Phytol


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5SPB-1SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.50.30.50.
Tend (C) 250.260.300.250.250.
Heat rate (K/min) 3.4.50.4.5.
Initial hold (min) 1. 5.3.3.
Final hold (min) 3.5.5.10.15.
I 2112.2109.2111.2106.2105.
ReferenceJian-Yu, Zhu, et al., 2012Miyazawa, Marumoto, et al., 2011Bi Kouame, Bedi, et al., 2010Escalona-Arranz, Perez-Roses, et al., 2010Lazarevic, Palic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-5 MSDB-5OV-1
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.50.35.70.40.
Tend (C) 290.220.195.240.300.
Heat rate (K/min) 5.4.2.5.4.
Initial hold (min)  2.5. 2.
Final hold (min)  2.30. 10.
I 2117.2098.2108.2096.2100.
ReferenceRadulovic, Dordevic, et al., 2010Xu, Tang, et al., 2010Kim and Chung, 2009Lawal and Oyedelji, 2009Nibret and Wink, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-5HP-5HP-5HP-1
Column length (m) 25.30.30.30.30.
Carrier gas HeliumNitrogenNitrogenHeHe
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 70.50.50.70.60.
Tend (C) 200.280.280.240.240.
Heat rate (K/min) 3.5.5.5.2.
Initial hold (min) 2.1.1.  
Final hold (min)  1.1. 20.
I 2142.2127.2135.2103.2091.
ReferenceBlazevic and Mastelic, 2008Bousaada, Ammar, et al., 2008Saidana, Mahjoub, et al., 2008Asekun, Olusegun, et al., 2007Hachicha, Skanji, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5Elite-5MSCP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeHeliumHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.5 
Tstart (C) 60.40.60.40.50.
Tend (C) 240.260.320.280.230.
Heat rate (K/min) 2.4.10.4.3.
Initial hold (min)    5. 
Final hold (min)   4.10. 
I 2107.2107.2111.2121.2090.
ReferenceMiyazawa and Tamura, 2007Ristic, Krivokuca-Dokic, et al., 2007Smelcerovic, Spiteller, et al., 2007Tava, Pecetti, et al., 2007Kasali, Ekundayo, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101DB-1PE-5Methyl SiliconeHP-5MS
Column length (m) 25.50.50.25.30.
Carrier gas HeN2HeN2He
Substrate      
Column diameter (mm) 0.20.250.320.30.25
Phase thickness (μm) 0.20.250.250.150.25
Tstart (C) 70.95.100.50.60.
Tend (C) 200.240.280.210.280.
Heat rate (K/min) 3.4.3.2.3.
Initial hold (min) 2. 1.5. 
Final hold (min) 15.    
I 2102.2106.2123.2135.2106.
ReferenceMastelic, Jerkovic, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pandey-Rai S., Mallavarapu G.R., et al., 2006Tonzibo, Coffy, et al., 2006Tzakou, Said, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5SPB-1DB-5HP-5
Column length (m) 30.30.50.25.30.
Carrier gas HeliumHeHeNitrogenHe
Substrate      
Column diameter (mm) 0.250.250.20.250.32
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 35.60.50.60.100.
Tend (C) 280.240.220.240.240.
Heat rate (K/min) 4.3.4.3.5.
Initial hold (min) 2. 3. 2.
Final hold (min)   30. 5.
I 2116.2106.2120.2116.2114.
ReferenceKowalski, 2005Miyazawa, Nishiguchi, et al., 2005Wong and Tan, 2005JAvidnia, Mojab, et al., 2004Chaves, Lago, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1DB-5DB-5DB-5
Column length (m) 25.25.30.30.30.
Carrier gas HeliumN2HeHeHe
Substrate      
Column diameter (mm) 0.320.500.250.250.25
Phase thickness (μm) 0.530.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 280.220.240.240.240.
Heat rate (K/min) 4.5.3.3.3.
Initial hold (min)      
Final hold (min)  10.   
I 2108.2086.2111.2112.2114.
ReferenceVelickovic, Ristic, et al., 2003Das, Ram, et al., 2002Kobaisy, Tellez, et al., 2002Tellez, Khan, et al., 2002Tellez M., Estell R., et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-1OV-101OV-101OV-101
Column length (m) 30.25.50.50.50.
Carrier gas N2H2N2N2Nitrogen
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.17   
Tstart (C) 60.40.80.80.70.
Tend (C) 300.260.200.200.200.
Heat rate (K/min) 4.3.2.2.2.
Initial hold (min)  5.   
Final hold (min)      
I 2110.2091.2105.2106.2097.
ReferenceKalemba, 1999Lopes, Koketsu, et al., 1999Tamura, Nakamoto, et al., 1995Tamura, Nakamoto, et al., 1995Sugisawa, Nakamura, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-101SE-54
Column length (m) 50.25.
Carrier gas NitrogenN2
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (μm)   
Tstart (C) 80.60.
Tend (C) 200.260.
Heat rate (K/min) 2.6.
Initial hold (min)  2.
Final hold (min)   
I 2105.2110.
ReferenceSugisawa, Nakamura, et al., 1990Bestmann, Classen, et al., 1988
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jian-Yu, Zhu, et al., 2012
Jian-Yu, S.; Zhu, L.; Tian, Y.-J., Chemical composition and antimicrobial activities of essential oil of Matricaria songarica, Int. J. Agriculture Biology, 2012, 14, 1, 107-110. [all data]

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Escalona-Arranz, Perez-Roses, et al., 2010
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Radulovic, N.S.; Dordevic, N.D.; Palic, R.M., Volatiles of Pleurospermum austriacum (L.) Hoffm. (Apiaceae), J. Serbian Chem. Soc., 2010, 75, 12, 1-11, https://doi.org/10.2298/JSC100323127R . [all data]

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Kim and Chung, 2009
Kim, J.-S.; Chung, H.Y., GC-MS analysis of the volatile components in dried boxthorn (Lycium chimensis) Fruit, J. Korean Soc. Appl. Biol. Chem., 2009, 52, 5, 516-524, https://doi.org/10.3839/jksabc.2009.088 . [all data]

Lawal and Oyedelji, 2009
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Nibret and Wink, 2009
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Blazevic and Mastelic, 2008
Blazevic, I.; Mastelic, J., Free and bounded volatiles of rocket (Eruca sativa Mill.), Fravour Fragr. J., 2008, 23, 4, 278-285, https://doi.org/10.1002/ffj.1883 . [all data]

Bousaada, Ammar, et al., 2008
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Saidana, Mahjoub, et al., 2008
Saidana, D.; Mahjoub, M.A.; Boussaada, O.; Chriaa, J.; Cheraif, I.; Daami, M.; Mighri, Z.; Helal, A.N., Chemical composition and antimicrobial activity of volatile compounds of Tamarix boveana (Tamaricaceae), Microbiol. Res., 2008, 163, 4, 445-455, https://doi.org/10.1016/j.micres.2006.07.009 . [all data]

Asekun, Olusegun, et al., 2007
Asekun, O.T.; Olusegun, E.; Adebola, O., The volatile constituents of the leaves and flowers of Kigelia africana Benth., Flavour Fragr. J., 2007, 22, 1, 21-23, https://doi.org/10.1002/ffj.1723 . [all data]

Hachicha, Skanji, et al., 2007
Hachicha, S.F.; Skanji, T.; Barrek, S.; Ghrabi, Z.G.; Zarrouk, H., Composition of the essential oil of Teucrium ramosissimum Desf. (Lamiaceae) from Tunisia, Flavour Fragr. J., 2007, 22, 2, 101-104, https://doi.org/10.1002/ffj.1764 . [all data]

Miyazawa and Tamura, 2007
Miyazawa, M.; Tamura, N., Components of the essential oil from sprouts of Polygonum hydropiper L. ('Benitade'), Flavour Fragr. J., 2007, 22, 3, 188-190, https://doi.org/10.1002/ffj.1779 . [all data]

Ristic, Krivokuca-Dokic, et al., 2007
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Smelcerovic, Spiteller, et al., 2007
Smelcerovic, A.; Spiteller, M.; Ligon, A.P.; Smelcerovic, Z.; Raabe, N., Essential oil composition of Hypericum L. species from Southeastern Serbia and their chemotaxonomy, Biochem. Syst. Ecol., 2007, 35, 2, 99-113, https://doi.org/10.1016/j.bse.2006.09.012 . [all data]

Tava, Pecetti, et al., 2007
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Kasali, Ekundayo, et al., 2006
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Mastelic, Jerkovic, et al., 2006
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JAvidnia, Mojab, et al., 2004
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Chaves, Lago, et al., 2003
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Velickovic, Ristic, et al., 2003
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Das, Ram, et al., 2002
Das, M.; Ram, G.; Singh, A.; Mallavarapu, G.R.; Ramesh, S.; Ram, M.; Kumar, S., Volatile constituents of different plant parts of Chamomilla recutita L. Rausch grown in the Indo-Gangetic plains, Flavour Fragr. J., 2002, 17, 1, 9-12, https://doi.org/10.1002/ffj.1035 . [all data]

Kobaisy, Tellez, et al., 2002
Kobaisy, M.; Tellez, M.R.; Dayan, F.E.; Duke, S.O., Phytotoxicity and volatile constituents from leaves of Callicarpa japonica Thunb., Phytochemistry, 2002, 61, 1, 37-40, https://doi.org/10.1016/S0031-9422(02)00207-8 . [all data]

Tellez, Khan, et al., 2002
Tellez, M.R.; Khan, I.A.; Kobaisy, M.; Schrader, K.K.; Dayan, F.E.; Osbrink, W., Composition of the essential oil of Lepidium meyenii (Walp.), Phytochemistry, 2002, 61, 2, 149-155, https://doi.org/10.1016/S0031-9422(02)00208-X . [all data]

Tellez M., Estell R., et al., 2001
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Kalemba, 1999
Kalemba, D., Constituents of the essential oil of Artemisia asiatica Nakai, Flavour Fragr. J., 1999, 14, 3, 173-176, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<173::AID-FFJ805>3.0.CO;2-Q . [all data]

Lopes, Koketsu, et al., 1999
Lopes, D.; Koketsu, M.; Carauta, J.P.P.; de Oliveira, R.R.; Kaplan, M.A.C., Chemical composition of Pourouma guianensis Aublet essential oils, Flavour Fragr. J., 1999, 14, 4, 233-236, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<233::AID-FFJ813>3.0.CO;2-L . [all data]

Tamura, Nakamoto, et al., 1995
Tamura, H.; Nakamoto, H.; Yang, R.-H.; Sugisawa, H., Characteristic aroma compounds in green algae (Ulva pertusa) volatiles, Nippon Shokuhin Kagaku Kogaku Kaishi, 1995, 42, 11, 887-891, https://doi.org/10.3136/nskkk.42.887 . [all data]

Sugisawa, Nakamura, et al., 1990
Sugisawa, H.; Nakamura, K.; Tamura, H., The aroma profile of the volatile in marine green algae (Ulva pertusa), Food Reviews International, 1990, 6, 4, 573-589, https://doi.org/10.1080/87559129009540893 . [all data]

Bestmann, Classen, et al., 1988
Bestmann, H.-J.; Classen, B.; Kobold, U.; Vostrowsky, O.; Klingauf, F.; Stein, U., Steam volatile constituents from leaves of Rhus typhina, Phytochemistry, 1988, 27, 1, 85-90, https://doi.org/10.1016/0031-9422(88)80595-8 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References