2,6-Octadienal, 3,7-dimethyl-, (E)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryPB-1130.1250.Engewald, Knobloch, et al., 1991Column length: 42. m; Column diameter: 0.32 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP-Sil PONA GB1249.Cunicao, Lopes, et al., 2007100. m/0.25 mm/0.25 μm, He, 140. C @ 10. min, 5. K/min, 230. C @ 25. min
CapillaryEquity-51287.Rocha, Coelho, et al., 200760. m/0.25 mm/1. μm, He, 40. C @ 1. min, 5. K/min, 260. C @ 15. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-51271.Wang, Finn, et al., 200530. m/0.32 mm/1. μm, He; Program: 40C(2min) => 5C/min => 100C => 4C/min => 230C (10min)
CapillaryDB-51270.Beaulieu and Grimm, 200130. m/0.25 mm/0.25 μm, He; Program: 50C (1min) => 5C/min => 100C => 10C/min => 250C (9min)

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax1733.Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 200730. m/0.25 mm/0.5 μm, He, 40. C @ 5. min, 4. K/min, 250. C @ 15. min
CapillaryDB-Wax1714.Osorio, Alarcon, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 4. min, 4. K/min, 220. C @ 20. min
CapillaryDB-Wax1731.Cha, Kim, et al., 199860. m/0.25 mm/0.25 μm, 40. C @ 5. min, 3. K/min, 200. C @ 60. min

Van Den Dool and Kratz RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax1718.Guillot, Peytavi, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 60C => 5C/min => 200C => 6C/min => 250C(5min)
CapillaryStabilwax1729.Wang, Finn, et al., 200530. m/0.32 mm/1. μm, He; Program: 40C(2min) => 5C/min => 100C => 4C/min => 230C (10min)
CapillaryStabilwax1725.Wang, Finn, et al., 200530. m/0.32 mm/1. μm, He; Program: 40C(2min) => 5C/min => 100C => 4C/min => 230C (10min)

Normal alkane RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-51269.Bertuzzi, Tirillini, et al., 201330. m/0.25 mm/0.25 μm, Helium, 60. C @ 3. min, 4. K/min, 300. C @ 15. min
CapillaryRTX-5 MS1278.Pinheiro, de Queiros, et al., 2013Helium, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 240. C
CapillaryRTX-11244.Bendiabdellah, El Amine Dib, et al., 201260. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 5. min; Tstart: 60. C
CapillaryDB-51277.Boukhris, Bouaziz, et al., 201230. m/0.25 mm/0.25 μm, Helium, 100. C @ 1. min, 10. K/min, 260. C @ 10. min
CapillaryHP-5 MS1269.Fanaro, Duarte, et al., 201230. m/0.25 mm/0.25 μm, Helium, 50. C @ 0.5 min, 5. K/min, 250. C @ 0.5 min
CapillaryCP-Sil 5 CB1268.Ameen, Usman, et al., 201125. m/0.25 mm/0.15 μm, Helium; Tstart: 50. C; Tend: 220. C
CapillarySE-30 MS1275.Menichini, Tundis, et al., 201130. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 5. K/min, 250. C @ 10. min
CapillaryHP-5 MS1269.Miyazawa, Marumoto, et al., 201130. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C
CapillaryDB-5 MS1271.Mesa-Arango, Betancur-Galvis, et al., 201060. m/0.25 mm/0.25 μm, Helium, 40. C @ 15. min, 5. K/min, 250. C @ 15. min
CapillaryDB-5 MS1279.Mesa-Arango, Betancur-Galvis, et al., 201060. m/0.25 mm/0.25 μm, Helium, 40. C @ 15. min, 5. K/min, 250. C @ 15. min
CapillaryBP-11244.Mishra, Chaudhary, et al., 2010Nitrogen, 60. C @ 10. min, 5. K/min, 220. C @ 30. min
CapillaryHP-5 MS1273.Radulovic, Blagojevic, et al., 201030. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C
CapillaryDB-1-MS1241.Takeoka, Hobbs, et al., 201060. m/0.25 mm/0.25 μm, Helium, 30. C @ 4. min, 2. K/min, 200. C @ 35. min
CapillaryCP Sil 5 CB1268.Usman, Zubair, et al., 201025. m/0.25 mm/0.15 μm, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryDB-11246.Xu, Tang, et al., 201030. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 4. K/min, 220. C @ 2. min
CapillaryZB-51218.Gardini, Beletti, et al., 200930. m/0.25 mm/0.25 μm, Helium, 3. K/min, 240. C @ 1. min; Tstart: 50. C
CapillaryDB-51267.Ho, Wang, et al., 200930. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryDB-5 MS1267.Koba, Sanda, et al., 200930. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 2. K/min; Tend: 250. C
CapillaryHP-51270.Maridass, 200925. m/0.20 mm/0.33 μm, Helium, 3. K/min, 240. C @ 7. min; Tstart: 60. C
CapillaryBP-11249.Ottavioli, Bighelli, et al., 200950. m/0.22 mm/0.25 μm, Helium, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-51270.Saeidnia and Hadjiakhoondi, 200830. m/0.25 mm/0.25 μm, Nitrogen, 100. C @ 1. min, 5. K/min, 200. C @ 15. min
CapillaryDBP-51236.Heravi and Sereshti, 200725. m/0.25 mm/0.22 μm, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 10. min
CapillaryFSOT-RSL-2001267.Jirovetz, Eller, et al., 200630. m/0.32 mm/0.25 μm, Hydrogen, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryOV-1011260.Lattoo, Dhar, et al., 200625. m/0.25 mm/0.25 μm, He, 8. K/min; Tstart: 100. C; Tend: 250. C
CapillaryDB-11223.Sawamura, Sou, et al., 200460. m/0.25 mm/0.25 μm, Nitrogen, 70. C @ 2. min, 2. K/min; Tend: 230. C
CapillaryMPS-51268.Nakahara, Alzoreky, et al., 200370. C @ 2. min, 5. K/min; Tend: 180. C
CapillaryDB-11252.Nishimura, 199560. m/0.32 mm/0.25 μm, He, 4. K/min; Tstart: 80. C; Tend: 210. C
CapillarySE-301252.Peacock and Kuneman, 1985N2, 45. C @ 1. min, 4. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tend: 250. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryRTX-5 MS1270.Pinheiro, de Queiros, et al., 2013Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryDB-11240.Albano, Lima, et al., 201230. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
CapillaryRTX-11239.Bendiabdellah, El Amine Dib, et al., 201260. m/0.22 mm/0.25 μm, Helium; Program: not specified
CapillarySLB-5 MS1268.Mondello, 201230. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillarySLB-5 MS1273.Mondello, 201230. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillarySiloxane, 5 % Ph1275.VOC BinBase, 2012Program: not specified
CapillaryDB-51268.Miyazaki, Plotto, et al., 201160. m/0.25 mm/1.00 μm, Helium; Program: 40 0C 4 0C/min -> 230 0C 100 0C/min -> 260 0C (11.7 min)
CapillaryHP-5 MS1270.Nance and Setzer, 201130. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
CapillaryHP-5 MS1271.Payo, Colo, et al., 2011Program: not specified
CapillaryHP-5 MS1271.Payo, Colo, et al., 2011Program: not specified
CapillaryPolydimethyl siloxane, 5 % phenyl1275.Skogerson, Wohlgemuth, et al., 2011Program: not specified
CapillaryHP-51267.Wang, Liu, et al., 201130. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)
CapillaryDB-51270.Nezhadali and Parsa, 201030. m/0.20 mm/0.32 μm, Helium; Program: 60 0C (1 min) 3 0C/min -> 140 0C 50 0C/min -> 250 0C (3 min)
CapillaryDB-1-MS1241.Takeoka, Hobbs, et al., 201060. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryDB-11262.Xu, Tang, et al., 201030. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryHP-51265.Custer, 200925. m/0.32 mm/0.17 μm, Helium; Program: 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)
CapillaryHP-51264.Custer, 200925. m/0.32 mm/0.17 μm, Helium; Program: not specified
CapillaryDB-51272.Yang, Yang, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 95 min) 3 0C/min -> 100 0C 4 0C/min -> 160 0C 5 0C/min -> 220 0C (15 min)
CapillaryDB-51270.Beaulieu and Lancaster, 200730. m/0.25 mm/0.25 μm; Program: 50C(1min) => 5C/min => 100C => 10C/min => 250C (9min)
Capillary5 % Phenyl methyl siloxane1272.Beaulieu J.C. and Lea J.M., 200630. m/0.25 mm/0.75 μm; Program: 50C(1min) => 5C/min => 100C => 10C/min => 190C => 30C/min => 250C(1min)
CapillaryDB-11249.Nishimura, 199560. m/0.32 mm/0.25 μm, He; Program: not specified

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-201730.Mishra, Chaudhary, et al., 2010Nitrogen, 5. K/min; Tstart: 60. C; Tend: 200. C
CapillaryBP-201743.Ottavioli, Bighelli, et al., 200950. m/0.22 mm/0.25 μm, Helium, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1737.Lattoo, Dhar, et al., 200625. m/0.25 mm/0.25 μm, He, 8. K/min; Tstart: 100. C; Tend: 250. C
CapillaryDB-Wax1721.Lee, Umano, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 180. C @ 40. min; Tstart: 50. C
CapillaryDB-Wax1744.Sawamura, Sou, et al., 200460. m/0.25 mm/0.25 μm, Nitrogen, 70. C @ 2. min, 2. K/min; Tend: 230. C
CapillaryDB-Wax1726.Umano, Hagi, et al., 200060. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 2. K/min; Tend: 200. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySupelco CO Wax-101738.Prompona, Kandylis, et al., 201260. m/0.32 mm/0.25 μm, Helium; Program: 35 0C (6 min) 2 0C/min -> 60 0C (5 min) 5 0C/min -> 200 0C 25 0C/min -> 250 0C (6 min)
CapillarySupelco CO Wax-101741.Prompona, Kandylis, et al., 201260. m/0.32 mm/0.25 μm, Helium; Program: not specified
CapillaryCP-Wax 52 CB1735.Genisheva and Oliveira, 200950. m/0.25 mm/0.20 μm, Helium; Program: 60 0C (5 min) 3 0C/min -> 250 0C (20 min) 1 0C/min -> 255 0C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Lattoo, S.K.; Dhar, R.S.; Dhar, A.K.; Sharma, P.R.; Agarwal, S.G., Dynamics of essential oil biosynthesis in relation to inflorescence and glandular ontogeny in Salvia sclarea, Flavour Fragr. J., 2006, 21, 5, 817-821, https://doi.org/10.1002/ffj.1733 . [all data]

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Notes

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