis R.P., 2007
Gudaityte, O.; Venskutonis R.P., Chemotypes of Achillea millefolium transferred from 14 different locations in Lithuania to the controlled environment, Biochem. Syst. Ecol., 2007, 35, 9, 582-592, https://doi.org/10.1016/j.bse.2007.03.016 . [all data]

Mohottalage, Tabacchi, et al., 2007
Mohottalage, S.; Tabacchi, R.; Guerin, P.M., Components from Sri Lankan Piper betle L. leaf oil and their analogues showing toxicity against the housefly, Musca domestica, Flavour Fragr. J., 2007, 22, 2, 130-138, https://doi.org/10.1002/ffj.1770 . [all data]

Pala-Paul, Brophy, et al., 2007
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Vagionas, Graikou, et al., 2007
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Elfami, Komar, et al., 2006
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Morteza-Semnani, Akbarzadeh, et al., 2006
Morteza-Semnani, K.; Akbarzadeh, M.; Changizi, S., Essential oils composition of Stachys byzantina, S. inflata, S. lavandulifolia and S. laxa from Iran, Flavour Fragr. J., 2006, 21, 2, 300-303, https://doi.org/10.1002/ffj.1594 . [all data]

Pintore G., Chessa M., et al., 2006
Pintore G.; Chessa M.; Manconi P.; Zanetti S.; Deriu A.; Tirillini B., Chemical composition and antimicrobial activities of essential oil of stachys glutinosa L. from Sardinia, Natural Product Communications, 2006, 1, 12, 1133-1136. [all data]

Pino, Marbot, et al., 2006
Pino, J.A.; Marbot, R.; Payo, A.; Chao, D.; Herrera, P., Aromatic Plants from Western Cuba VII. Composition of the Leaf Oil of Psidium wrightii KRug et Urb., Lantana involucrata L., Cinnamonum montanum (Sw.) Berchtold et J. Persl. and Caesalpinia violacea (Mill.) Standley, J. Essent. Oil. Res., 2006, 18, 2, 170-174, https://doi.org/10.1080/10412905.2006.9699058 . [all data]

Tonzibo, Coffy, et al., 2006
Tonzibo, Z.F.; Coffy, A.A.; Chalachat, J.C.; N'guessan, Y.T., Chemical composition of essential oils of Hoslundia opposita Vahl. from Ivory Coast., Flavour Fragr. J., 2006, 21, 5, 789-791, https://doi.org/10.1002/ffj.1715 . [all data]

Chaverri and Cicció, 2005
Chaverri, C.; Cicció, J.F., Essential oil of trees of the genus Ocotea (Lauraceae) in Costa Rica. I. Ocotea brenesii, Rev. Biol. Trop., 2005, 53, 3-4, 431-436, https://doi.org/10.15517/rbt.v53i3-4.14611 . [all data]

Figuérédo, Cabassu, et al., 2005
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations- V. Chemical composition of essential oils of oregano: Origanum syriacum L. var. bevanii (Holmes) Ietswaart, O. syriacum L. var. sinaicum (Boiss.) Ietswaart, and O. syriacum L. var. syriacum from Lebanon and Israel, Flavour Fragr. J., 2005, 20, 164-168. [all data]

Melkani, Dev, et al., 2005
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Morteza-Semnani and Saeedi, 2005
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Notes

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