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6-Octen-1-ol, 3,7-dimethyl-, acetate


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSPolydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsDB-5HP-5
Column length (m) 30.  60.30.
Carrier gas Helium  Helium 
Substrate      
Column diameter (mm) 0.25  0.250.32
Phase thickness (mum)    1.00 
Program not specifiednot specifiednot specified40 0C 4 0C/min -> 230 0C 100 0C/min -> 260 0C (11.7 min)not specified
I 1354.1352.1353.1341.1354.
ReferencePinheiro, de Queiros, et al., 2013Robinson, Adams, et al., 2012Robinson, Adams, et al., 2012Miyazaki, Plotto, et al., 2011Riahi, Pourbasheer, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-55 % Phenyl methyl siloxaneCP Sil 8 CBHP-5
Column length (m) 30.30. 50.30.
Carrier gas HeliumHelium HeliumHe
Substrate      
Column diameter (mm) 0.250.25 0.320.25
Phase thickness (mum) 0.250.25 0.250.25
Program 40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)not specifiednot specified60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min)60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
I 1354.1348.1362.1353.1356.
ReferenceQiao, Xie, et al., 2008Qiao, Xie, et al., 2008Agabriel, Cornu, et al., 2007Radusiene, Judzentiene, et al., 2007Jordan, Martinez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5CP Sil 8 CBCP Sil 8 CB
Column length (m) 30.30.30.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Program 60C => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)60C(1min) => 1.5C => 185C => 9C/min => 275C (2min)60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
I 1353.1354.1354.1353.1353.
ReferenceSingh, Marimuthu, et al., 2006Singh G., Maurya S., et al., 2006Srivastava, Mallavarapu, et al., 2006Butkienë, Nivinskienë, et al., 2005Butkienë, Nivinskienë, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SE-30HP-5Methyl SiliconeSE-30
Column length (m) 30. 30. 60.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.25 0.25 0.25
Phase thickness (mum) 0.25 0.25  
Program 60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250Cnot specified60C (4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250Cnot specified50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0C
I 1356.1335.1356.1334.1337.
ReferenceSotomayor, Martínez, et al., 2004Vinogradov, 2004Jordán, Martínez, et al., 2003Bakshu and Raju, 2002Li, Wu, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30CBP-1DB-5HP-1Methyl Silicone
Column length (m) 60.25. 12. 
Carrier gas HeNitrogen He 
Substrate      
Column diameter (mm) 0.250.25 0.20 
Phase thickness (mum)  0.25 0.33 
Program not specifiednot specifiednot specified40 0C 6.7 0C/min -> 87 0C (9 min) 10 0C/min -> 187 0Cnot specified
I 1335.1335.1351.1335.1337.
ReferenceLi, Wu, et al., 2002Ly, Yamauchi, et al., 2001Petrakis, Tsitsimpikou, et al., 2001Betts, 2000Zenkevich, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPacked
Active phase DB-1DB-5OV-101OV-101
Column length (m) 30.  2.5
Carrier gas H2  N2
Substrate    Chromosorb G 60-80mesh DMCS
Column diameter (mm) 0.25   
Phase thickness (mum) 0.25   
Program 45C => 3C/min => 175C => 15C => 240C(10min)not specifiednot specifiednot specified
I 1343.1354.1335.1335.
Referenceda Silva, Figueiredo, et al., 1998Isidorov, Zenkevich, et al., 1997Shibamoto, 1987Swigar and Silverstein, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pinheiro, de Queiros, et al., 2013
Pinheiro, P.F.; de Queiros, V.T.; Rondelli, V.M.; Costa, A.V.; MArcelino, T. deP.; Pratissoli, D., Insecticidal activity of citronells grass essential oil on Frankliniella schultzei and Myzus persicae, Cienc. Agrotec. Lavras, 2013, 37, 2, 138-144, https://doi.org/10.1590/S1413-70542013000200004 . [all data]

Robinson, Adams, et al., 2012
Robinson, A.L.; Adams, D.O.; Boss, P.K.; Heymann, H.; Solomon, P.S.; Trengove, R.D., Influence of geographic origine on the sensory characteristics and wine composition of Vitus viniferas cv. Cabernet Sauvignon wines from Australia (Supplemental data), Am. J. Enol. Vitic., 2012, 64, 4, 467-476, https://doi.org/10.5344/ajev.2012.12023 . [all data]

Miyazaki, Plotto, et al., 2011
Miyazaki, T.; Plotto, A.; Goodner, K.; Gmitter F.G., Distribution of aroma volatile compounds in tangerine hybrids and proposed inheritance, J. Sci. Food Agric., 2011, 91, 3, 449-460, https://doi.org/10.1002/jsfa.4205 . [all data]

Riahi, Pourbasheer, et al., 2009
Riahi, S.; Pourbasheer, E.; Ganjali, M.R.; Norouzi, P., Investigation of different linear and non-linear chemometric methods for modeling of retention index of essential oil components: Concerns to support vector mashine, J. Hazard. Mat., 2009, 166, 2-3, 853-859, https://doi.org/10.1016/j.jhazmat.2008.11.097 . [all data]

Qiao, Xie, et al., 2008
Qiao, Y.; Xie, B.J.; Zhang, Y.; Zhang, Y.; FAn, G.; Yao, X.L.; Pan, S.Y., Characterization of aroma active compounds in fruit juice and peel oil of Junchen sweet orange fruit (Citrus sinensis (L.) Osbeck) by GC-MS and GC-O, Molecules, 2008, 13, 6, 1333-1344, https://doi.org/10.3390/molecules13061333 . [all data]

Agabriel, Cornu, et al., 2007
Agabriel, C.; Cornu, A.; Journal, C.; Sibra, C.; Groller, C.; MArtin, B., Tanker milk variability according to farm feeding practices: vitamins A and E, carotenoids, color, and terpenoids, J. Dairy Sci., 2007, 90, 10, 4884-4896, https://doi.org/10.3168/jds.2007-0171 . [all data]

Radusiene, Judzentiene, et al., 2007
Radusiene, J.; Judzentiene, A.; Peciulyte, D.; Janulis, V., Essential Oil Composition and Antimicrobial Assay of Acorus calamus Leaves from Different Wild Populations, Plant Genetic Resources: Characterization and Utilization, 2007, 5, 1, 37-44, https://doi.org/10.1017/S1479262107390928 . [all data]

Jordan, Martinez, et al., 2006
Jordan, M.J.; Martinez, R.M.; Goodner, K.L.; Baldwin, E.A.; Sotomayor, J.A., Seasonal variation of Thymus hyemalis Lange and Spanish Thymus vulgaris L. essential oils composition, Ind. Crops Prod., 2006, 24, 3, 253-263, https://doi.org/10.1016/j.indcrop.2006.06.011 . [all data]

Singh, Marimuthu, et al., 2006
Singh, G.; Marimuthu, P.; de Heluani, C.S.; Catalan, C.A.N., Antioxidant and biocidal activities of Carum nigrum (seed) essential oil, oleoresin, and their selected components, J. Agric. Food Chem., 2006, 54, 1, 174-181, https://doi.org/10.1021/jf0518610 . [all data]

Singh G., Maurya S., et al., 2006
Singh G.; Maurya S.; de Lampasona M.P.; Catalan C.A.N., Studies on essential oils, Part 41. Chemical composition, antifungal, antioxidant and sprout suppressant activities of coriander (Coriandrum sativum) essential oil and its oleoresin, Flavour Fragr. J., 2006, 21, 3, 472-479, https://doi.org/10.1002/ffj.1608 . [all data]

Srivastava, Mallavarapu, et al., 2006
Srivastava, S.; Mallavarapu, G.R.; Rai, S.K.; Singh, D.; Mishra, R.; Pandey-Rai, S.; Kumar, S., Composition of the essential oils of the leaves and flowers of Rhus mysurensis Heyne ex Wight Arn growing in the Aravalli mountain range at New Delhi, Flavour Fragr. J., 2006, 21, 2, 228-229, https://doi.org/10.1002/ffj.1561 . [all data]

Butkienë, Nivinskienë, et al., 2005
Butkienë, R.; Nivinskienë, O.; Mockutë, D., «alpha»-Pinene chemotype of leaf (needle) essential oils of Juniperus communis L. growing wild in Vilnius district, Chemija, 2005, 16, 1, 53-60. [all data]

Butkienë, Nivinskienë, et al., 2004
Butkienë, R.; Nivinskienë, O.; Mockutë, D., Chemical composition of unripe and ripe berry essential oils of Juniperus communis L. growing wild in Vilnius district, Chemija, 2004, 15, 4, 57-63. [all data]

Sotomayor, Martínez, et al., 2004
Sotomayor, J.A.; Martínez, R.M.; García, A.J.; Jordán, M.J., Thymus zygis Subsp. Gracilis: watering level effect on phytomass production and essential oil quality, J. Agric. Food Chem., 2004, 52, 17, 5418-5424, https://doi.org/10.1021/jf0496245 . [all data]

Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Jordán, Martínez, et al., 2003
Jordán, M.J.; Martínez, R.M.; Cases, M.A.; Sotomayor. J.A., Watering level effect on Thymus hyemalis lange essential oil yield and composition, J. Agric. Food Chem., 2003, 51, 18, 5420-5427, https://doi.org/10.1021/jf034335m . [all data]

Bakshu and Raju, 2002
Bakshu, L.Md.; Raju, R.R.V., Essential oil composition and antimicrobial activity of tuberous roots of Pimpinella tirupatiensis Bal. Subr., an endemic taxon from eastern ghats, India, Flavour Fragr. J., 2002, 17, 6, 413-415, https://doi.org/10.1002/ffj.1118 . [all data]

Li, Wu, et al., 2002
Li, C.; Wu, H.; Yang, L.; ren, Y., Study of the composition of ginger oil from Laifeng, Flavour Fragr. Cosmetics, 2002, 5, 15-17. [all data]

Ly, Yamauchi, et al., 2001
Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

Petrakis, Tsitsimpikou, et al., 2001
Petrakis, P.V.; Tsitsimpikou, C.; Tzakou, O.; Couladis, M.; Vagias, C.; Roussis, V., Needle volatiles from five Pinus species growing in Greece, Flavour Fragr. J., 2001, 16, 4, 249-252, https://doi.org/10.1002/ffj.990 . [all data]

Betts, 2000
Betts, T.J., Solid phase microextraction of volatile constituents from individual fresh Eucalyptis leaves of three species, Planta Medica, 2000, 66, 2, 193-195, https://doi.org/10.1055/s-0029-1243133 . [all data]

Zenkevich, 1999
Zenkevich, I.G., Analytical Parameters of Components of essential Oils for their Gas Chromatographic and Chromato-Mass-Spectral Identification. Acetates of Terpene Alcohols, Rastitelnye Resursy (Plant Resources), 1999, 35, 1, 30-37. [all data]

da Silva, Figueiredo, et al., 1998
da Silva, J.A.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.; Gomes, M.A.; Fontinha, S.S.; Scheffer, J.J.C., Composition of the essential oil of Melanoselinum decipiens (Schrad. Wendl.) Hoffm., an endemic species of the Madeira and Azores archipelagos, Flavour Fragr. J., 1998, 13, 2, 90-92, https://doi.org/10.1002/(SICI)1099-1026(199803/04)13:2<90::AID-FFJ700>3.0.CO;2-D . [all data]

Isidorov, Zenkevich, et al., 1997
Isidorov, V.; Zenkevich, I.; Sacharevich, T., Calculation of Gas Chromatographic Retention Indices for Monoterpenes and Terpenoids from Their Physico-Chemical Constants, Chem. Anal. (Warsaw), 1997, 42, 627-634. [all data]

Shibamoto, 1987
Shibamoto, T., Retention Indices in Essential Oil Analysis in Capillary Gas Chromatography in Essential Oil Analysis, Sandra, P.; Bicchi, C., ed(s)., Hutchig Verlag, Heidelberg, New York, 1987, 259-274. [all data]

Swigar and Silverstein, 1981
Swigar, A.A.; Silverstein, R.M., Monoterpenes, Aldrich Chemical Company, Milwaukee, WI, USA, 1981, 130. [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References