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Pyrazine, 2-ethyl-3,5-dimethyl-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-301059.Greenberg, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C
CapillarySE-301062.Greenberg, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-51079.Steinhaus and Schieberle, 200730. m/0.32 mm/0.25 «mu»m, 40. C @ 2. min, 6. K/min, 240. C @ 10. min
CapillaryCP Sil 8 CB1075.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryBPX-51093.Bredie, Mottram, et al., 200250. m/0.32 mm/0.5 «mu»m, 60. C @ 5. min, 4. K/min, 250. C @ 20. min
CapillaryBPX-51088.Ames, Guy, et al., 200150. m/0.32 mm/0.25 «mu»m, He, 60. C @ 5. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51092.Ames, Guy, et al., 200150. m/0.32 mm/0.25 «mu»m, He, 60. C @ 5. min, 4. K/min, 250. C @ 10. min
CapillaryDB-5MS1074.Baek, Kim, et al., 200160. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 3. K/min, 200. C @ 60. min
CapillaryBPX-51084.Oruna-Concha, Duckham, et al., 200150. m/0.32 mm/0.25 «mu»m, He, 35. C @ 3. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51082.Oruna-Concha, Duckham, et al., 200150. m/0.32 mm/0.25 «mu»m, He, 35. C @ 3. min, 4. K/min, 250. C @ 10. min
CapillaryDB-11070.Wu, Wang, et al., 200060. m/0.25 mm/1. «mu»m, N2, 5. K/min, 200. C @ 30. min; Tstart: 30. C
CapillaryDB-11068.Wu, Wang, et al., 200060. m/0.25 mm/1. «mu»m, N2, 5. K/min, 200. C @ 30. min; Tstart: 30. C
CapillaryBPX-51086.Hill, Isaacs, et al., 199950. m/0.325 mm/0.5 «mu»m, He, 20. C @ 2. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51087.Hill, Isaacs, et al., 199950. m/0.325 mm/0.5 «mu»m, He, 20. C @ 2. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51085.Ames, Defaye, et al., 199750. m/0.325 mm/0.5 «mu»m, He, 50. C @ 2. min, 4. K/min, 250. C @ 10. min
CapillaryDB-11064.Specht and Baltes, 199460. m/0.25 mm/0.25 «mu»m, 35. C @ 10. min, 2. K/min, 280. C @ 10. min
CapillaryHP-11064.Zhang, Dorjpalam, et al., 199250. m/0.32 mm/1.5 «mu»m, 2. K/min, 220. C @ 30. min; Tstart: 40. C
CapillarySE-301060.Misharina, Golovnya, et al., 199150. m/0.32 mm/0.25 «mu»m, 4. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-11067.Zhang and Ho, 199160. m/0.25 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 10. min; Tstart: 40. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySPB-51081.Majcher and Jelen, 200730. m/0.53 mm/1.5 «mu»m; Program: 40C(1min) => 6C/min => 180C => 20C/min => 280C
CapillarySE-541084.Frauendorfer and Schieberle, 200625. m/0.32 mm/0.25 «mu»m, He; Program: 40C(1min) => 40C/min => 60C(1min) => 4C/min => 140C => 20C/min => 240C(5min)
CapillaryZB-51059.Lu, Hao, et al., 200530. m/0.25 mm/0.25 «mu»m, He; Program: 50C(1min) => 3C/min => 209C => 20C/min => 280C
CapillaryDB-51081.Majcher and Jelén, 200530. m/0.25 mm/0.25 «mu»m, He; Program: 40C(1min) => 6C/min => 180C => 20C/min => 280C
CapillaryCP Sil 8 CB1088.Duckham, Dodson, et al., 200160. m/0.25 mm/0.25 «mu»m; Program: 0C => rapidly => 40C(8min) => 4C/min => 250C(10min)
CapillaryDB-51082.Rychlik and Bosset, 200130. m/0.32 mm/0.25 «mu»m, He; Program: 35C(2min) => 40C/min => 60C (2min) => 4C/min => 240C
CapillaryDB-51098.Parker, Hassell, et al., 200050. m/0.32 mm/0.5 «mu»m, He; Program: oC(5min) => 60C/min => 60C (5min) => 4C/min => 250C
CapillarySE-541083.Tairu, Hofmann, et al., 200030. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C (5min) => 10C/min => 230C (5min)
CapillaryBPX-51087.Bredie, Mottram, et al., 199850. m/0.32 mm/0.5 «mu»m, He; Program: OC (5min) => 60C/min => 60C(5min) => 4C/min => 250C
CapillarySE-541085.Fickert and Schieberle, 199825. m/0.32 mm/0.5 «mu»m, He; Program: 35C (2min) => 4C/min => 150C => 10C/min => 240C
CapillarySE-541083.Hofmann and Schieberle, 199830. m/0.32 mm/0.25 «mu»m; Program: 35C(2min) => 40C/min => 50C(5min) => 6C/min => 230C(15min)
CapillarySE-541079.Münch, Hofmann, et al., 199730. m/0.32 mm/0.25 «mu»m, He; Program: 40C (2min) => 40C/min => 50C (2min) => 240C (10min)
CapillaryBPX-51088.Owens J.D., Allagheny N., et al., 199750. m/0.32 mm/0.5 «mu»m, He; Program: OC => 60C/min => 60C(5min) => 4C/min => 250C(20min)
CapillaryDB-11068.Kuo, Zhang, et al., 198960. m/0.32 mm/0.25 «mu»m, He; Program: -40C => 40C/min => 40C => 2C/min => 260C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax1464.Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 200730. m/0.25 mm/0.5 «mu»m, He, 40. C @ 5. min, 4. K/min, 250. C @ 15. min
CapillaryDB-Wax1464.Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 200730. m/0.25 mm/0.5 «mu»m, He, 40. C @ 5. min, 4. K/min, 250. C @ 15. min
CapillaryFFAP1435.Steinhaus and Schieberle, 200730. m/0.32 mm/0.25 «mu»m, 40. C @ 2. min, 6. K/min, 240. C @ 10. min
CapillaryDB-Wax1455.Lopez-Galilea I., Fournier N., et al., 200630. m/0.32 mm/0.5 «mu»m, He, 5. K/min, 240. C @ 10. min; Tstart: 40. C
CapillaryDB-Wax1455.Lopez-Galilea I., Fournier N., et al., 200630. m/0.32 mm/0.5 «mu»m, He, 5. K/min, 240. C @ 10. min; Tstart: 40. C
CapillaryCP-Wax 52CB1449.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCP-Wax 52CB1456.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryFFAP1494.Stephan and Steinhart, 199960. m/0.25 mm/0.5 «mu»m, 50. C @ 3. min, 5. K/min, 230. C @ 15. min
CapillaryPEG-20M1462.Shimoda, Nakada, et al., 199760. m/0.25 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillaryDB-Wax1462.Shimoda, Shiratsuchi, et al., 199660. m/0.25 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillarySupelcowax-101434.Cadwallader, Tan, et al., 199560. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 200. C @ 30. min
CapillarySupelcowax-101446.Tanchotikul and Hsieh, 198960. m/0.25 mm/0.25 «mu»m, 40. C @ 5. min, 2. K/min, 175. C @ 20. min
CapillarySupelcowax-101447.Tanchotikul and Hsieh, 198960. m/0.25 mm/0.25 «mu»m, 40. C @ 5. min, 2. K/min, 175. C @ 20. min
CapillaryCP-WAX 57CB1466.Salter L.J., Mottram D.S., et al., 198860. C @ 5. min, 4. K/min; Column length: 50. m; Column diameter: 0.32 mm; Tend: 200. C
CapillaryCP-WAX 57CB1466.Whitfield, Mottram, et al., 1988He, 60. C @ 5. min, 4. K/min, 200. C @ 10. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCP-WAX 57CB1466.Whitfield, Mottram, et al., 1988He, 60. C @ 5. min, 4. K/min, 200. C @ 10. min; Column length: 50. m; Column diameter: 0.32 mm

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySupelcowax-101443.Bianchi, Careri, et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 35C(8min) => 4C/min => 60C => 6C/min => 160C => 20C/min => 200C(1min)
CapillarySupelcowax-101444.Bianchi, Careri, et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 35C(8min) => 4C/min => 60C => 6C/min => 160C => 20C/min => 200C(1min)
CapillarySupelcowax-101437.Majcher and Jelen, 200730. m/0.25 mm/0.25 «mu»m; Program: 40C(2min) => 40C/min => 60C(2min) => 5C/min => 240C
CapillaryFFAP1446.Frauendorfer and Schieberle, 200625. m/0.32 mm/0.2 «mu»m, He; Program: 40C(1min) => 40C/min => 60C(1min) => 6C/min => 180C => 15C/min => 240C
CapillarySupelcowax-101437.Majcher and Jelén, 200530. m/0.25 mm/0.25 «mu»m, He; Program: 40C(2min) => 40C/min => 60(2min)C => 5C/min => 240C
CapillaryCP-Wax 52CB1454.Alasalvar, Shahidi, et al., 200360. m/0.25 mm/0.25 «mu»m, He; Program: 40C => 5C/min => 60C => 2.5C/min => 155C
CapillaryFFAP1453.Rhlid, Fleury, et al., 200230. m/0.32 mm/0.25 «mu»m; Program: 50C (2min) => 6C/min => 180C => 10C/min => 240C(10min)
CapillaryFFAP1451.Rhlid, Fleury, et al., 200230. m/0.32 mm/0.25 «mu»m; Program: 50C (2min) => 6C/min => 180C => 10C/min => 240C(10min)
CapillaryFFAP1455.Tairu, Hofmann, et al., 200030. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C (5min) => 10C/min => 230C (5min)
CapillaryFFAP1454.Fickert and Schieberle, 199825. m/0.32 mm/0.5 «mu»m, He; Program: 35C (2min) => 40C/min => 60C => 6C/min => 230C (10min)
CapillaryFFAP1461.Hofmann and Schieberle, 199830. m/0.32 mm/0.25 «mu»m; Program: 35C(2min) => 40C/min => 60C(5min) => 6C/min => 230C(15min)
CapillaryFFAP1440.Münch, Hofmann, et al., 199730. m/0.32 mm/0.25 «mu»m, He; Program: 40C (2min) => 40C/min => 60C (2min) => 240C (10min)
CapillarySupelcowax-101455.Baek and Cadwallader, 199660. m/0.25 mm/0.25 «mu»m; Program: 40C => (6C/min) => 80C(6min) => (15C/min) => 200C(10min)
CapillaryDB-Wax1455.Amrani-Hemaimi, Cerny, et al., 199530. m/0.32 mm/0.25 «mu»m, He; Program: 35C(2min) => 6C/min => 150C => 30C/min => 240C(1min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5 MS1091.Chen, Song, et al., 200930. m/0.32 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 6. K/min, 230. C @ 20. min
CapillaryDB-5 MS1092.Chen, Song, et al., 200930. m/0.32 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 6. K/min, 250. C @ 20. min
CapillarySLB-5MS1094.Risticevic, Carasek, et al., 200810. m/0.18 mm/0.18 «mu»m, Helium, 40. C @ 1.5 min, 10. K/min; Tend: 295. C
CapillaryDB-51090.Fadel, Mageed, et al., 2006He, 60. C @ 5. min, 4. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tend: 250. C
CapillaryDB-5 MS1095.Schirack, Drake, et al., 200630. m/0.25 mm/0.25 «mu»m, 40. C @ 3. min, 8. K/min, 200. C @ 20. min
CapillaryHP-51078.6Leffingwell and Alford, 200560. m/0.32 mm/0.25 «mu»m, He, 30. C @ 2. min, 2. K/min, 260. C @ 28. min
CapillaryMDN-51085.van Loon, Linssen, et al., 200560. m/0.25 mm/0.25 «mu»m, He, 40. C @ 4. min, 4. K/min, 270. C @ 5. min
CapillaryMDN-51090.van Loon, Linssen, et al., 200560. m/0.25 mm/0.25 «mu»m, He, 40. C @ 4. min, 4. K/min, 270. C @ 5. min
CapillaryDB-51080.Sanz, Czerny, et al., 200230. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 6. K/min, 230. C @ 5. min
CapillaryDB-5MS1084.Cadwallader and Heo, 200130. m/0.53 mm/1.5 «mu»m, He, 40. C @ 5. min, 6. K/min, 225. C @ 30. min
CapillaryDB-5MS1095.Welty, Marshall, et al., 2001He, 40. C @ 5. min, 5. K/min, 220. C @ 5. min; Column length: 50. m; Column diameter: 0.25 mm
CapillaryHP-51085.Boylston and Viniyard, 199850. m/0.32 mm/0.52 «mu»m, 35. C @ 15. min, 2. K/min, 250. C @ 45. min
CapillaryOV-1011045.Deibler, Acree, et al., 199810. m/0.25 mm/0.52 «mu»m, Helium, 35. C @ 3. min, 6. K/min; Tend: 225. C
CapillaryDB-11054.Buttery, Ling, et al., 199730. C @ 25. min, 4. K/min, 200. C @ 20. min; Column length: 60. m; Column diameter: 0.25 mm
CapillaryUltra 11058.Farkas, Sádecká, et al., 199750. m/0.20 mm/0.33 «mu»m, Helium, 30. C @ 1. min, 1.7 K/min; Tend: 250. C
CapillaryDB-11072.Lu, Yu, et al., 199760. m/0.32 mm/1. «mu»m, He, 40. C @ 2. min, 2. K/min, 280. C @ 40. min
CapillaryDB-11065.Yu and Ho, 199560. m/0.25 mm/1. «mu»m, He, 40. C @ 5. min, 2. K/min, 260. C @ 60. min
CapillaryDB-11072.Yu, Wu, et al., 199460. m/0.25 mm/1.0 «mu»m, He, 40. C @ 5. min, 2. K/min, 260. C @ 60. min
CapillaryOV-1011064.Mihara and Masuda, 1987N2, 2. K/min; Column length: 50. m; Column diameter: 0.22 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-11056.Wu, Liou, et al., 1987Hydrogen, 1. K/min, 200. C @ 35. min; Column length: 50. m; Column diameter: 0.20 mm; Tstart: 50. C
CapillaryMethyl Silicone1056.Lorenz, Stern, et al., 19834. K/min, 200. C @ 15. min; Column length: 25. m; Column diameter: 0.2 mm; Tstart: 50. C
CapillaryMethyl Silicone1059.Lorenz, Stern, et al., 19834. K/min, 200. C @ 15. min; Column length: 25. m; Column diameter: 0.2 mm; Tstart: 50. C
CapillarySE-301062.Heydanek and McGorrin, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-51077.Yu and Zhang, 201030. m/0.25 mm/0.25 «mu»m; Program: 40 0C (5 min) 5 0C/min -> 260 0C 15 0C/min -> 280 0C (1 min)
CapillarySE-541084.Frauendorfer and Schieberle, 2008Helium; Program: not specified
CapillarySLB-5MS1083.Risticevic, Carasek, et al., 200810. m/0.18 mm/0.18 «mu»m, Helium; Program: not specified
CapillaryHP-5 MS1088.Wan Aida, Ho, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C (2 min) 20 0C/min -> 80 0C (1 min) 20 0C -> 100 0C (1 min) 30 0C/min -> 230 0C (2 min)
CapillaryHP-51077.Characterization of Pyrazines in Some Chinese Liquors and Their Approximate Concentrations, 200730. m/0.25 mm/0.25 «mu»m, He; Program: 50C(2min) => 2C/min => 140C => 10C/min => 280C (10min)
CapillaryHP-5MS1088.Ho, Wan Aida, et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 50C(2min) => 20C/min => 80C (1min) => 20C/min => 100C(1min) => 30C/min => 230C(3min)
CapillarySE-541083.Lasekan, Buettner, et al., 200730. m/0.32 mm/0.25 «mu»m; Program: 35C(2min) => 40C/min => 60C(2min) => 6C/min => 180C => 10C/min => 230C(10min)
CapillaryCP Sil 5 CB1058.Bailly, Jerkovic, et al., 200650. m/0.32 mm/1.2 «mu»m, He; Program: 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C
CapillaryHP-11047.Carpino, Mallia, et al., 200412. m/0.32 mm/0.52 «mu»m; Program: 35C(3min) => 6C/min => 190C => 30C/min => 225C
CapillaryCP Sil 5 CB1056.Counet, Ouwerx, et al., 200450. m/0.32 mm/1.2 «mu»m; Program: 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)
CapillaryDB-51062.Bücking and Steinhart, 200230. m/0.53 mm/1.5 «mu»m; Program: -5C(1min) => 4C/min => 50C => 6C/min => 120C => 8C/min => 250C(2min)
CapillaryCP Sil 5 CB1057.Counet, Callemien, et al., 200250. m/0.32 mm/1.2 «mu»m; Program: 36C => 20C/min => 85C => 1C/min => 145C=3C/min => 250C(30min)
CapillaryCP Sil 8 CB1087.Duckham, Dodson, et al., 200160. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryCP Sil 8 CB1093.Duckham, Dodson, et al., 200160. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryRTX-51089.Masanetz, Guth, et al., 1998Program: not specified
CapillaryDB-51082.Matsui, Guth, et al., 199830. m/0.32 mm/0.25 «mu»m, He; Program: 35C(1min) => 40C/min => 60C (1min) => 6C/min => 230C
CapillarySE-541086.Zehentbauer and Grosch, 199825. m/0.32 mm/0.25 «mu»m, He; Program: 35C(2min) => 50C/min => 60C(2min) => 4C/min => 230C
CapillarySE-541083.Schermann and Schieberle, 199730. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillarySE-541083.Schermann and Schieberle, 199730. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillarySE-541083.Schermann and Schieberle, 199730. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillaryDB-51083.Schieberle, 1996Column length: 30. m; Column diameter: 0.32 mm; Program: not specified
CapillaryDB-51083.Schieberle and Grosch, 1994He; Column length: 30. m; Column diameter: 0.32 mm; Program: 35C => 40C/min => 50C(2min) => 4C/min => 240C
CapillarySE-541082.Guth and Grosch, 1993Program: not specified
CapillarySE-541083.Blank, Sen, et al., 1992Program: not specified
CapillaryDB-11060.Kawai, Ishida, et al., 199160. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryDB-11061.Kawai, Ishida, et al., 199160. m/0.25 mm/0.25 «mu»m; Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1440.Puvipirom and Chaisei, 201215. m/0.32 mm/0.50 «mu»m, Helium, 3. K/min; Tstart: 40. C; Tend: 250. C
CapillaryDB-Wax1470.Onishi, Inoue, et al., 201160. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 2. min, 3. K/min, 220. C @ 20. min
CapillaryDB-Wax1464.Kumazawa, Sakai, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1477.Rochat, Egger, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 3. min, 8. K/min, 200. C @ 9.5 min
CapillaryDB-Wax1447.Characterization of Pyrazines in Some Chinese Liquors and Their Approximate Concentrations, 200730. m/0.25 mm/0.25 «mu»m, He, 4. K/min, 230. C @ 15. min; Tstart: 50. C
CapillaryDB-Wax1443.Schirack, Drake, et al., 200630. m/0.25 mm/0.25 «mu»m, 40. C @ 3. min, 8. K/min, 200. C @ 20. min
CapillaryTC-Wax1474.Ishizaki, Tachihara, et al., 200560. m/0.25 mm/0.25 «mu»m, N2, 3. K/min, 220. C @ 40. min; Tstart: 70. C
CapillaryDB-Wax1470.Kumazawa, Kubota, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryTC-Wax1475.Ishikawa, Ito, et al., 200460. m/0.25 mm/0.5 «mu»m, He, 40. C @ 8. min, 3. K/min; Tend: 230. C
CapillaryDB-Wax1445.Akiyama, Murakami, et al., 200360. m/0.32 mm/0.25 «mu»m, He, 6. K/min, 230. C @ 20. min; Tstart: 40. C
CapillaryHP-Wax1475.Andueza, Maeztu, et al., 200360. m/0.25 mm/0.5 «mu»m, He, 40. C @ 6. min, 3. K/min; Tend: 199. C
CapillaryHP-Wax1475.Andueza, de Peña, et al., 200360. m/0.25 mm/0.5 «mu»m, He, 40. C @ 6. min, 3. K/min; Tend: 190. C
CapillaryDB-Wax1470.Kumazawa and Masuda, 200230. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1470.Kumazawa and Masuda, 200260. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-FFAP1444.Sanz, Czerny, et al., 200230. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 6. K/min, 230. C @ 5. min
CapillaryDB-Wax1467.Cadwallader and Heo, 200130. m/0.53 mm/1. «mu»m, He, 40. C @ 5. min, 6. K/min, 225. C @ 30. min
CapillaryHP-Wax1475.Maeztu, Sanz, et al., 200160. m/0.25 mm/0.5 «mu»m, He, 40. C @ 6. min, 3. K/min; Tend: 190. C
CapillaryDB-Wax1469.Kim, Baek, et al., 200030. m/0.32 mm/0.25 «mu»m, 40. C @ 5. min, 8. K/min, 280. C @ 30. min
CapillaryDB-Wax1455.Buttery, Orts, et al., 199930. C @ 4. min, 2. K/min, 170. C @ 60. min; Column length: 60. m; Column diameter: 0.32 mm
CapillaryDB-Wax1476.Kumazawa and Masuda, 199930. m/0.53 mm/1. «mu»m, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1475.Kumazawa and Masuda, 199960. m/0.25 mm/0.25 «mu»m, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1455.Buttery and Ling, 199830. C @ 4. min, 2. K/min, 170. C @ 30. min; Column length: 60. m; Column diameter: 0.25 mm
CapillaryCP-Wax 52CB1465.Chyau, Lin, et al., 199750. m/0.32 mm/0.25 «mu»m, He, 50. C @ 5. min, 1.5 K/min, 210. C @ 10. min
CapillaryDB-Wax1460.Umano, Hagi, et al., 1995He, 40. C @ 2. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 200. C
CapillaryFFAP1450.Vernin, Metzger, et al., 1988He, 60. C @ 5. min, 2. K/min; Column length: 50. m; Column diameter: 0.28 mm; Tend: 240. C
CapillaryFFAP1450.Vernin, Metzger, et al., 1988He, 60. C @ 5. min, 2. K/min; Column length: 50. m; Column diameter: 0.28 mm; Tend: 240. C
CapillaryDB-Wax1455.Wong and Bernhard, 1988He, 70. C @ 8. min, 2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 160. C
CapillaryCarbowax 20M1446.Wu, Liou, et al., 1987Hydrogen, 1. K/min, 200. C @ 35. min; Column length: 50. m; Column diameter: 0.20 mm; Tstart: 50. C
PackedCarbowax1434.Schieberle and Grosch, 1983He, Chromosorb G AW DMCS, 4. K/min; Column length: 3. m; Tstart: 60. C; Tend: 180. C
CapillaryCarbowax 20M1447.Liardon and Ledermann, 1980H2, 2. K/min; Column length: 39. m; Column diameter: 0.30 mm; Tstart: 60. C; Tend: 220. C
CapillaryCarbowax 20M1460.Shibamoto and Russell, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillaryCarbowax 20M1460.Shibamoto and Russell, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryEC-10001440.Delabre and Bendall, 9999Program: not specified
CapillaryDB-Wax1458.Rochat, Egger, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryFFAP1430.Frauendorfer and Schieberle, 2008Helium; Program: not specified
CapillaryDB-FFAP1451.Lasekan, Buettner, et al., 200730. m/0.32 mm/0.25 «mu»m; Program: 35C(2min) => 40C/min => 50C(2min) => 6C/min => 180C => 10C/min => 230C(10min)
CapillaryFFAP1463.Bailly, Jerkovic, et al., 200625. m/0.32 mm/0.3 «mu»m, He; Program: 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C
CapillaryTC-Wax1474.Kraft and Switt, 2005Program: not specified
CapillaryFFAP1459.Didzbalis, Ritter, et al., 200430. m/0.32 mm/0.25 «mu»m, He; Program: 35C(1min) => 60C/min => 60C => 6C/min => 230C
CapillaryInnowax1472.Ito and Mori, 200430. m/0.25 mm/0.50 «mu»m, Helium; Program: 40 0C (2 min) 10 0C/min -> 100 0C 3 0C/min -> 160 0C 5 0C/min -> 260 0C (10 min)
CapillaryTC-Wax1474.Tachihara, Ishizaki, et al., 2004Program: not specified
CapillarySupelcowax-101455.Baek and Cadwallader, 200360. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryFFAP1451.Bel Rhild, Fleury, et al., 200230. m/0.32 mm/0.25 «mu»m, Helium; Program: 50 0C (2 min) 6 0C/min -> 180 0C 10 0C/min -> 180 0C (10 min)
CapillaryFFAP1453.Bel Rhild, Fleury, et al., 200230. m/0.32 mm/0.25 «mu»m, Helium; Program: 50 0C (2 min) 6 0C/min -> 180 0C 10 0C/min -> 180 0C (10 min)
CapillaryFFAP1451.Bel Rhild, Fleury, et al., 2002, 230. m/0.32 mm/0.25 «mu»m, Helium; Program: 50 0C (2 min) 6 oC/min -> 180 0C 10 0C/min -> 240 0C (10 min)
CapillaryDB-FFAP1450.Mayer and Grosch, 200130. m/0.32 mm/0.25 «mu»m, He; Program: 35 0C (2 min) 40 K/min -> 60 0C (1 min) 6 K/min -> 240 0C
CapillaryFFAP1432.Matsui, Guth, et al., 199830. m/0.32 mm/0.25 «mu»m, He; Program: 35C(1min) => 40C/min => 60C (1min) => 6C/min => 230C
CapillaryFFAP1439.Zehentbauer and Grosch, 199825. m/0.32 mm/0.25 «mu»m, He; Program: 35C(2min) => 40C/min => 60C(2min) => 6C/min => 230C
CapillaryFFAP1461.Schermann and Schieberle, 199730. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillaryFFAP1461.Schermann and Schieberle, 199730. m/0.32 mm/0.25 «mu»m, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillarySupelcowax-101447.Schieberle and Grosch, 1994He; Column length: 30. m; Column diameter: 0.32 mm; Program: 35C => 40C/min => 60C(2min) => 4C/min => 240C
CapillaryFFAP1443.Guth and Grosch, 1993Program: not specified
CapillaryFFAP1453.Blank, Sen, et al., 1992Program: not specified
CapillaryCarbowax 20M1415.Mihara and Masuda, 1987Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Greenberg, 1981
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Kuo, Zhang, et al., 1989
Kuo, M.-C.; Zhang, Y.; Hartman, T.G.; Rosen, R.T.; Ho, C.-T., Selective purge-and-trap method for the analysis of volatile pyrazines, J. Agric. Food Chem., 1989, 37, 4, 1020-1022, https://doi.org/10.1021/jf00088a045 . [all data]

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Lopez-Galilea I., Fournier N., et al., 2006
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Stephan and Steinhart, 1999
Stephan, A.; Steinhart, H., Identification of character impact odorants of different soybean lecithins, J. Agric. Food Chem., 1999, 47, 7, 2854-2859, https://doi.org/10.1021/jf981387g . [all data]

Shimoda, Nakada, et al., 1997
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Rhlid, Fleury, et al., 2002
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Baek and Cadwallader, 1996
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Wu, Liou, et al., 1987
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Lorenz, Stern, et al., 1983
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Notes

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