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Bicyclo[3.1.1]heptan-3-one, 2,6,6-trimethyl-, (1«alpha»,2«beta»,5«alpha»)-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSCP Sil 5 CBDB-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas He N2HeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.50.35.70.
Tend (C) 250.280.200.220.210.
Heat rate (K/min) 5.4.5.2.52.
Initial hold (min)      
Final hold (min)    6.60.
I 1157.1176.1160.1175.1173.
ReferenceSalehi, Fakhari, et al., 2007Ebrahim Sajjadi and Mehregan, 2006Agnaniet, Menut, et al., 2004Rohloff, Mordal, et al., 2004Mookdasanit, Tamura, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-1HP-5SPB-Sulfur
Column length (m) 30.30.50.30.30.
Carrier gas HeH2N2N2He
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum) 0.250.250.250.254.
Tstart (C) 60.40.60.60.45.
Tend (C) 280.245.240.220.240.
Heat rate (K/min) 3.3.3.5.5.
Initial hold (min)  20. 10.13.
Final hold (min)     5.
I 1162.1134.1148.1175.1171.
ReferencePitarokili, Tzakou, et al., 2003Gancel, Ollé, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Gallori, Flamini, et al., 2001Mariaca, Berger, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase RSL-150SE-30
Column length (m) 30.40.
Carrier gas  He
Substrate   
Column diameter (mm) 0.320.50
Phase thickness (mum) 0.200.75
Tstart (C) 30.30.
Tend (C) 200.220.
Heat rate (K/min) 3.3.
Initial hold (min)   
Final hold (min)   
I 1154.1149.
ReferenceRonse and De Pooter, 1990de Pooter, de Buyck, et al., 1989
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Salehi, Fakhari, et al., 2007
Salehi, P.; Fakhari, A.R.; Ebrahimi, S.N.; Heydari, R., Rapid essential oil screening of Rosmarinus officinalis L. by hydrodistillation-headspace solvent microextraction, Flavour Fragr. J., 2007, 22, 4, 280-285, https://doi.org/10.1002/ffj.1793 . [all data]

Ebrahim Sajjadi and Mehregan, 2006
Ebrahim Sajjadi, S.; Mehregan, I., Volatile constituents of flowers and leaves of Anthemis hyalina, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 531-533, https://doi.org/10.1007/s10600-006-0207-2 . [all data]

Agnaniet, Menut, et al., 2004
Agnaniet, H.; Menut, C.; Bessière, J.-M., Aromatic plants of tropical central Africa. Part XLIX: chemical composition of essential oils of the leaf and rhizome of Aframomum giganteum K. Schum from Gabon, Flavour Fragr. J., 2004, 19, 3, 205-209, https://doi.org/10.1002/ffj.1403 . [all data]

Rohloff, Mordal, et al., 2004
Rohloff, J.; Mordal, R.; Dragland, S., Chemotypical variation of tansy (Tanacetum vulgare L.) from 40 different locations in Norway, J. Agric. Food Chem., 2004, 52, 6, 1742-1748, https://doi.org/10.1021/jf0352430 . [all data]

Mookdasanit, Tamura, et al., 2003
Mookdasanit, J.; Tamura, H.; Yoshizawa T.; Tokunaga T.; Nakanishi, K., Trace Volatile Compounds in Essential Oil of Citrus Sudachi by Means of Modified Solvent Extraction Method, Food Sci Technol. Res., 2003, 9, 1, 54-61, https://doi.org/10.3136/fstr.9.54 . [all data]

Pitarokili, Tzakou, et al., 2003
Pitarokili, D.; Tzakou, O.; Loukis, A.; Harvala, C., Volatile metabolites from Salvia fruticosa as antifungal agents in soilborne pathogens, J. Agric. Food Chem., 2003, 51, 11, 3294-3301, https://doi.org/10.1021/jf0211534 . [all data]

Gancel, Ollé, et al., 2002
Gancel, A.-L.; Ollé, D.; Ollitrault, P.; Luro, F.; Brillouet, J.-M., Leaf and peel volatile compounds of an interspecific citrus somatic hybrid [Citrus aurantifolia (Christm.) Swing. + Citrus paradisi Macfayden], Flavour Fragr. J., 2002, 17, 6, 416-424, https://doi.org/10.1002/ffj.1119 . [all data]

Velasco-Negueruela, Pérez-Alonso, et al., 2002
Velasco-Negueruela, A.; Pérez-Alonso, M.J.; Palá-Paúl, J.; Íñigo, A.; López, G., Leaf essential oils analysis of Juniperus navicularis Gandoger, Botanica Complutensis, 2002, 26, 85-91. [all data]

Gallori, Flamini, et al., 2001
Gallori, S.; Flamini, G.; Bilia, A.R.; Morelli, I.; Landini, A.; Vincieri, F.F., Chemical composition of some traditional herbal drug preparations: essential oil and aromatic water of costmary (Balsamita suaveolens Pers.), J. Agric. Food Chem., 2001, 49, 12, 5907-5910, https://doi.org/10.1021/jf0107656 . [all data]

Mariaca, Berger, et al., 1997
Mariaca, R.G.; Berger, T.F.H.; Gauch, R.; Imhof, M.I.; Jeangros, B.; Bosset, J.O., Occurrence of volatile mono- and sesquiterpenoids in highland and lowland plant species as possible precursors for flavor compounds in milk and dairy products, J. Agric. Food Chem., 1997, 45, 11, 4423-4434, https://doi.org/10.1021/jf970216t . [all data]

Ronse and De Pooter, 1990
Ronse, A.C.; De Pooter, H.L., Essential Oil Production by Belgian Artemisia alba (Turra) before and after Micropropagation, J. Essent. Oil Res., 1990, 2, 5, 237-242, https://doi.org/10.1080/10412905.1990.9697873 . [all data]

de Pooter, de Buyck, et al., 1989
de Pooter, H.L.; de Buyck, L.F.; Schamp, N.M.; Billiet, F.; De Bruyn, A., The volatile fraction of Otacanthus coeruleus Lindl. Containing the new copaene derivative «beta»-copaen-4«alpha»-ol, Flavour Fragr. J., 1989, 4, 2, 47-51, https://doi.org/10.1002/ffj.2730040202 . [all data]


Notes

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