2-Methylhexacosane

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryDB-1250.2664.Szafranek, Malinski, et al., 2001Ar; Column length: 30. m; Column diameter: 0.28 mm
CapillaryDexsil 300220.2660.Szafranek, Kusmierz, et al., 1982He; Column length: 30. m; Column diameter: 0.30 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
Capillary5 % Phenyl methyl siloxane2663.Zaikin, 201030. m/0.25 mm/0.25 μm, 15. K/min, 270. C @ 15. min; Tstart: 60. C
CapillaryUltra-12663.Nelson, Adams, et al., 2003150. C @ 4. min, 4. K/min, 320. C @ 30. min; Column length: 12. m; Column diameter: 0.2 mm
CapillaryDB-5MS2656.Steinmetz, Schmolz, et al., 200330. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 150. C; Tend: 280. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS2662.7Andriamaharavo, 201430. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-12663.Mutis, Parra, et al., 200930. m/0.22 mm/0.25 μm, Helium, 5. K/min, 290. C @ 15. min; Tstart: 40. C
CapillaryBP-12664.Mutis, Parra, et al., 200930. m/0.22 mm/0.25 μm, Helium, 5. K/min, 290. C @ 15. min; Tstart: 40. C
CapillaryOV-12665.3Krkosova, Kubinec, et al., 2007100. m/0.32 mm/0.25 μm, Helium, 5. K/min, 310. C @ 5. min; Tstart: 30. C
CapillaryUltra-12664.Nelson and Charlet, 2003He, 4. K/min; Column length: 12.5 m; Column diameter: 0.2 mm; Tstart: 150. C; Tend: 320. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Szafranek, Malinski, et al., 2001
Szafranek, B.; Malinski, E.; Nawrot, J.; Sosnowska, D.; Ruszkowska, M.; Pihlaja, K.; Trumpakaj, Z.; Szafranek, J., In Vitro effects of cuticular lipids of the aphids Sitobion avenae, Hyalopterus pruni and Brevicoryne brassicae on growth and sporulation of the Paecilomyces fumosoroseus and Beauveria bassiana, Arkivoc, 2001, 2001, 3, 81-94, https://doi.org/10.3998/ark.5550190.0002.311 . [all data]

Szafranek, Kusmierz, et al., 1982
Szafranek, J.; Kusmierz, J.; Czerwiec, W., Gas chromatographic-mass spectrometric investigations of high-boiling crude oil alkane fractions, J. Chromatogr., 1982, 245, 2, 219-228, https://doi.org/10.1016/S0021-9673(00)88591-X . [all data]

Zaikin, 2010
Zaikin, V.G., Personal communication: Retention indices measured during 2010, 2010. [all data]

Nelson, Adams, et al., 2003
Nelson, D.R.; Adams, T.S.; Fatland, C.L., Hydrocarbons in the surface wax of eggs and adults of the Colorado potato beetle, Leptinotarsa decemlineata, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 134, 3, 447-466, https://doi.org/10.1016/S1096-4959(02)00262-2 . [all data]

Steinmetz, Schmolz, et al., 2003
Steinmetz, I.; Schmolz, E.; Ruther, J., Cuticular lipids as trail pheromone in a social wasp, Proc. R. Soc. London B:, 2003, 270, 1513, 385-391, https://doi.org/10.1098/rspb.2002.2256 . [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Mutis, Parra, et al., 2009
Mutis, A.; Parra, L.; Palma, R.; Pardo, F.; Perich, F.; Quiroz, A., Evidence of contact pheromone use in mating behavior of the raspberry weevil (Coleoptera: Corculionidae), Environ. Entomol., 2009, 38, 1, 192-197, https://doi.org/10.1603/022.038.0124 . [all data]

Krkosova, Kubinec, et al., 2007
Krkosova, Z.; Kubinec, R.; Addova, G.; Jurdakova, H.; Blasko, J.; Ostrovsky, I.; Sojak, L., Gas chromatographic - mass spectrometric characterization of monomethylalkanes from fuel diesel, Petroleum Coal, 2007, 49, 3, 51-62. [all data]

Nelson and Charlet, 2003
Nelson, D.R.; Charlet, L.D., Cuticular hydrocarbons of the sunflower beetle,Zygogramma exclamationis, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 135, 2, 273-284, https://doi.org/10.1016/S1096-4959(03)00080-0 . [all data]


Notes

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