2,6-Octadien-1-ol, 3,7-dimethyl-, acetate, (Z)-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSRTX-1SE-30 MSDB-5 MSRTX-1
Column length (m) 60.60.30.25.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.300.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.50.50.60.
Tend (C) 250.230.250.240.230.
Heat rate (K/min) 3.2.5.3.2.
Initial hold (min) 1. 5.  
Final hold (min) 20.5.10. 30.
I 1367.1342.1370.1358.1342.
ReferenceSardashti, Valizadeh, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012Menichini, Tundis, et al., 2011Chalchat, Figueredo, et al., 2010Dib, Djabou, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1BP-1HP-5HP-5 MSDB-1-MS
Column length (m) 60. 30.30.60.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.22 0.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.60.40.70.30.
Tend (C) 230.220.260.290.200.
Heat rate (K/min) 2.5.4.5.2.
Initial hold (min)  10.  4.
Final hold (min) 30.30.5.10.35.
I 1342.1337.1366.1359.1343.
ReferenceDib, Djabou, et al., 2010Mishra, Chaudhary, et al., 2010Miyazawa, Kawauchi, et al., 2010Radulovic, Dordevic, et al., 2010Takeoka, Hobbs, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5BP-1DB-5 MSDB-5DB-1 MS
Column length (m) 60.50.60.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.350.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.45.40.
Tend (C) 230.220.330.250.250.
Heat rate (K/min) 4.2.2.3.6.
Initial hold (min)   12.3.1.
Final hold (min) 40.20.30.5.4.
I 1363.1341.1378.1366.1341.
ReferenceGauvin-Bialecki and Marodon, 2009Ottavioli, Bighelli, et al., 2009Patil, Jayaprakasha, et al., 2009Porto, Decorti, et al., 2009Seo, Kim, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSLB-5 MSDB-5RTX-1OV-1
Column length (m) 30.30.60.60.30.
Carrier gas HeliumHeliumNitrogenHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.65.
Tend (C) 240.250.250.230.260.
Heat rate (K/min) 5.3.5.2.6.
Initial hold (min)  2.   
Final hold (min)  10.10.35. 
I 1385.1357.1365.1342.1396.
ReferenceWannes, Mhamdi, et al., 2009Lo Presti, Sciarrone, et al., 2008Mosayebi, Amin, et al., 2008Paolini, Tomi, et al., 2008Wang, Yi, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSHP-5MSDB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeliumHydrogen
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 300.250.250.260.250.
Heat rate (K/min) 4.2.2.2.54.
Initial hold (min)  8.8.1. 
Final hold (min)  15.15.20. 
I 1344.1372.1361.1340.1363.
ReferenceBaran, von Reuss, et al., 2007Ferhat, Meklati, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Monser-Esfahani, Karamkhani, et al., 2007Pontes, de Olivera, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1HP-1HP-1DB-5
Column length (m) 30.60.50.50.30.
Carrier gas HeliumNitrogenHeHeN2
Substrate      
Column diameter (mm) 0.250.250.20.20.25
Phase thickness (μm) 0.250.250.50.330.25
Tstart (C) 60.60.60.60.70.
Tend (C) 220.250.250.250.230.
Heat rate (K/min) 5.5.2.2.2.
Initial hold (min) 3.  4.2.
Final hold (min) 3.10.120.30.20.
I 1341.1358.1336.1336.1362.
ReferenceSafaei-Ghomi, Bamoniri, et al., 2007Sonboli, Kanani, et al., 2007Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Choi, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1FSOT-RSL-200DB-1DB-1
Column length (m) 50.60.30.60.60.
Carrier gas He Hydrogen  
Substrate      
Column diameter (mm) 0.220.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.70.70.
Tend (C) 220.250.280.230.230.
Heat rate (K/min) 2.5.6.2.2.
Initial hold (min)   5.2.2.
Final hold (min) 20.10.5.20.20.
I 1340.1342.1364.1341.1341.
ReferenceFanciullino, Tomi, et al., 2006Hadian, Sonboli, et al., 2006Jirovetz, Eller, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5CP-Sil 5 CBNB-30HP-5
Column length (m) 30.30.25.30.25.
Carrier gas N2HeliumHydrogenHeH2
Substrate      
Column diameter (mm) 0.320.250.250.20.32
Phase thickness (μm) 0.250.250.150.250.25
Tstart (C) 50.50.50.50.60.
Tend (C) 300.250.230.250.240.
Heat rate (K/min) 4.3.3.2.3.
Initial hold (min)  5.   
Final hold (min)      
I 1348.1363.1342.1345.1371.
ReferenceLis and Milczarek, 2006Mirza, Navaei, et al., 2006Olawore, Usman, et al., 2006Orav, Raal, et al., 2006Potzernheim, Bizzo, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSDB-1SPB-1DB-5
Column length (m) 60.30.30.30.30.
Carrier gas  Helium HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.60.50.40.
Tend (C) 230.250.230.250.250.
Heat rate (K/min) 2.2.3.4.4.
Initial hold (min) 2.8.3.1. 
Final hold (min) 20.15.10.10. 
I 1343.1361.1343.1361.1351.
ReferenceSawamura, Onishi, et al., 2006Tigrine-Kordiani, Meklati, et al., 2006Tohar, Mohd, et al., 2006Wong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-5SPB-1HP-5MS
Column length (m) 25.60.30.30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.20.250.250.250.2
Phase thickness (μm) 0.330.250.250.2 
Tstart (C) 60.60.50.60.60.
Tend (C) 240.250.300.250.280.
Heat rate (K/min) 3.5.5.6.3.
Initial hold (min)   5.2. 
Final hold (min) 7. 5.  
I 1364.1343.1357.1346.1362.
ReferenceDuarte, Figueira, et al., 2005Fakhari, Salehi, et al., 2005Figuérédo, Cabassu, et al., 2005Hamilton, Hall, et al., 2005Petrakis, Roussis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5SPB-1DB-5SE-54
Column length (m) 30.30.50.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.20.250.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 60.60.50.40.60.
Tend (C) 280.280.220.280.260.
Heat rate (K/min) 3.3.4.4.2.
Initial hold (min) 5. 3.4.5.
Final hold (min)   30.  
I 1368.1334.1343.1365.1365.
ReferenceSetzer, Noletto, et al., 2005Tzakou and Constantinidis, 2005Wong and Tan, 2005Kalvandi, Sefidkon, et al., 2004Kilic, Hafizoglu, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-5MSHP-5MSNB-30
Column length (m) 30.30.30.30.50.
Carrier gas N2 HeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.20
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.50.
Tend (C) 300.210.280.280.250.
Heat rate (K/min) 4.2.3.3.2.
Initial hold (min)  2.   
Final hold (min)  33.30.  
I 1343.1368.1334.1364.1345.
ReferenceLis, Boczek, et al., 2004Lopez Arze, Collin, et al., 2004Marongiu, Piras, et al., 2004Mimica-Dukic, Bozin, et al., 2004Raal, Paaver, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1DB-1DB-5BPX-5
Column length (m) 30.60.60.30.25.
Carrier gas He NitrogenHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.250.251.
Tstart (C) 60.70.70.40.60.
Tend (C) 280.230.230.250.250.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min)  2.2.5.5.
Final hold (min)  20. 20.10.
I 1360.1352.1352.1351.1386.
ReferenceSadeghpour, Asghari, et al., 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Senatore, Rigano, et al., 2004Vilaseca, Guy, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RTX-5SilDB-5ZB-1HP-5
Column length (m) 60.30.50.30.30.
Carrier gas HeHeHeN2Helium
Substrate      
Column diameter (mm) 0.250.250.20.250.32
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 70.70.50.45.70.
Tend (C) 230.200.220.230.210.
Heat rate (K/min) 2.4.3.3.2.
Initial hold (min) 2. 2.  
Final hold (min) 20.10.10. 60.
I 1352.1362.1366.1344.1366.
ReferenceChoi, 2003Dudai, Larkov, et al., 2003Juteau, Jerkovic, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mookdasanit, Tamura, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-1DB-1DB-5
Column length (m) 30.30.60.60.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.70.70.60.
Tend (C) 280.240.230.230.280.
Heat rate (K/min) 3.3.2.2.3.
Initial hold (min)   2.2. 
Final hold (min)   20.20.30.
I 1345.1366.1352.1352.1357.
ReferencePitarokili, Tzakou, et al., 2003da Silva, Luz, et al., 2003Tu, Onishi, et al., 2003Tu, Onishi, et al., 2003, 2Caredda, Marongiu, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-1DB-1DB-1
Column length (m) 30.30.30.50.60.
Carrier gas H2HeHeN2He
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.80.40.
Tend (C) 245.290.250.225.280.
Heat rate (K/min) 3.7.4.4.4.
Initial hold (min) 20. 10. 5.
Final hold (min)      
I 1336.1385.1368.1340.1338.
ReferenceGancel, Ollé, et al., 2002Lin, Rouseff, et al., 2002Norouzi-Arasi, Yavari, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002Sefidkon, Jalili, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSBP-1DB-5DB-5
Column length (m) 30.60.50.60.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.35.60.50.60.
Tend (C) 240.250.230.250.285.
Heat rate (K/min) 3.3.2.3.3.
Initial hold (min)  5. 5. 
Final hold (min)   35.  
I 1355.1360.1340.1365.1364.
ReferenceCherchi, Deidda, et al., 2001Fernando and Grün, 2001Lota, de Rocca Serra, et al., 2001Rousis, Papadogianni, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SPB-5DB-1DB-5BP-1
Column length (m) 50.60.25.30.25.
Carrier gas N2HeNitrogenN2N2
Substrate      
Column diameter (mm) 0.250.250.500.220.33
Phase thickness (μm)  0.250.250.251.0
Tstart (C) 80.70.60.70.60.
Tend (C) 200.240.220.230.275.
Heat rate (K/min) 2.5.5.4.4.
Initial hold (min)  8. 2. 
Final hold (min)  20. 20. 
I 1341.1365.1341.1358.1365.
ReferenceYang, 2001Kim, Kim, et al., 2000Mallavarapu, Rao, et al., 2000Mitiku, Sawamura, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-1OV-101HP-5HP-1
Column length (m) 25.60.25.25.60.
Carrier gas H2HeNitrogenHeHe
Substrate      
Column diameter (mm) 0.250.320.200.20.25
Phase thickness (μm) 0.25  0.330.25
Tstart (C) 40.60.60.70.50.
Tend (C) 220.230.220.290.280.
Heat rate (K/min) 3.3.4.3.4.
Initial hold (min) 5. 0.8.5.
Final hold (min) 5.5.0.20. 
I 1344.1347.1347.1366.1326.
ReferenceOberhofer, Nikiforov, et al., 1999Shafiee, Javidnia, et al., 1999Tropnikova, Zenkevich, et al., 1999Poiana, Sicari, et al., 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101BP-1OV-101DB-1
Column length (m) 30.50.25.52.60.
Carrier gas HeliumHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.500.260.25
Phase thickness (μm) 0.25   0.25
Tstart (C) 60.50.60.50.70.
Tend (C) 240.250.220.220.270.
Heat rate (K/min) 3.2.5.3.2.5
Initial hold (min)     5.
Final hold (min)      
I 1365.1345.1344.1343.1340.
ReferenceTellez, Estell, et al., 1997Orav, Kailas, et al., 1996Rajeswara, Kaul, et al., 1996Dzumayev, Tsibulskaya, et al., 1995Tirado, Stashenko, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeMethyl SiliconeOV-101OV-101SPB-5
Column length (m) 50.50.50.50.30.
Carrier gas N2N2   
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (μm) 0.170.17  1.0
Tstart (C) 80.80.80.80.50.
Tend (C) 200.200.200.200.250.
Heat rate (K/min) 2.3.2.2.8.
Initial hold (min)      
Final hold (min)      
I 1345.1346.1341.1344.1361.
ReferenceGopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993King and Knight, 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 50.50.50.50.50.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)      
Tstart (C) 80.80.80.80.80.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1343.1344.1344.1342.1344.
ReferenceYang and Sugisawa, 1990Yang and Sugisawa, 1990Sugisawa, Yamamoto, et al., 1989Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-101DB-1SE-30+IgepalSE-30+Igepal
Column length (m) 60.30.60.100.100.
Carrier gas HeliumHe   
Substrate      
Column diameter (mm) 0.500.50.320.250.25
Phase thickness (μm) 1.20.8   
Tstart (C) 40.40.50.70.70.
Tend (C) 220.220.250.170.170.
Heat rate (K/min) 2.2.4.1.1.
Initial hold (min)   0.1  
Final hold (min)   5.  
I 1343.1348.1339.1345.1349.
ReferenceWahab, Aboutabl, et al., 1987De Pooter and Schamp, 1986Flath, Mon, et al., 1983Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

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Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

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Chalchat, Figueredo, et al., 2010
Chalchat, J.-C.; Figueredo, G.; Ozcan, M.M.; Unver, A., Effect of hydrodistillation and microwave distillation extraction methods on chemical composition of essential oil of pickling herb and myrtle plants, South Western J. of Agriculture, 2010, 1, 2, 133-141. [all data]

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Radulovic, Dordevic, et al., 2010
Radulovic, N.; Dordevic, N.; Markovic, M.; Palic, R., Volatile constituents of Glechoma Hirsuta Waldst. Kit. and G. Hederacea L. (Lamiaceae), Bull. Chem. Soc. Ethiop., 2010, 24, 1, 67-76, https://doi.org/10.4314/bcse.v24i1.52962 . [all data]

Takeoka, Hobbs, et al., 2010
Takeoka, G.R.; Hobbs, C.; Byeoung-Soo, P., Volatile constituents of the aerial parts of Salvia apiana Jepson, J. Essential Oil. Res., 2010, 22, 3, 241-244, https://doi.org/10.1080/10412905.2010.9700314 . [all data]

Gauvin-Bialecki and Marodon, 2009
Gauvin-Bialecki, A.; Marodon, C., Essential oil of Ayapana triplinervis from Reunion island: a good natural source of thymohydroquinone dimethyl ether, Biochem. Systematics Ecol., 2009, 36, 11, 853-858, https://doi.org/10.1016/j.bse.2008.09.006 . [all data]

Ottavioli, Bighelli, et al., 2009
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Notes

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