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13-Methylheptacosane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryOV-1255.2734.Hebanowska, Malinski, et al., 1989Ar; Column length: 30. m; Phase thickness: 0.1 «mu»m
CapillaryDexsil 300255.2728.Hebanowska, Malinski, et al., 1989Ar; Column length: 30. m; Phase thickness: 0.1 «mu»m

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS2731.Steinmetz, Schmolz, et al., 200330. m/0.32 mm/0.25 «mu»m, He, 3. K/min; Tstart: 150. C; Tend: 280. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS2723.3Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryMethyl Silicone2733.Kaib, Jmhasly, et al., 2004Program: 80C(1.5min) =.40C/min => 160C => 2.5C/min => 280C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-5 MS2736.Fox, Pianaro, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium, 12. K/min, 330. C @ 1. min; Tstart: 50. C
CapillaryDB-12735.Strohm, Herner, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium, 6. K/min, 300. C @ 20. min; Tstart: 100. C
CapillaryOV-12735.0Krkosova, Kubinec, et al., 2007100. m/0.32 mm/0.25 «mu»m, Helium, 5. K/min, 310. C @ 5. min; Tstart: 30. C
CapillaryUltra-12733.Nelson and Charlet, 2003He, 4. K/min; Column length: 12.5 m; Column diameter: 0.2 mm; Tstart: 150. C; Tend: 320. C
CapillaryDB-52731.Juárez, Blomquist, et al., 2001He, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 200. C; Tend: 280. C
CapillaryOV-12734.Szafranek, Malinski, et al., 1994Ar, 2. K/min; Column length: 40. m; Tstart: 200. C; Tend: 310. C
CapillaryBP-12733.Lockey and Oraha, 199012. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min; Tstart: 100. C; Tend: 300. C
CapillaryBP-12734.Lockey and Dularay, 198625. m/0.25 mm/0.25 «mu»m, Helium, 1.5 K/min; Tstart: 160. C; Tend: 300. C
CapillaryBP-12735.Lockey and Dularay, 198625. m/0.25 mm/0.25 «mu»m, Helium, 1.5 K/min; Tstart: 160. C; Tend: 300. C
CapillaryDexsil 3002731.Lockey, 19785. K/min; Column length: 15. m; Tstart: 50. C; Tend: 370. C
CapillaryDexsil 3002728.Lockey, 1978, 22. K/min; Column length: 15. m; Tstart: 240. C; Tend: 330. C
CapillaryDexsil 3002730.Lockey, 1978, 22. K/min; Column length: 15. m; Tstart: 240. C; Tend: 330. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryRTX-5 MS2733.Fox, Pianaro, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
Capillary 2734.Steiger, Peschke, et al., 2007Program: not specified
Capillary 2734.Lapointe, Hunter, et al., 2004Program: not specified
CapillaryDB-12735.Carlson, Geden, et al., 199930. m/0.32 mm/0.25 «mu»m, He; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C (12 - 42 min)
CapillaryCP Sil 5 CB2733.Kenig, Sinninghe Damsté, et al., 199525. m/0.32 mm/0.2 «mu»m, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min)
CapillaryApiezon2726.Petrov, 1984Program: not specified
CapillaryDexsil 3002743.Lockey, 1981Column length: 15. m; Program: 50 0C 5 0C/min -> 200 0C 2 0C/min -> 340 0C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Hebanowska, Malinski, et al., 1989
Hebanowska, E.; Malinski, E.; Dubis, E.; Pihlaja, K.; Oksman, P.; Winamaki, K.; Nawrot, J.; Szafranek, J., The composition of cuticular hydrocarbons of the Tribolium destructor, Comp. Biochem. Physiol. B: Comp. Biochem., 1989, 93, 2, 437-442. [all data]

Steinmetz, Schmolz, et al., 2003
Steinmetz, I.; Schmolz, E.; Ruther, J., Cuticular lipids as trail pheromone in a social wasp, Proc. R. Soc. London B:, 2003, 270, 1513, 385-391, https://doi.org/10.1098/rspb.2002.2256 . [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Kaib, Jmhasly, et al., 2004
Kaib, M.; Jmhasly, P.; Wilfert, L.; Durka, W.; Franke, S.; Francke, W.; Leuthold, R.H.; Brandl, R., Cuticular hydrocarbons and aggression in the termite Macrotermes Subhyalinus, J. Chem. Ecol., 2004, 30, 2, 365-385, https://doi.org/10.1023/B:JOEC.0000017983.89279.c5 . [all data]

Fox, Pianaro, et al., 2012
Fox, E.G.P.; Pianaro, A.; Solis, D.R.; Delabie, J.H.C.; Vairo, B.C.; Machado, E. deA.; Bueno, O.C., Intraspecific and intracolonial variations in the profile of vanom alkaloids and cuticular hydrocarbons of the fire ant Solenopsis saevissima Smith (Hymenoptera: Formicidae), Psyshe, 2012, 1-10. [all data]

Strohm, Herner, et al., 2008
Strohm, E.; Herner, G.; Kaltenpoth, M.; Boland, W.; Schreier, P.; Geiselhardt, S.; Peschke, K.; Schmitt, T., The chemistry of the postpharyngeal gland of female European beewolves, J. Chem. Ecol., 2008, 34, 5, 575-583, https://doi.org/10.1007/s10886-008-9447-x . [all data]

Krkosova, Kubinec, et al., 2007
Krkosova, Z.; Kubinec, R.; Addova, G.; Jurdakova, H.; Blasko, J.; Ostrovsky, I.; Sojak, L., Gas chromatographic - mass spectrometric characterization of monomethylalkanes from fuel diesel, Petroleum Coal, 2007, 49, 3, 51-62. [all data]

Nelson and Charlet, 2003
Nelson, D.R.; Charlet, L.D., Cuticular hydrocarbons of the sunflower beetle,Zygogramma exclamationis, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 135, 2, 273-284, https://doi.org/10.1016/S1096-4959(03)00080-0 . [all data]

Juárez, Blomquist, et al., 2001
Juárez, P.; Blomquist, G.J.; Schofield, C.J., Hydrocarbons of Rhodnius prolixus, a Chagas disease vector, Comp. Biochem. Physiol. B: Comp. Biochem., 2001, 129, 4, 733-746, https://doi.org/10.1016/S1096-4959(01)00380-3 . [all data]

Szafranek, Malinski, et al., 1994
Szafranek, J.; Malinski, E.; Dubis, E.; Hebanowska, E.; Nawrot, J.; Oksman, P.; Pihlaja, K., Identification of branched alkanes in lipids of Leptinotarsa decemlineata say and Tribolium destructor by GC-MS: a comparison of main-beam and link-scanned spectra, J. Chem. Ecol., 1994, 20, 9, 2197-2212, https://doi.org/10.1007/BF02033197 . [all data]

Lockey and Oraha, 1990
Lockey, K.H.; Oraha, V.S., Cuticular lipids of adult Locusta Migratoria Migratoriodes (R and F), Schstocerca Gregaria (Forskal) (Acrididae) and other orthopteran species - II. Hydrocarbons, Comp. Biochem. Physiol., 1990, 95B, 4, 721-744. [all data]

Lockey and Dularay, 1986
Lockey, K.H.; Dularay, B., Cuticular methylalkanes of adult cockroaches, Blatta orientalis and Periplaneta Americana, Comp. Biochem. Physiol., 1986, 85B, 3, 567-572. [all data]

Lockey, 1978
Lockey, K.H., The adult cuticular hydrocarbons of Tenebrio Molitor L. and Tenebrio Obscurus F. (Coleoptera: Tenebrionidae), Insect Biochem., 1978, 8, 4, 237-250, https://doi.org/10.1016/0020-1790(78)90032-X . [all data]

Lockey, 1978, 2
Lockey, K.H., Hydrocarbons of adult Tribolum castaneum Hbst. and Tribolium confusum duv. (Coleoptera: Tenebrionidae), Comparative Biochem. Physiol., 1978, 61B, 401-407. [all data]

Steiger, Peschke, et al., 2007
Steiger, S.; Peschke, K.; Francke, W.; Muller, J.K., The smell of parents: breeding status influences cuticular hydrocarbon pattern in the burying beetle Nicrophorus vespilloides, Proc. Roy. Soc. B, 2007, 274, 1622, 2211-2220, https://doi.org/10.1098/rspb.2007.0656 . [all data]

Lapointe, Hunter, et al., 2004
Lapointe, S.L.; Hunter, W.B.; Alessandro, R.T., Cuticular hydrocarbons on elytra of the Diaprepes root weevil Diaprepes abbreviatus (L.) (Coleoptera: Curculionidae), Agric. For. Entomol., 2004, 6, 4, 251-257, https://doi.org/10.1111/j.1461-9555.2004.00230.x . [all data]

Carlson, Geden, et al., 1999
Carlson, D.A.; Geden, C.J.; Bernier, U.R., Identification of pupal exiviae of Nasania vitripennis and Muscidifurax raptorellus parasitoids using cuticular hydrocarbons, Biol. Control, 1999, 15, 2, 97-106, https://doi.org/10.1006/bcon.1999.0708 . [all data]

Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W., Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates, Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5 . [all data]

Petrov, 1984
Petrov, A.A., Hydrocarbons of petroleum, Nauka (publishing house), Moscow, 1984, 263. [all data]

Lockey, 1981
Lockey, K.H., Cuticular hydrocarbons of adult Cylindrinotus laevioctostriatus (Goeze) and Phylan gibbus (Fabricius) (Coleoptera: Tenebrionidae), Insect. Biochem., 1981, 11, 5, 549-561, https://doi.org/10.1016/0020-1790(81)90023-8 . [all data]


Notes

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