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6-Octen-1-ol, 3,7-dimethyl-, acetate


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1BP-1HP-5DB-5
Column length (m) 30.50.50.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.50.60.
Tend (C) 250.220.220.220.246.
Heat rate (K/min) 5.2.2.5.3.
Initial hold (min) 1.  10. 
Final hold (min) 10.20.20.  
I 1353.1331.1331.1356.1351.
ReferenceBenzo, Gilardoni, et al., 2007Boti, Koukoua, et al., 2007Duquesnoy, Castola, et al., 2007Flamini, Tebano, et al., 2007Hongratanaworakit and Buchbauer, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5HP-5MSDB-5
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 55.60.60.60.50.
Tend (C) 240.220.250.300.250.
Heat rate (K/min) 3.2.3.3.5.
Initial hold (min) 2.   2.
Final hold (min) 15.20.   
I 1353.1334.1354.1355.1353.
ReferenceSilva, Barbosa, et al., 2007Gonny, Cavaleiro, et al., 2006Javidnia, Miri, et al., 2006Silva-Brandão, Solferini, et al., 2006Su, Ho, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1MDN-5DB-1
Column length (m) 60.30.30.30.30.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.50.50.50.40.
Tend (C) 230.260.260.250.250.
Heat rate (K/min) 2.2.2.3.3.
Initial hold (min) 2.3.3.  
Final hold (min) 20.5.5. 20.
I 1357.1332.1354.1347.1336.
ReferenceChoi, 2005Dob, Berramdane, et al., 2005Dob, Berramdane, et al., 2005, 2Dugo, Mondello, et al., 2005Fanciullino, Gancel, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSHP-5MSMega 5MSHP-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.40.60.
Tend (C) 250.250.200.240.220.
Heat rate (K/min) 3.4.2.3.5.
Initial hold (min)  2. 2.10.
Final hold (min) 20.20.10.  
I 1333.1354.1351.1349.1335.
ReferenceGancel, Ollitrault, et al., 2005Pino, Mesa, et al., 2005Smadja, Rondeau, et al., 2005Verzera, Trozzi, et al., 2005Bertoli, Pistelli, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-1DB-5MSBP-1SPB-1
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.320.250.320.2
Phase thickness (mum) 0.250.170.250.250.2
Tstart (C) 45.50.40.60.70.
Tend (C) 300.200.280.220.220.
Heat rate (K/min) 3.3.4.5.3.
Initial hold (min) 6. 2.  
Final hold (min) 10.  13.15.
I 1353.1314.1357.1326.1331.
ReferenceDugo, Mondello, et al., 2004Fernández-Ocaña, Gómez-Rodríguez, et al., 2004Mardarowicz, Wianowska, et al., 2004Raina, Kumar, et al., 2004Cavaleiro, Salgueiro, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5DB-1DB-5HP-5
Column length (m) 25.30.30.30.30.
Carrier gas  N2He He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.50.25
Tstart (C) 35.70.40.40.40.
Tend (C) 225.230.250.265.240.
Heat rate (K/min) 4.2.3.7.3.
Initial hold (min) 10.2.   
Final hold (min)  20.20.5. 
I 1340.1357.1333.1348.1355.
ReferenceChisholm, Wilson, et al., 2003Choi, 2003Gancel, Ollitrault, et al., 2003Högnadóttir and Rouseff, 2003Shellie and Marriott, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Mega 5MSBP-1RTX-5HP-1SPB-1
Column length (m) 30.50.30.24.15.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.220.250.320.25
Phase thickness (mum) 0.250.250.250.170.25
Tstart (C) 40.60.45.60.35.
Tend (C) 240.220.300.250.225.
Heat rate (K/min) 3.2.3.4.6.
Initial hold (min) 2. 6.2.3.
Final hold (min)  20.10.20.10.
I 1349.1332.1355.1335.1338.
ReferenceVerzera, Trozzi, et al., 2003Lota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002Chisholm, Wilson, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5DB-5Mega 5MSMega 5MS
Column length (m) 50.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.200.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.40.
Tend (C) 220.180.290.240.240.
Heat rate (K/min) 2.4.4.3.3.
Initial hold (min)  8.2.2.2.
Final hold (min)  2.5.  
I 1332.1352.1336.1349.1349.
ReferenceLota, Serra, et al., 2001Alonzo, Bosco, et al., 2000Bartley and Jacobs, 2000Verzera, la Rosa, et al., 2000Verzera, Trozzi, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1Methyl SiliconeCP Sil 5 CBDB-1
Column length (m) 50.50.50.25.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.250.250.17 0.25
Tstart (C) 60.60.80.60.50.
Tend (C) 230.230.200.260.250.
Heat rate (K/min) 2.2.2.5.3.5
Initial hold (min)     5.
Final hold (min) 35.35.   
I 1332.1332.1338.1335.1343.
ReferenceLota, Serra, et al., 1999Lota, Serra, et al., 1999Sumathykutty, Rao, et al., 1999Weyerstahl, Marschall, et al., 1999Stashenko, Prada, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-101OV-101DB-5DB-1
Column length (m) 25.50.50.60.30.
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.20.250.250.320.25
Phase thickness (mum) 0.3  1. 
Tstart (C) 40.80.80.40.50.
Tend (C) 200.200.200.220.300.
Heat rate (K/min) 2.2.2.3.2.
Initial hold (min)      
Final hold (min)      
I 1338.1333.1336.1348.1332.1
ReferencePíry, Príbela, et al., 1995Yang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Le Quere and Latrasse, 1990Chang, Sheng, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1OV-1OV-1
Column length (m) 30.30.30.30.30.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.250.250.250.50.5
Phase thickness (mum)    0.80.8
Tstart (C) 50.50.50.40.40.
Tend (C) 300.300.300.220.220.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1333.41332.11333.71334.1336.
ReferenceChang, Sheng, et al., 1989Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989De Pooter, Omar, et al., 1985De Pooter, Omar, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Benzo, Gilardoni, et al., 2007
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Choi, H.-S., Character impact odorants of Citrus Hallabong [(C. unshiu Marcov × C. sinensis Osbeck) × C. reticulata Blanco] cold-pressed peel oil, J. Agric. Food Chem., 2003, 51, 9, 2687-2692, https://doi.org/10.1021/jf021069o . [all data]

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Lota, de Rocca Serra, et al., 2002
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Nath, Sarma, et al., 2002
Nath, S.C.; Sarma, K.K.; Vajezikova, I.; Leclercq, P.A., Comparison of volatile inflorescence oils and taxonomy of certain Cymbopogon taxa described as Cymbopogon flexuosus (Nees ex Steud.) Wats., Biochem. Syst. Ecol., 2002, 30, 2, 151-162, https://doi.org/10.1016/S0305-1978(01)00066-7 . [all data]

Chisholm, Wilson, et al., 2001
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Lota, Serra, et al., 2001
Lota, M.-L.; Serra, D.R.; Jacquemond, C.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of sour orange, Flavour Fragr. J., 2001, 16, 2, 89-96, https://doi.org/10.1002/1099-1026(200103/04)16:2<89::AID-FFJ950>3.0.CO;2-D . [all data]

Alonzo, Bosco, et al., 2000
Alonzo, G.; Bosco, S.F.D.; Palazzolo, E.; Saiano, F.; Tusa, N., Citrus somatic hybrid leaf essential oil, Flavour Fragr. J., 2000, 15, 4, 258-262, https://doi.org/10.1002/1099-1026(200007/08)15:4<258::AID-FFJ906>3.0.CO;2-F . [all data]

Bartley and Jacobs, 2000
Bartley, J.P.; Jacobs, A.L., Effects of drying on flavour compounds in Australian-grown ginger (Zingiber officinale), J. Sci. Food Agric., 2000, 80, 2, 209-215, https://doi.org/10.1002/(SICI)1097-0010(20000115)80:2<209::AID-JSFA516>3.0.CO;2-8 . [all data]

Verzera, la Rosa, et al., 2000
Verzera, A.; la Rosa, G.; Zappalà, M.; Cotroneo, A., Essential oil composition of different cultivars of bergamot grown in Sicily, Ital. J. Food Sci., 2000, 12, 4, 493-501. [all data]

Verzera, Trozzi, et al., 2000
Verzera, A.; Trozzi, A.; Cotroneo, A.; Lorenzo, D.; Dellacassa, E., Uruguayan essential oil. 12. Composition of Nova and Satsuma mandarin oils, J. Agric. Food Chem., 2000, 48, 7, 2903-2909, https://doi.org/10.1021/jf990734z . [all data]

Lota, Serra, et al., 1999
Lota, M.-L.; Serra, D.R.; Tomi, F.; Bessiere, J.-M.; Casanova, J., Chemical composition of peel and leaf essential oils of Citrus medica L. and C. limonimedica Lush., Flavour Fragr. J., 1999, 14, 3, 161-166, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<161::AID-FFJ801>3.0.CO;2-8 . [all data]

Sumathykutty, Rao, et al., 1999
Sumathykutty, M.A.; Rao, J.M.; Padmakumari, K.P.; Narayanan, C.S., Essential oil constituents of some Piper species, Flavour Fragr. J., 1999, 14, 5, 279-282, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<279::AID-FFJ821>3.0.CO;2-0 . [all data]

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Notes

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