Pyrazine, 2-ethyl-3,5-dimethyl-


Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin GEORGE R. WALLER AND BOBBY R. JOHNSON, OKLAHOMA STATE UNIV, USA
NIST MS number 51849

All mass spectra in this site (plus many more) are available from the NIST/EPA/NIH Mass Spectral Library. Please see the following for information about the library and its accompanying search program.


Gas Chromatography

Go To: Top, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-301059.Greenberg, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C
CapillarySE-301062.Greenberg, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-51079.Steinhaus and Schieberle, 200730. m/0.32 mm/0.25 μm, 40. C @ 2. min, 6. K/min, 240. C @ 10. min
CapillaryCP Sil 8 CB1075.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryBPX-51093.Bredie, Mottram, et al., 200250. m/0.32 mm/0.5 μm, 60. C @ 5. min, 4. K/min, 250. C @ 20. min
CapillaryBPX-51088.Ames, Guy, et al., 200150. m/0.32 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51092.Ames, Guy, et al., 200150. m/0.32 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min, 250. C @ 10. min
CapillaryDB-5MS1074.Baek, Kim, et al., 200160. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min, 200. C @ 60. min
CapillaryBPX-51084.Oruna-Concha, Duckham, et al., 200150. m/0.32 mm/0.25 μm, He, 35. C @ 3. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51082.Oruna-Concha, Duckham, et al., 200150. m/0.32 mm/0.25 μm, He, 35. C @ 3. min, 4. K/min, 250. C @ 10. min
CapillaryDB-11070.Wu, Wang, et al., 200060. m/0.25 mm/1. μm, N2, 5. K/min, 200. C @ 30. min; Tstart: 30. C
CapillaryDB-11068.Wu, Wang, et al., 200060. m/0.25 mm/1. μm, N2, 5. K/min, 200. C @ 30. min; Tstart: 30. C
CapillaryBPX-51086.Hill, Isaacs, et al., 199950. m/0.325 mm/0.5 μm, He, 20. C @ 2. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51087.Hill, Isaacs, et al., 199950. m/0.325 mm/0.5 μm, He, 20. C @ 2. min, 4. K/min, 250. C @ 10. min
CapillaryBPX-51085.Ames, Defaye, et al., 199750. m/0.325 mm/0.5 μm, He, 50. C @ 2. min, 4. K/min, 250. C @ 10. min
CapillaryDB-11064.Specht and Baltes, 199460. m/0.25 mm/0.25 μm, 35. C @ 10. min, 2. K/min, 280. C @ 10. min
CapillaryHP-11064.Zhang, Dorjpalam, et al., 199250. m/0.32 mm/1.5 μm, 2. K/min, 220. C @ 30. min; Tstart: 40. C
CapillarySE-301060.Misharina, Golovnya, et al., 199150. m/0.32 mm/0.25 μm, 4. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-11067.Zhang and Ho, 199160. m/0.25 mm/0.25 μm, He, 2. K/min, 220. C @ 10. min; Tstart: 40. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillarySPB-51081.Majcher and Jelen, 200730. m/0.53 mm/1.5 μm; Program: 40C(1min) => 6C/min => 180C => 20C/min => 280C
CapillarySE-541084.Frauendorfer and Schieberle, 200625. m/0.32 mm/0.25 μm, He; Program: 40C(1min) => 40C/min => 60C(1min) => 4C/min => 140C => 20C/min => 240C(5min)
CapillaryZB-51059.Lu, Hao, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 50C(1min) => 3C/min => 209C => 20C/min => 280C
CapillaryDB-51081.Majcher and Jelén, 200530. m/0.25 mm/0.25 μm, He; Program: 40C(1min) => 6C/min => 180C => 20C/min => 280C
CapillaryCP Sil 8 CB1088.Duckham, Dodson, et al., 200160. m/0.25 mm/0.25 μm; Program: 0C => rapidly => 40C(8min) => 4C/min => 250C(10min)
CapillaryDB-51082.Rychlik and Bosset, 200130. m/0.32 mm/0.25 μm, He; Program: 35C(2min) => 40C/min => 60C (2min) => 4C/min => 240C
CapillaryDB-51098.Parker, Hassell, et al., 200050. m/0.32 mm/0.5 μm, He; Program: oC(5min) => 60C/min => 60C (5min) => 4C/min => 250C
CapillarySE-541083.Tairu, Hofmann, et al., 200030. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C (5min) => 10C/min => 230C (5min)
CapillaryBPX-51087.Bredie, Mottram, et al., 199850. m/0.32 mm/0.5 μm, He; Program: OC (5min) => 60C/min => 60C(5min) => 4C/min => 250C
CapillarySE-541085.Fickert and Schieberle, 199825. m/0.32 mm/0.5 μm, He; Program: 35C (2min) => 4C/min => 150C => 10C/min => 240C
CapillarySE-541083.Hofmann and Schieberle, 199830. m/0.32 mm/0.25 μm; Program: 35C(2min) => 40C/min => 50C(5min) => 6C/min => 230C(15min)
CapillarySE-541079.Münch, Hofmann, et al., 199730. m/0.32 mm/0.25 μm, He; Program: 40C (2min) => 40C/min => 50C (2min) => 240C (10min)
CapillaryBPX-51088.Owens J.D., Allagheny N., et al., 199750. m/0.32 mm/0.5 μm, He; Program: OC => 60C/min => 60C(5min) => 4C/min => 250C(20min)
CapillaryDB-11068.Kuo, Zhang, et al., 198960. m/0.32 mm/0.25 μm, He; Program: -40C => 40C/min => 40C => 2C/min => 260C

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax1464.Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 200730. m/0.25 mm/0.5 μm, He, 40. C @ 5. min, 4. K/min, 250. C @ 15. min
CapillaryDB-Wax1464.Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 200730. m/0.25 mm/0.5 μm, He, 40. C @ 5. min, 4. K/min, 250. C @ 15. min
CapillaryFFAP1435.Steinhaus and Schieberle, 200730. m/0.32 mm/0.25 μm, 40. C @ 2. min, 6. K/min, 240. C @ 10. min
CapillaryDB-Wax1455.Lopez-Galilea I., Fournier N., et al., 200630. m/0.32 mm/0.5 μm, He, 5. K/min, 240. C @ 10. min; Tstart: 40. C
CapillaryDB-Wax1455.Lopez-Galilea I., Fournier N., et al., 200630. m/0.32 mm/0.5 μm, He, 5. K/min, 240. C @ 10. min; Tstart: 40. C
CapillaryCP-Wax 52CB1449.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCP-Wax 52CB1456.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryFFAP1494.Stephan and Steinhart, 199960. m/0.25 mm/0.5 μm, 50. C @ 3. min, 5. K/min, 230. C @ 15. min
CapillaryPEG-20M1462.Shimoda, Nakada, et al., 199760. m/0.25 mm/0.25 μm, He, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillaryDB-Wax1462.Shimoda, Shiratsuchi, et al., 199660. m/0.25 mm/0.25 μm, He, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillarySupelcowax-101434.Cadwallader, Tan, et al., 199560. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 200. C @ 30. min
CapillarySupelcowax-101446.Tanchotikul and Hsieh, 198960. m/0.25 mm/0.25 μm, 40. C @ 5. min, 2. K/min, 175. C @ 20. min
CapillarySupelcowax-101447.Tanchotikul and Hsieh, 198960. m/0.25 mm/0.25 μm, 40. C @ 5. min, 2. K/min, 175. C @ 20. min
CapillaryCP-WAX 57CB1466.Salter L.J., Mottram D.S., et al., 198860. C @ 5. min, 4. K/min; Column length: 50. m; Column diameter: 0.32 mm; Tend: 200. C
CapillaryCP-WAX 57CB1466.Whitfield, Mottram, et al., 1988He, 60. C @ 5. min, 4. K/min, 200. C @ 10. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCP-WAX 57CB1466.Whitfield, Mottram, et al., 1988He, 60. C @ 5. min, 4. K/min, 200. C @ 10. min; Column length: 50. m; Column diameter: 0.32 mm

Van Den Dool and Kratz RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillarySupelcowax-101443.Bianchi, Careri, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C(8min) => 4C/min => 60C => 6C/min => 160C => 20C/min => 200C(1min)
CapillarySupelcowax-101444.Bianchi, Careri, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C(8min) => 4C/min => 60C => 6C/min => 160C => 20C/min => 200C(1min)
CapillarySupelcowax-101437.Majcher and Jelen, 200730. m/0.25 mm/0.25 μm; Program: 40C(2min) => 40C/min => 60C(2min) => 5C/min => 240C
CapillaryFFAP1446.Frauendorfer and Schieberle, 200625. m/0.32 mm/0.2 μm, He; Program: 40C(1min) => 40C/min => 60C(1min) => 6C/min => 180C => 15C/min => 240C
CapillarySupelcowax-101437.Majcher and Jelén, 200530. m/0.25 mm/0.25 μm, He; Program: 40C(2min) => 40C/min => 60(2min)C => 5C/min => 240C
CapillaryCP-Wax 52CB1454.Alasalvar, Shahidi, et al., 200360. m/0.25 mm/0.25 μm, He; Program: 40C => 5C/min => 60C => 2.5C/min => 155C
CapillaryFFAP1453.Rhlid, Fleury, et al., 200230. m/0.32 mm/0.25 μm; Program: 50C (2min) => 6C/min => 180C => 10C/min => 240C(10min)
CapillaryFFAP1451.Rhlid, Fleury, et al., 200230. m/0.32 mm/0.25 μm; Program: 50C (2min) => 6C/min => 180C => 10C/min => 240C(10min)
CapillaryFFAP1455.Tairu, Hofmann, et al., 200030. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C (5min) => 10C/min => 230C (5min)
CapillaryFFAP1454.Fickert and Schieberle, 199825. m/0.32 mm/0.5 μm, He; Program: 35C (2min) => 40C/min => 60C => 6C/min => 230C (10min)
CapillaryFFAP1461.Hofmann and Schieberle, 199830. m/0.32 mm/0.25 μm; Program: 35C(2min) => 40C/min => 60C(5min) => 6C/min => 230C(15min)
CapillaryFFAP1440.Münch, Hofmann, et al., 199730. m/0.32 mm/0.25 μm, He; Program: 40C (2min) => 40C/min => 60C (2min) => 240C (10min)
CapillarySupelcowax-101455.Baek and Cadwallader, 199660. m/0.25 mm/0.25 μm; Program: 40C => (6C/min) => 80C(6min) => (15C/min) => 200C(10min)
CapillaryDB-Wax1455.Amrani-Hemaimi, Cerny, et al., 199530. m/0.32 mm/0.25 μm, He; Program: 35C(2min) => 6C/min => 150C => 30C/min => 240C(1min)

Normal alkane RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-5 MS1091.Chen, Song, et al., 200930. m/0.32 mm/0.25 μm, Helium, 40. C @ 2. min, 6. K/min, 230. C @ 20. min
CapillaryDB-5 MS1092.Chen, Song, et al., 200930. m/0.32 mm/0.25 μm, Helium, 40. C @ 2. min, 6. K/min, 250. C @ 20. min
CapillarySLB-5MS1094.Risticevic, Carasek, et al., 200810. m/0.18 mm/0.18 μm, Helium, 40. C @ 1.5 min, 10. K/min; Tend: 295. C
CapillaryDB-51090.Fadel, Mageed, et al., 2006He, 60. C @ 5. min, 4. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tend: 250. C
CapillaryDB-5 MS1095.Schirack, Drake, et al., 200630. m/0.25 mm/0.25 μm, 40. C @ 3. min, 8. K/min, 200. C @ 20. min
CapillaryHP-51078.6Leffingwell and Alford, 200560. m/0.32 mm/0.25 μm, He, 30. C @ 2. min, 2. K/min, 260. C @ 28. min
CapillaryMDN-51085.van Loon, Linssen, et al., 200560. m/0.25 mm/0.25 μm, He, 40. C @ 4. min, 4. K/min, 270. C @ 5. min
CapillaryMDN-51090.van Loon, Linssen, et al., 200560. m/0.25 mm/0.25 μm, He, 40. C @ 4. min, 4. K/min, 270. C @ 5. min
CapillaryDB-51080.Sanz, Czerny, et al., 200230. m/0.32 mm/0.25 μm, He, 40. C @ 2. min, 6. K/min, 230. C @ 5. min
CapillaryDB-5MS1084.Cadwallader and Heo, 200130. m/0.53 mm/1.5 μm, He, 40. C @ 5. min, 6. K/min, 225. C @ 30. min
CapillaryDB-5MS1095.Welty, Marshall, et al., 2001He, 40. C @ 5. min, 5. K/min, 220. C @ 5. min; Column length: 50. m; Column diameter: 0.25 mm
CapillaryHP-51085.Boylston and Viniyard, 199850. m/0.32 mm/0.52 μm, 35. C @ 15. min, 2. K/min, 250. C @ 45. min
CapillaryOV-1011045.Deibler, Acree, et al., 199810. m/0.25 mm/0.52 μm, Helium, 35. C @ 3. min, 6. K/min; Tend: 225. C
CapillaryDB-11054.Buttery, Ling, et al., 199730. C @ 25. min, 4. K/min, 200. C @ 20. min; Column length: 60. m; Column diameter: 0.25 mm
CapillaryUltra 11058.Farkas, Sádecká, et al., 199750. m/0.20 mm/0.33 μm, Helium, 30. C @ 1. min, 1.7 K/min; Tend: 250. C
CapillaryDB-11072.Lu, Yu, et al., 199760. m/0.32 mm/1. μm, He, 40. C @ 2. min, 2. K/min, 280. C @ 40. min
CapillaryDB-11065.Yu and Ho, 199560. m/0.25 mm/1. μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 60. min
CapillaryDB-11072.Yu, Wu, et al., 199460. m/0.25 mm/1.0 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 60. min
CapillaryOV-1011064.Mihara and Masuda, 1987N2, 2. K/min; Column length: 50. m; Column diameter: 0.22 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-11056.Wu, Liou, et al., 1987Hydrogen, 1. K/min, 200. C @ 35. min; Column length: 50. m; Column diameter: 0.20 mm; Tstart: 50. C
CapillaryMethyl Silicone1056.Lorenz, Stern, et al., 19834. K/min, 200. C @ 15. min; Column length: 25. m; Column diameter: 0.2 mm; Tstart: 50. C
CapillaryMethyl Silicone1059.Lorenz, Stern, et al., 19834. K/min, 200. C @ 15. min; Column length: 25. m; Column diameter: 0.2 mm; Tstart: 50. C
CapillarySE-301062.Heydanek and McGorrin, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-51077.Yu and Zhang, 201030. m/0.25 mm/0.25 μm; Program: 40 0C (5 min) 5 0C/min -> 260 0C 15 0C/min -> 280 0C (1 min)
CapillarySE-541084.Frauendorfer and Schieberle, 2008Helium; Program: not specified
CapillarySLB-5MS1083.Risticevic, Carasek, et al., 200810. m/0.18 mm/0.18 μm, Helium; Program: not specified
CapillaryHP-5 MS1088.Wan Aida, Ho, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2 min) 20 0C/min -> 80 0C (1 min) 20 0C -> 100 0C (1 min) 30 0C/min -> 230 0C (2 min)
CapillaryHP-51077.Characterization of Pyrazines in Some Chinese Liquors and Their Approximate Concentrations, 200730. m/0.25 mm/0.25 μm, He; Program: 50C(2min) => 2C/min => 140C => 10C/min => 280C (10min)
CapillaryHP-5MS1088.Ho, Wan Aida, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 50C(2min) => 20C/min => 80C (1min) => 20C/min => 100C(1min) => 30C/min => 230C(3min)
CapillarySE-541083.Lasekan, Buettner, et al., 200730. m/0.32 mm/0.25 μm; Program: 35C(2min) => 40C/min => 60C(2min) => 6C/min => 180C => 10C/min => 230C(10min)
CapillaryCP Sil 5 CB1058.Bailly, Jerkovic, et al., 200650. m/0.32 mm/1.2 μm, He; Program: 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C
CapillaryHP-11047.Carpino, Mallia, et al., 200412. m/0.32 mm/0.52 μm; Program: 35C(3min) => 6C/min => 190C => 30C/min => 225C
CapillaryCP Sil 5 CB1056.Counet, Ouwerx, et al., 200450. m/0.32 mm/1.2 μm; Program: 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)
CapillaryDB-51062.Bücking and Steinhart, 200230. m/0.53 mm/1.5 μm; Program: -5C(1min) => 4C/min => 50C => 6C/min => 120C => 8C/min => 250C(2min)
CapillaryCP Sil 5 CB1057.Counet, Callemien, et al., 200250. m/0.32 mm/1.2 μm; Program: 36C => 20C/min => 85C => 1C/min => 145C=3C/min => 250C(30min)
CapillaryCP Sil 8 CB1087.Duckham, Dodson, et al., 200160. m/0.25 mm/0.25 μm; Program: not specified
CapillaryCP Sil 8 CB1093.Duckham, Dodson, et al., 200160. m/0.25 mm/0.25 μm; Program: not specified
CapillaryRTX-51089.Masanetz, Guth, et al., 1998Program: not specified
CapillaryDB-51082.Matsui, Guth, et al., 199830. m/0.32 mm/0.25 μm, He; Program: 35C(1min) => 40C/min => 60C (1min) => 6C/min => 230C
CapillarySE-541086.Zehentbauer and Grosch, 199825. m/0.32 mm/0.25 μm, He; Program: 35C(2min) => 50C/min => 60C(2min) => 4C/min => 230C
CapillarySE-541083.Schermann and Schieberle, 199730. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillarySE-541083.Schermann and Schieberle, 199730. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillarySE-541083.Schermann and Schieberle, 199730. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillaryDB-51083.Schieberle, 1996Column length: 30. m; Column diameter: 0.32 mm; Program: not specified
CapillaryDB-51083.Schieberle and Grosch, 1994He; Column length: 30. m; Column diameter: 0.32 mm; Program: 35C => 40C/min => 50C(2min) => 4C/min => 240C
CapillarySE-541082.Guth and Grosch, 1993Program: not specified
CapillarySE-541083.Blank, Sen, et al., 1992Program: not specified
CapillaryDB-11060.Kawai, Ishida, et al., 199160. m/0.25 mm/0.25 μm; Program: not specified
CapillaryDB-11061.Kawai, Ishida, et al., 199160. m/0.25 mm/0.25 μm; Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1440.Puvipirom and Chaisei, 201215. m/0.32 mm/0.50 μm, Helium, 3. K/min; Tstart: 40. C; Tend: 250. C
CapillaryDB-Wax1470.Onishi, Inoue, et al., 201160. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 3. K/min, 220. C @ 20. min
CapillaryDB-Wax1464.Kumazawa, Sakai, et al., 201030. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1477.Rochat, Egger, et al., 200930. m/0.25 mm/0.25 μm, Helium, 60. C @ 3. min, 8. K/min, 200. C @ 9.5 min
CapillaryDB-Wax1447.Characterization of Pyrazines in Some Chinese Liquors and Their Approximate Concentrations, 200730. m/0.25 mm/0.25 μm, He, 4. K/min, 230. C @ 15. min; Tstart: 50. C
CapillaryDB-Wax1443.Schirack, Drake, et al., 200630. m/0.25 mm/0.25 μm, 40. C @ 3. min, 8. K/min, 200. C @ 20. min
CapillaryTC-Wax1474.Ishizaki, Tachihara, et al., 200560. m/0.25 mm/0.25 μm, N2, 3. K/min, 220. C @ 40. min; Tstart: 70. C
CapillaryDB-Wax1470.Kumazawa, Kubota, et al., 200530. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryTC-Wax1475.Ishikawa, Ito, et al., 200460. m/0.25 mm/0.5 μm, He, 40. C @ 8. min, 3. K/min; Tend: 230. C
CapillaryDB-Wax1445.Akiyama, Murakami, et al., 200360. m/0.32 mm/0.25 μm, He, 6. K/min, 230. C @ 20. min; Tstart: 40. C
CapillaryHP-Wax1475.Andueza, Maeztu, et al., 200360. m/0.25 mm/0.5 μm, He, 40. C @ 6. min, 3. K/min; Tend: 199. C
CapillaryHP-Wax1475.Andueza, de Peña, et al., 200360. m/0.25 mm/0.5 μm, He, 40. C @ 6. min, 3. K/min; Tend: 190. C
CapillaryDB-Wax1470.Kumazawa and Masuda, 200230. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1470.Kumazawa and Masuda, 200260. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-FFAP1444.Sanz, Czerny, et al., 200230. m/0.32 mm/0.25 μm, He, 40. C @ 2. min, 6. K/min, 230. C @ 5. min
CapillaryDB-Wax1467.Cadwallader and Heo, 200130. m/0.53 mm/1. μm, He, 40. C @ 5. min, 6. K/min, 225. C @ 30. min
CapillaryHP-Wax1475.Maeztu, Sanz, et al., 200160. m/0.25 mm/0.5 μm, He, 40. C @ 6. min, 3. K/min; Tend: 190. C
CapillaryDB-Wax1469.Kim, Baek, et al., 200030. m/0.32 mm/0.25 μm, 40. C @ 5. min, 8. K/min, 280. C @ 30. min
CapillaryDB-Wax1455.Buttery, Orts, et al., 199930. C @ 4. min, 2. K/min, 170. C @ 60. min; Column length: 60. m; Column diameter: 0.32 mm
CapillaryDB-Wax1476.Kumazawa and Masuda, 199930. m/0.53 mm/1. μm, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1475.Kumazawa and Masuda, 199960. m/0.25 mm/0.25 μm, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax1455.Buttery and Ling, 199830. C @ 4. min, 2. K/min, 170. C @ 30. min; Column length: 60. m; Column diameter: 0.25 mm
CapillaryCP-Wax 52CB1465.Chyau, Lin, et al., 199750. m/0.32 mm/0.25 μm, He, 50. C @ 5. min, 1.5 K/min, 210. C @ 10. min
CapillaryDB-Wax1460.Umano, Hagi, et al., 1995He, 40. C @ 2. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 200. C
CapillaryFFAP1450.Vernin, Metzger, et al., 1988He, 60. C @ 5. min, 2. K/min; Column length: 50. m; Column diameter: 0.28 mm; Tend: 240. C
CapillaryFFAP1450.Vernin, Metzger, et al., 1988He, 60. C @ 5. min, 2. K/min; Column length: 50. m; Column diameter: 0.28 mm; Tend: 240. C
CapillaryDB-Wax1455.Wong and Bernhard, 1988He, 70. C @ 8. min, 2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 160. C
CapillaryCarbowax 20M1446.Wu, Liou, et al., 1987Hydrogen, 1. K/min, 200. C @ 35. min; Column length: 50. m; Column diameter: 0.20 mm; Tstart: 50. C
PackedCarbowax1434.Schieberle and Grosch, 1983He, Chromosorb G AW DMCS, 4. K/min; Column length: 3. m; Tstart: 60. C; Tend: 180. C
CapillaryCarbowax 20M1447.Liardon and Ledermann, 1980H2, 2. K/min; Column length: 39. m; Column diameter: 0.30 mm; Tstart: 60. C; Tend: 220. C
CapillaryCarbowax 20M1460.Shibamoto and Russell, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillaryCarbowax 20M1460.Shibamoto and Russell, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryEC-10001440.Delabre and Bendall, 9999Program: not specified
CapillaryDB-Wax1458.Rochat, Egger, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryFFAP1430.Frauendorfer and Schieberle, 2008Helium; Program: not specified
CapillaryDB-FFAP1451.Lasekan, Buettner, et al., 200730. m/0.32 mm/0.25 μm; Program: 35C(2min) => 40C/min => 50C(2min) => 6C/min => 180C => 10C/min => 230C(10min)
CapillaryFFAP1463.Bailly, Jerkovic, et al., 200625. m/0.32 mm/0.3 μm, He; Program: 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C
CapillaryTC-Wax1474.Kraft and Switt, 2005Program: not specified
CapillaryFFAP1459.Didzbalis, Ritter, et al., 200430. m/0.32 mm/0.25 μm, He; Program: 35C(1min) => 60C/min => 60C => 6C/min => 230C
CapillaryInnowax1472.Ito and Mori, 200430. m/0.25 mm/0.50 μm, Helium; Program: 40 0C (2 min) 10 0C/min -> 100 0C 3 0C/min -> 160 0C 5 0C/min -> 260 0C (10 min)
CapillaryTC-Wax1474.Tachihara, Ishizaki, et al., 2004Program: not specified
CapillarySupelcowax-101455.Baek and Cadwallader, 200360. m/0.25 mm/0.25 μm; Program: not specified
CapillaryFFAP1451.Bel Rhild, Fleury, et al., 200230. m/0.32 mm/0.25 μm, Helium; Program: 50 0C (2 min) 6 0C/min -> 180 0C 10 0C/min -> 180 0C (10 min)
CapillaryFFAP1453.Bel Rhild, Fleury, et al., 200230. m/0.32 mm/0.25 μm, Helium; Program: 50 0C (2 min) 6 0C/min -> 180 0C 10 0C/min -> 180 0C (10 min)
CapillaryFFAP1451.Bel Rhild, Fleury, et al., 2002, 230. m/0.32 mm/0.25 μm, Helium; Program: 50 0C (2 min) 6 oC/min -> 180 0C 10 0C/min -> 240 0C (10 min)
CapillaryDB-FFAP1450.Mayer and Grosch, 200130. m/0.32 mm/0.25 μm, He; Program: 35 0C (2 min) 40 K/min -> 60 0C (1 min) 6 K/min -> 240 0C
CapillaryFFAP1432.Matsui, Guth, et al., 199830. m/0.32 mm/0.25 μm, He; Program: 35C(1min) => 40C/min => 60C (1min) => 6C/min => 230C
CapillaryFFAP1439.Zehentbauer and Grosch, 199825. m/0.32 mm/0.25 μm, He; Program: 35C(2min) => 40C/min => 60C(2min) => 6C/min => 230C
CapillaryFFAP1461.Schermann and Schieberle, 199730. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillaryFFAP1461.Schermann and Schieberle, 199730. m/0.32 mm/0.25 μm, He; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 240C
CapillarySupelcowax-101447.Schieberle and Grosch, 1994He; Column length: 30. m; Column diameter: 0.32 mm; Program: 35C => 40C/min => 60C(2min) => 4C/min => 240C
CapillaryFFAP1443.Guth and Grosch, 1993Program: not specified
CapillaryFFAP1453.Blank, Sen, et al., 1992Program: not specified
CapillaryCarbowax 20M1415.Mihara and Masuda, 1987Program: not specified

References

Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Greenberg, 1981
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Ames, Guy, et al., 2001
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Baek, Kim, et al., 2001
Baek, H.H.; Kim, C.J.; Ahn, B.H.; Nam, H.S.; Cadwallader, K.R., Aroma extract dilution analysis of a beeflike process flavor from extruded enzyme-hydrolyzed soybean protein, J. Agric. Food Chem., 2001, 49, 2, 790-793, https://doi.org/10.1021/jf000609j . [all data]

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Rychlik and Bosset, 2001
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Parker, Hassell, et al., 2000
Parker, J.K.; Hassell, G.M.E.; Mottram, D.S.; Guy, R.C.E., Sensory and instrumental analyses of volatiles generated during the extrusion cooking of oat flours, J. Agric. Food Chem., 2000, 48, 8, 3497-3506, https://doi.org/10.1021/jf991302r . [all data]

Tairu, Hofmann, et al., 2000
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Bredie, Mottram, et al., 1998
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Fickert and Schieberle, 1998
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Hofmann and Schieberle, 1998
Hofmann, T.; Schieberle, P., Identification of key aroma compounds generated from cysteine and carbohydrates under roasting conditions, Z. Lebensm. Unters. Forsch. A, 1998, 207, 3, 229-236, https://doi.org/10.1007/s002170050324 . [all data]

Münch, Hofmann, et al., 1997
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Owens J.D., Allagheny N., et al., 1997
Owens J.D.; Allagheny N.; Kipping G.; Ames J.M., Formation of volatile compounds during Bacillus subtilis fermentation of soya beans, J. Sci. Food Agric., 1997, 74, 1, 132-140, https://doi.org/10.1002/(SICI)1097-0010(199705)74:1<132::AID-JSFA779>3.0.CO;2-8 . [all data]

Kuo, Zhang, et al., 1989
Kuo, M.-C.; Zhang, Y.; Hartman, T.G.; Rosen, R.T.; Ho, C.-T., Selective purge-and-trap method for the analysis of volatile pyrazines, J. Agric. Food Chem., 1989, 37, 4, 1020-1022, https://doi.org/10.1021/jf00088a045 . [all data]

Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007
Pozo-Bayon M.A.; Ruiz-Rodriguez A.; Pernin K.; Cayot N., Influence of eggs on the aroma composition of a sponge cake and on the aroma release in model studies on flavored sponge cakes, J. Agric. Food Chem., 2007, 55, 4, 1418-1426, https://doi.org/10.1021/jf062203y . [all data]

Lopez-Galilea I., Fournier N., et al., 2006
Lopez-Galilea I.; Fournier N.; Cid C.; Guichard E., Changes in headspace volatile concentrations of coffee brews caused by the roasting process and the brewing procedure, J. Agric. Food Chem., 2006, 54, 22, 8560-8566, https://doi.org/10.1021/jf061178t . [all data]

Stephan and Steinhart, 1999
Stephan, A.; Steinhart, H., Identification of character impact odorants of different soybean lecithins, J. Agric. Food Chem., 1999, 47, 7, 2854-2859, https://doi.org/10.1021/jf981387g . [all data]

Shimoda, Nakada, et al., 1997
Shimoda, M.; Nakada, Y.; Nakashima, M.; Osajima, Y., Quantitative comparison of volatile flavor compounds in deep-roasted and light-roasted sesame seed oil, J. Agric. Food Chem., 1997, 45, 8, 3193-3196, https://doi.org/10.1021/jf970172o . [all data]

Shimoda, Shiratsuchi, et al., 1996
Shimoda, M.; Shiratsuchi, H.; Nakada, Y.; Wu, Y.; Osajima, Y., Identification and sensory characterization of volatile flavor compounds in sesame seed oil, J. Agric. Food Chem., 1996, 44, 12, 3909-3912, https://doi.org/10.1021/jf960115f . [all data]

Cadwallader, Tan, et al., 1995
Cadwallader, K.R.; Tan, Q.; Chen, F.; Meyers, S.P., Evaluation of the aroma of cooked spiny lobster tail meat by aroma extract dilution analysis, J. Agric. Food Chem., 1995, 43, 9, 2432-2437, https://doi.org/10.1021/jf00057a022 . [all data]

Tanchotikul and Hsieh, 1989
Tanchotikul, U.; Hsieh, T.C.-Y., Volatile Flavor Components in Crayfish Waste, J. Food Sci., 1989, 54, 6, 1515-1520, https://doi.org/10.1111/j.1365-2621.1989.tb05149.x . [all data]

Salter L.J., Mottram D.S., et al., 1988
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Whitfield, Mottram, et al., 1988
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Alasalvar, Shahidi, et al., 2003
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Rhlid, Fleury, et al., 2002
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Baek and Cadwallader, 1996
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Leffingwell and Alford, 2005
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van Loon, Linssen, et al., 2005
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Lu, Yu, et al., 1997
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Yu and Ho, 1995
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Mihara and Masuda, 1987
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Wu, Liou, et al., 1987
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Lorenz, Stern, et al., 1983
Lorenz, G.; Stern, D.J.; Flath, R.A.; Haddon, W.F.; Tillin, S.J.; Teranishi, R., Identification of sheep liver volatiles, J. Agric. Food Chem., 1983, 31, 5, 1052-1057, https://doi.org/10.1021/jf00119a033 . [all data]

Heydanek and McGorrin, 1981
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Notes

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