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6-Octen-1-ol, 3,7-dimethyl-, acetate


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSSE-30 MSDB-5 MSDB-1 MSHP-5
Column length (m) 30.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.250.32
Tstart (C) 60.50.40.40.60.
Tend (C) 240.250.250.250.250.
Heat rate (K/min) 3.5.5.6.5.
Initial hold (min)  5.15.1.30.
Final hold (min)  10.15.4. 
I 1360.1360.1343.1333.1355.
ReferencePinheiro, de Queiros, et al., 2013Menichini, Tundis, et al., 2011Mesa-Arango, Betancur-Galvis, et al., 2010Seo, Kim, et al., 2009Yassa and Akhani, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5HP-5MSHP-5MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.35.60.60.60.
Tend (C) 300.220.250.250.220.
Heat rate (K/min) 4.3.2.2.6.
Initial hold (min)   8.8. 
Final hold (min)  40.15.15. 
I 1335.1342.1361.1349.1326.
ReferenceBaran, von Reuss, et al., 2007El-Ghorab A., El-Massry K.F., et al., 2007Ferhat, Meklati, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Loghmani-Khouzani, Fini, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1Elite-5MSHP-5BP-1
Column length (m) 30.60.30.30.50.
Carrier gas HeliumNitrogenHeHe 
Substrate      
Column diameter (mm) 0.250.250.320.250.22
Phase thickness (mum) 0.250.250.50.320.25
Tstart (C) 60.60.40.60.60.
Tend (C) 220.250.280.250.220.
Heat rate (K/min) 6.5.4.5.2.
Initial hold (min)   5.30. 
Final hold (min)  10.10. 20.
I 1354.1332.1355.1355.1333.
ReferenceLoghmani-Khouzani, Fini, et al., 2007Sonboli, Kanani, et al., 2007Tava, Pecetti, et al., 2007Yassa and Akhani, 2007Boti, Yao, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FSOT-RSL-200CP Sil 5 CBBPX-5Methyl SiliconeHP-5
Column length (m) 30.30.50.60.25.
Carrier gas HydrogenN2 HeHe
Substrate      
Column diameter (mm) 0.320.320.220.30.2
Phase thickness (mum) 0.250.251. 0.33
Tstart (C) 40.50.70.50.60.
Tend (C) 280.300.280.240.240.
Heat rate (K/min) 6.4.4.3.3.
Initial hold (min) 5.    
Final hold (min) 5. 4. 7.
I 1363.1338.1358.1347.1352.
ReferenceJirovetz, Eller, et al., 2006Lis and Milczarek, 2006Wohlmuth, Smith, et al., 2006Chalchat and Özcan, 2005Duarte, Figueira, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-1DB-5HP-5MS
Column length (m) 25.30.60.30.30.
Carrier gas He N2N2He
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 50.60.70.40.60.
Tend (C) 250.280.230.230.275.
Heat rate (K/min) 3.3.2.2.4.
Initial hold (min) 3. 2.  
Final hold (min) 10. 20.  
I 1357.1353.1343.1314.1353.
ReferenceGhasemi Y., Faridi P., et al., 2005Petrakis, Roussis, et al., 2005Choi, 2004González, Guerra, et al., 2004Hajhashemi V., Ghannadi A., et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1NB-30DB-1DB-1HP-5MS
Column length (m) 30.50.60.60.30.
Carrier gas N2He NitrogenHe
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.70.70.60.
Tend (C) 300.250.230.230.275.
Heat rate (K/min) 4.2.2.2.4.
Initial hold (min)   2.2. 
Final hold (min)   20.  
I 1334.1344.1342.1342.1350.
ReferenceLis, Boczek, et al., 2004Raal, Arak, et al., 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Ghannadi, Aghazari, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1BPX-5DB-1OV-101
Column length (m) 30.60. 30.50.
Carrier gas HeliumN2 H2He
Substrate      
Column diameter (mm) 0.320.25 0.320.2
Phase thickness (mum)  0.25 0.250.5
Tstart (C) 70.70.40.40.50.
Tend (C) 210.230.260.245.250.
Heat rate (K/min) 2.2.5.3.2.
Initial hold (min)  2. 20. 
Final hold (min) 60.20.   
I 1354.1342.1368.1330.1334.
ReferenceMookdasanit, Tamura, et al., 2003Tu, Onishi, et al., 2003Diaz and Kite, 2002Gancel, Ollé, et al., 2002Orav, Kailas, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1CBP-1DB-5OV-101
Column length (m) 30.50.25.60.50.
Carrier gas N2HeNitrogenHeN2
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.25  
Tstart (C) 60.60.50.50.80.
Tend (C) 220.230.210.250.200.
Heat rate (K/min) 5.2.3.3.2.
Initial hold (min)   2.5. 
Final hold (min)  35.   
I 1334.1332.1341.1355.1333.
ReferenceGupta, Mallavarapu, et al., 2001Lota, de Rocca Serra, et al., 2001Ly, Yamauchi, et al., 2001Rousis, Papadogianni, et al., 2001Yang, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200SPB-5DB-5OV-101SPB-1
Column length (m) 60.60.30.50.50.
Carrier gas H2HeN2Nitrogen 
Substrate      
Column diameter (mm) 0.320.250.220.250.2
Phase thickness (mum) 0.250.250.25 0.33
Tstart (C) 40.70.70.40.60.
Tend (C) 250.240.230.200.260.
Heat rate (K/min) 6.5.4.2.4.
Initial hold (min)  8.2.10. 
Final hold (min)  20.20.  
I 1334.1353.1351.1334.1333.
ReferenceJirovetz, Puschmann, et al., 2000Kim, Kim, et al., 2000Mitiku, Sawamura, et al., 2000Tamura, Boonbumrung, et al., 2000Choo, Wong, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-101DB-5CBP-1HP-5
Column length (m) 25.25.30.30.25.
Carrier gas H2NitrogenHeHeHe
Substrate      
Column diameter (mm) 0.250.200.250.250.2
Phase thickness (mum) 0.25 0.25 0.33
Tstart (C) 40.60.60.60.70.
Tend (C) 220.220.240.240.290.
Heat rate (K/min) 3.4.3.4.3.
Initial hold (min) 5.0.  8.
Final hold (min) 5.0.  20.
I 1335.1338.1354.1338.1355.
ReferenceOberhofer, Nikiforov, et al., 1999Tropnikova, Zenkevich, et al., 1999Zoghbi, Andrade, et al., 1999Lamarque, Maestri, et al., 1998Poiana, Sicari, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBBP-1BP-1BP-1
Column length (m) 25.25.25.25.25.
Carrier gas N2HeN2N2N2
Substrate      
Column diameter (mm) 0.320.250.500.500.50
Phase thickness (mum) 0.250.25   
Tstart (C) 50.60.60.60.60.
Tend (C) 290.300.220.220.220.
Heat rate (K/min) 4.6.5.5.5.
Initial hold (min)      
Final hold (min)      
I 1332.1332.1335.1336.1340.
ReferenceBos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1DB-1OV-101
Column length (m) 30.60.60.60.50.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.25 
Tstart (C) 40.80.70.70.80.
Tend (C) 210.210.270.270.200.
Heat rate (K/min) 2.3.2.52.52.
Initial hold (min) 2. 5.5. 
Final hold (min) 33.    
I 1358.1335.1335.1335.1333.
ReferenceSohounhloue, Dangou, et al., 1996Nishimura, 1995Tirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1OV-101OV-101OV-101
Column length (m) 50.30.50.50.50.
Carrier gas  N2N2N2N2
Substrate      
Column diameter (mm) 0.25 0.250.250.25
Phase thickness (mum)      
Tstart (C) 80.80.80.80.80.
Tend (C) 200.220.200.200.200.
Heat rate (K/min) 2.4.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1336.1339.1335.1336.1336.
ReferenceTamura, Yang, et al., 1993Velasco-Negueruela, Pérez Alonso, et al., 1991Yang and Sugisawa, 1990Yang and Sugisawa, 1990Sugisawa, Yamamoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-1DB-1SE-30+Igepal
Column length (m) 50.50.60.60.100.
Carrier gas N2N2Helium  
Substrate      
Column diameter (mm) 0.250.250.500.320.25
Phase thickness (mum)   1.2  
Tstart (C) 80.80.40.50.70.
Tend (C) 200.200.220.250.170.
Heat rate (K/min) 2.2.2.4.1.
Initial hold (min)    0.1 
Final hold (min)    5. 
I 1336.1336.1335.1333.1334.
ReferenceSugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Wahab, Aboutabl, et al., 1987Flath, Mon, et al., 1983Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30+Igepal
Column length (m) 100.
Carrier gas  
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum)  
Tstart (C) 70.
Tend (C) 170.
Heat rate (K/min) 1.
Initial hold (min)  
Final hold (min)  
I 1338.
ReferenceShibamoto and Jennings, 1977
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pinheiro, de Queiros, et al., 2013
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Notes

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