1-Nonanol

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1MSDB-1DB-5DB-5MSSE-30
Column length (m) 30.30.30.30.25.
Carrier gas HeHeH2H2He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.251.
Temperature (C) 90.90.60.60.120.
I 1157.21156.91173.1172.1161.9
ReferenceVickers, Kuhn, et al., 2003Vickers, Kuhn, et al., 2003Kuhn, 2001Kuhn, 2001Golovnya, Kuz'menko, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m) 25.40.25.25.25.
Carrier gas He    
Substrate      
Column diameter (mm) 0.320.350.330.330.33
Phase thickness (μm) 1.0.35   
Temperature (C) 130.100.100.120.140.
I 1161.31153.61149.1147.1143.
ReferenceGolovnya, Kuz'menko, et al., 2000Tudor, 1997Haken and Korhonen, 1985Haken and Korhonen, 1985Haken and Korhonen, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m) 25.25.25.25.3.
Carrier gas     Ar
Substrate     Gas Chrom Q (80-100 mesh)
Column diameter (mm) 0.330.330.330.33 
Phase thickness (μm)      
Temperature (C) 160.180.200.80.150.
I 1140.1140.1167.1154.1160.
ReferenceHaken and Korhonen, 1985Haken and Korhonen, 1985Haken and Korhonen, 1985Haken and Korhonen, 1985Tiess, 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SE-30Apiezon LSE-30SE-30SE-30
Column length (m) 3.7 1.1.1.
Carrier gas   ArArAr
Substrate Celatom AW silanizedCelite 545Chromosorb W AW DMCS HP (80-100 mesh)Chromosorb W AW DMCS HP (80-100 mesh)Chromosorb W AW DMCS HP (80-100 mesh)
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 150.160.100.120.140.
I 1162.1143.1166.1160.1162.
ReferenceHaken, Nguyen, et al., 1979Bogoslovsky, Anvaer, et al., 1978Pías and Gascó, 1975Pías and Gascó, 1975Pías and Gascó, 1975
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPacked
Active phase SE-30SE-30
Column length (m) 2.2.
Carrier gas   
Substrate Chromosorb WChromosorb W
Column diameter (mm)   
Phase thickness (μm)   
Temperature (C) 140.180.
I 1160.1160.
ReferenceZarazir, Chovin, et al., 1970Zarazir, Chovin, et al., 1970
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Vickers, Kuhn, et al., 2003
Vickers, A.K.; Kuhn, E.; Lautamo, R., A novel, inert, low bleed column for GC-MS, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/gcapps.htm. [all data]

Kuhn, 2001
Kuhn, E.R., Selectivity vs. polarity: the fundamentals of chromatographic separation, J. Sep. Sci., 2001, 24, 6, 473-476, https://doi.org/10.1002/1615-9314(20010601)24:6<473::AID-JSSC473>3.0.CO;2-Y . [all data]

Golovnya, Kuz'menko, et al., 2000
Golovnya, R.V.; Kuz'menko, T.E.; Samusenko, A.L., Gas-chromatographic method of evaluation of n-alkanol ability for self-association in pure liquid, Russ. Chem. Bull. (Engl. Transl.), 2000, 49, 2, 317-320, https://doi.org/10.1007/BF02494680 . [all data]

Tudor, 1997
Tudor, E., Temperature dependence of the retention index for perfumery compounds on a SE-30 glass capillary column. I. Linear equations, J. Chromatogr. A, 1997, 779, 1-2, 287-297, https://doi.org/10.1016/S0021-9673(97)00453-6 . [all data]

Haken and Korhonen, 1985
Haken, J.K.; Korhonen, I.O.O., Gas chromatography of homologous esters. XXVII. Retention increments of C1-C18 primary alkanols and their 2-chloropropanoyl and 3-chloropropanoyl derivatives on SE-30 and OV-351 capillary columns, J. Chromatogr., 1985, 319, 131-142, https://doi.org/10.1016/S0021-9673(01)90548-5 . [all data]

Tiess, 1984
Tiess, D., Gaschromatographische Retentionsindices von 125 leicht- bis mittelflüchtigen organischen Substanzen toxikologisch-analytischer Relevanz auf SE-30, Wiss. Z. Wilhelm-Pieck-Univ. Rostock Math. Naturwiss. Reihe, 1984, 33, 6-9. [all data]

Haken, Nguyen, et al., 1979
Haken, J.K.; Nguyen, A.; Wainwright, M.S., Application of linear extrathermodynamic relationships to alcohols, aldehydes, ketones, amd ethoxy alcohols, J. Chromatogr., 1979, 179, 1, 75-85, https://doi.org/10.1016/S0021-9673(00)80658-5 . [all data]

Bogoslovsky, Anvaer, et al., 1978
Bogoslovsky, Yu.N.; Anvaer, B.I.; Vigdergauz, M.S., Chromatographic constants in gas chromatography (in Russian), Standards Publ. House, Moscow, 1978, 192. [all data]

Pías and Gascó, 1975
Pías, J.B.; Gascó, L., GC Retention Data of Alcohols and Benzoyl Derivatives of Alcohols, J. Chromatogr. - Chrom. Data, 1975, d14-d16. [all data]

Zarazir, Chovin, et al., 1970
Zarazir, D.; Chovin, P.; Guiochon, G., Identification of hydroxylic compounds and their derivatives by gas chromatography, Chromatographia, 1970, 3, 4, 180-195, https://doi.org/10.1007/BF02269018 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References