Limonene

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-8(2)10-6-4-9(3)5-7-10/h4,10H,1,5-7H2,2-3H3
IUPAC Standard InChIKey: XMGQYMWWDOXHJM-UHFFFAOYSA-N
CAS Registry Number: 138-86-3
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Species with the same structure:
- Limonene
Stereoisomers:
- D-Limonene
- Cyclohexene, 1-methyl-4-(1-methylethenyl)-, (S)-
Other names: Cyclohexene, 1-methyl-4-(1-methylethenyl)-; p-Mentha-1,8-diene; α-Limonene; Cajeputen; Cajeputene; Cinen; Cinene; Dipenten; Dipentene; Eulimen; Kautschin; Limonen; Nesol; p-Mentha-1,8(9)-diene; δ-1,8-Terpodiene; p-Mentha-1,8-diene, dl-; Acintene DP dipentene; Di-p-mentha-1,8-diene; DL-Limonene; Inactive limonene; 1-Methyl-4-isopropenyl-1-cyclohexene; 1,8(9)-p-Menthadiene; 4-Isopropenyl-1-methyl-1-cyclohexene; Acintene DP; Dipanol; UN 2052; Unitene; 4-Isopropenyl-1-methylcyclohexene; 1,8-p-Menthadiene; 1-Methyl-4-(1-methylethenyl)cyclohexene; 1-Methyl-4-isopropenylcyclohexene; (.+/-.)-Limonene; Achilles dipentene; 1-methyl-4-isopropenylcyclohex-1-ene; 1-methyl-4-(prop-1-en-2-yl)cyclohex-1-ene; Cyclohexene, 1-methyl-4-(1-methylethynyl); Cyclohexene, 1-methyl-4-(1-methylethenyl)-, (.+/-.)-; (.+/-.)-Dipentene; (.+/-.)-α-Limonene; Flavor orange; Goldflush II; NSC 21446; Orange flavor; PC 560; D-Limonene; (+)-limonene; (+)-(4R)-limonene; ( R/ S)-limonene; (R)-(+)-Limonene; (R)-Limonene; (±)-limonene; Limonene [4R-(+), 4S-(-)]; δ-Limonene; 1-Limonene; 1-methyl-4-isopropenylcyclohex-1-ene (limonene); (S)-(-)-Limonene; Limonene+; Dipentene limonene
Information on this page:
Other data available:
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- Gas Phase Kinetics Database
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Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-5 MS	DB-5	HP-1	RTX-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	300.	240.	240.	240.	230.
Heat rate (K/min)	4.	3.	3.	3.	2.
Initial hold (min)	3.
Final hold (min)	15.				5.
I	1028.	1036.	1026.	1025.	1025.
Reference	Bertuzzi, Tirillini, et al., 2013	Pinheiro, de Queiros, et al., 2013	Rodriques, Amorim, et al., 2013	Alizadeh and Shaabani, 2012	Bendiabdellah, El Amine Dib, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	Mega-5	Optima-5 MS	HP-5 MS	HP-5 MS
Column length (m)	60.	25.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	35.	40.	35.
T_end (C)	230.	220.	250.	250.	300.
Heat rate (K/min)	2.	3.	10.	3.	3.
Initial hold (min)		1.	3.	1.	5.
Final hold (min)	5.	5.	5.	3.	15.
I	1025.	1029.	1032.	1032.	1025.
Reference	Bendiabdellah, El Amine Dib, et al., 2012	Dell'Agli, Sanna, et al., 2012	Goeminne, Vandendriessche, et al., 2012	Jian-Yu, Zhu, et al., 2012	Kotowska, Zalikowski, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5 MS	Petrocol DH	Petrocol DH	HP-5	HP-5
Column length (m)	60.	100.	100.	25.	25.
Carrier gas	Helium	Helium	Helium	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.50	0.50	0.52	0.52
T_start (C)	40.	20.	20.	40.	40.
T_end (C)	250.	220.	220.	280.	280.
Heat rate (K/min)	4.	15.	15.	4.	4.
Initial hold (min)	2.	15.	15.
Final hold (min)		30.	30.	10.	10.
I	1030.	1026.	1026.	1024.	1024.
Reference	Srisajjalerwaja, Apichartsrangkoon, et al., 2012	Supelco, 2012	Supelco, 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	HP-5 MS	HP-5	DB-5	DB-5 MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	40.	60.
T_end (C)	230.	250.	240.	250.	270.
Heat rate (K/min)	2.	7.	3.	3.	3.
Initial hold (min)		1.		5.
Final hold (min)	45.	5.		20.
I	1017.	1030.	1029.	1029.	1037.
Reference	Yapi, Boti, et al., 2012	Zouari, Ayadi, et al., 2012	Bertoli, Lepnardi, et al., 2011	Cao, Li, et al., 2011	Cui, Yang, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP-Sil 5 CB	DB-1	DB-5	HP-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	Hydrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	230.	210.	240.	240.	240.
Heat rate (K/min)	3.	5.	3.	3.	3.
Initial hold (min)				2.
Final hold (min)
I	1033.	1032.	1032.	1031.	1031.
Reference	Esseien, Aboaba, et al., 2011	Fathi, Sahari, et al., 2011	Fraternale, Ricci, et al., 2011	Kahriman, Tosun, et al., 2011	Karimi, Farmani, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5 MS	VF-5 MS	SE-30 MS	DB-1	Methylsiloxane + 5 % Ph-groups
Column length (m)	60.	60.	30.	50.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	30.	30.	50.	60.	60.
T_end (C)	260.	260.	250.	250.	230.
Heat rate (K/min)	2.	2.	5.	8.	7.
Initial hold (min)			5.		2.
Final hold (min)	28.	28.	10.		20.
I	1029.	1032.	1032.	1025.	1030.
Reference	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011	Menichini, Tundis, et al., 2011	Misharina T., 2011	Nadim, Malik, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	RTX-5	ZB-5
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	35.	35.	60.	40.
T_end (C)	300.	200.	220.	210.	200.
Heat rate (K/min)	4.	2.	10.	3.	5.
Initial hold (min)	4.		1.		5.
Final hold (min)	5.		15.
I	1032.	1031.	1032.	1025.	1032.
Reference	Osorio, Carriazo, et al., 2011	Pattiram, Lasekan, et al., 2011	Piyachaiseth, Jirapakkul, et al., 2011	Prasad, Moulekhi, et al., 2011	Vazques, Aimar, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	ZB-5 MS	HP-5	DB-5 MS	DB-5 MS
Column length (m)	30.	30.	30.	25.	25.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.252	0.30	0.30
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	50.
T_end (C)	200.	290.	240.	240.	240.
Heat rate (K/min)	5.	5.	3.	3.	3.
Initial hold (min)	5.
Final hold (min)	5.
I	1032.	1032.	1026.	1030.	1030.
Reference	Vazquez, Demmel, et al., 2011	Boix, Victorio, et al., 2010	Cavar, Maksimovic, et al., 2010	Chalchat, Figueredo, et al., 2010	Chalchat, Figueredo, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTx-1	RTX-1	SPB-1	DB-1	DB-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.22	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	30.	50.	50.
T_end (C)	230.	230.	250.	265.	250.
Heat rate (K/min)	2.	2.	4.	2.5	2.
Initial hold (min)			3.	1.
Final hold (min)	35.	30.	10.	20.
I	1020.	1025.	1054.	1024.	1029.
Reference	Dib, Bendahou, et al., 2010	Dib, Djabou, et al., 2010	Escalona-Arranz, Perez-Roses, et al., 2010	Hajimahdipoor, Samadi, et al., 2010	Ho, Wang, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	HP-5 MS	HP-5	DB-5 MS	DB-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	70.	60.	40.	60.
T_end (C)	250.	200.	240.	250.	250.
Heat rate (K/min)	5.	3.	3.	5.	5.
Initial hold (min)	3.	2.	2.	15.
Final hold (min)	2.	18.		15.
I	1021.	1036.	1030.	1034.	1021.
Reference	Hu, Liang, et al., 2010	Jerkovic, Hegic, et al., 2010	Kahriman, Tosun, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Meshkatalsadat, Safaei-Ghomi. J., et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5	SPB-1	HP-5 MS	HP-5 MS
Column length (m)		30.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)		0.25	0.20	0.25	0.25
Phase thickness (μm)		0.25	0.20	0.25	0.25
T_start (C)	60.	40.	70.	60.	60.
T_end (C)	220.	260.	220.	220.	220.
Heat rate (K/min)	5.	4.	3.	5.	5.
Initial hold (min)	10.			10.	10.
Final hold (min)	30.	5.	15.
I	1024.	1030.	1020.	1033.	1034.
Reference	Mishra, Chaudhary, et al., 2010	Miyazawa, Kawauchi, et al., 2010	Neves, Rosa, et al., 2010	Ogunwande, Flamini, et al., 2010	Ogunwande, Flamini, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	HP-5 MS	HP-5	SLB-5 MS
Column length (m)	30.	30.	30.	30.	10.
Carrier gas	Helium	Helium	Helium	Hydrogen	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.10
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.10
T_start (C)	50.	100.	70.	70.	50.
T_end (C)	240.	220.	290.	290.	250.
Heat rate (K/min)	4.	2.	5.	5.	10.
Initial hold (min)	2.
Final hold (min)	10.		10.
I	1030.	1028.	1022.	1033.	1032.
Reference	Pino, Marquez, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Blagojevic, et al., 2010	Radulovic, Dordevic, et al., 2010	Scandinaro, Tranchida, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	DB-5	DB-5 MS	DB-5	DB-1-MS
Column length (m)	10.	30.	30.	30.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.10	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.10	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	40.	30.
T_end (C)	250.	240.	240.	240.	200.
Heat rate (K/min)	10.	3.	3.	3.	2.
Initial hold (min)				1.	4.
Final hold (min)					35.
I	1040.	1032.	1028.	1007.	1018.
Reference	Scandinaro, Tranchida, et al., 2010	Scherer, Wagner, et al., 2010	Silva, Pott, et al., 2010	de Souza, Lopes, et al., 2010	Takeoka, Hobbs, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	DB-1	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas		Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	80.	50.	40.	60.
T_end (C)	230.	240.	220.	250.	240.
Heat rate (K/min)	3.	3.	4.	10.	3.
Initial hold (min)			2.	1.
Final hold (min)		2.	2.	3.
I	1027.	1030.	1018.	1029.	1028.
Reference	Usman, Zubair, et al., 2010	Vahirua-Lechat, Mitermite, et al., 2010	Xu, Tang, et al., 2010	Yang, Zhang, et al., 2010	Alim, Goze, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	SE-54	HP-5 MS	ZB-5
Column length (m)	50.	50.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	60.	60.	50.
T_end (C)	220.	220.	260.	250.	240.
Heat rate (K/min)	2.	2.	2.	2.	3.
Initial hold (min)			5.	8.
Final hold (min)			999.	15.	1.
I	1025.	1028.	1028.	1034.	1011.
Reference	Benites, Moiteiro, et al., 2009	Benites, Moiteiro, et al., 2009	Dayisoylu and Alma, 2009	Farhat, Ginies, et al., 2009	Gardini, Beletti, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	HP-5 MS	DB-5	DB-5 MS
Column length (m)	60.	30.	30.	50.	30.
Carrier gas	Nitrogen	Helium	Hydrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.35	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.32	0.25
T_start (C)	60.	50.	30.	60.	50.
T_end (C)	230.	250.	230.	220.	250.
Heat rate (K/min)	4.	5.	8.	5.	2.
Initial hold (min)		2.	5.	3.	5.
Final hold (min)	40.		10.
I	1033.	1029.	1034.	1031.	1036.
Reference	Gauvin-Bialecki and Marodon, 2009	Ho, Wang, et al., 2009	Karlsson, Birgersson, et al., 2009	Kazemi and Akhavani, 2009	Koba, Sanda, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	VF-5	HP-5MS	VF-1 MS	HP-5
Column length (m)	30.	30.	60.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	70.	60.	70.	60.	60.
T_end (C)	240.	300.	250.	280.	240.
Heat rate (K/min)	5.	10.	3.	4.	3.
Initial hold (min)		2.		5.
Final hold (min)		10.		10.	7.
I	1030.	1039.	1030.	1023.	1028.
Reference	Lawal and Oyedelji, 2009	Li and Zhao, 2009	Males, Plazibat, et al., 2009	Marchesini, Prada, et al., 2009	Maridass, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	BP-1	DB-5 MS	DB-5
Column length (m)	60.	60.	50.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	45.
T_end (C)	230.	230.	220.	330.	250.
Heat rate (K/min)	2.	2.	2.	2.	3.
Initial hold (min)				12.	3.
Final hold (min)	30.	30.	20.	30.	5.
I	1021.	1023.	1020.	1041.	1029.
Reference	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Ottavioli, Bighelli, et al., 2009	Patil, Jayaprakasha, et al., 2009	Porto, Decorti, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	5 % Phenyl methyl siloxane	Mega 5 MS	DB-5	DB-1 MS
Column length (m)	30.	60.	60.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	90.	40.	40.	40.
T_end (C)	250.	225.	240.	230.	250.
Heat rate (K/min)	3.	3.	3.	2.	6.
Initial hold (min)	1.		2.		1.
Final hold (min)	10.	3.			4.
I	1030.	1031.	1021.	1030.	1020.
Reference	Rahimi-Nasrabadi, Gholivand, et al., 2009	Retta, Gattuso, et al., 2009	Romeo, Verzera, et al., 2009	Scrivanti, Anton, et al., 2009	Seo, Kim, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5 MS	SPB-5	DB-5	DB-5 MS
Column length (m)	50.	30.	60.	30.	30.
Carrier gas	Nitrogen	Helium		Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.32	0.25	1.00	0.25	0.25
T_start (C)	60.	50.	40.	40.	40.
T_end (C)	220.	220.	230.	240.	250.
Heat rate (K/min)	5.	3.	3.	3.	4.
Initial hold (min)	3.	2.	5.	1.	2.
Final hold (min)	5.	70.	10.		2.
I	1031.	1028.	1040.	1007.	1035.
Reference	Shafaghat and Sadeghi, 2009	Shimizu, Imayoshi, et al., 2009	Sivadier, Ratel, et al., 2009	de Souza, Lopes, et al., 2009	Su, Wang, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5 MS	HP-5	DB-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	50.	60.	60.
T_end (C)	240.	280.	280.	220.	280.
Heat rate (K/min)	5.	4.	9.	3.	3.
Initial hold (min)			3.
Final hold (min)			3.
I	1030.	1028.	1030.	1028.	1027.
Reference	Wannes, Mhamdi, et al., 2009	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008	Bastos, Ishimoto, et al., 2008	Baziou, Couladis, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	BPX-5	BPX-5	BPX-5	BPX-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Hydrogen	Hydrogen	Hydrogen	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	100.	60.	60.	60.	60.
T_end (C)	999.	999.	999.	999.	999.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)
Final hold (min)
I	1041.	1034.	1035.	1035.	1035.
Reference	Bieri and Marriott, 2008	Bieri and Marriott, 2008	Bieri and Marriott, 2008	Bieri and Marriott, 2008	Bieri and Marriott, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	HP-5	HP-5 MS	SLB-5 MS	ZB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Hydrogen	N2	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	45.
T_end (C)	999.	220.	230.	250.	230.
Heat rate (K/min)	5.	5.	4.	3.	3.
Initial hold (min)		10.	4.	2.
Final hold (min)			10.	10.
I	1037.	1033.	1029.	1029.	1015.
Reference	Bieri and Marriott, 2008	Flamini, Tebano, et al., 2008	Forero, Quijano, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Equity-5 MS	Elite-1	HP-5 MS	BPX-5	RTX-5
Column length (m)	30.	30.	30.	7.5	20.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.10	0.18
Phase thickness (μm)	0.25	0.25	0.25	10.	0.20
T_start (C)	40.	60.	50.	60.	50.
T_end (C)	260.	246.	240.	240.	280.
Heat rate (K/min)	1.5	3.	3.	3.	4.
Initial hold (min)					1.
Final hold (min)
I	1030.	1024.	995.	1034.	1033.
Reference	Mondello, Casilli, et al., 2008	Raj, Baby, et al., 2008	Sarikurkcu, Tepe, et al., 2008	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	OV-1	HP-5	5 % Phenyl methyl siloxane	HP-5 MS
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium		Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	60.	65.	60.	50.	50.
T_end (C)	240.	260.	250.	250.	230.
Heat rate (K/min)	4.	6.	5.	3.	3.
Initial hold (min)	2.		30.		10.
Final hold (min)					10.
I	1032.	1035.	1030.	1030.	1031.
Reference	Verdian-rizi, 2008	Wang, Yi, et al., 2008	Yassa and Akhani, 2008	Zellner, Bicchi, et al., 2008	Adams, Beauchamp, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-5	DB-5MS	HP-5	DB-5
Column length (m)	30.	50.	30.	30.	50.
Carrier gas	Helium	Nitrogen	He	He	He
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.32	0.25		0.25
T_start (C)	60.	60.	60.	70.	50.
T_end (C)	260.	220.	240.	240.	280.
Heat rate (K/min)	2.	5.	3.	5.	5.
Initial hold (min)	5.	3.			2.
Final hold (min)	20.	5.			10.
I	1029.	1025.	1030.	1027.	1032.
Reference	Alma, Ertas, et al., 2007	Amiri, 2007	Andrade, Oliveira, et al., 2007	Asekun, Olusegun, et al., 2007	Baranauskiene R., Bylaite E., et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5MS	HP-5MS	SE-52	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He		He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	300.	280.	280.	220.	240.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)				1.
Final hold (min)				5.
I	1022.	1025.	1025.	1021.	1026.
Reference	Baran, von Reuss, et al., 2007	Basta, Pavlovic, et al., 2007	Basta, Tzakou, et al., 2007	Bicchi, Cordero, et al., 2007	Bos, Woerdenbag, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5 MS	HP-5	DB-5	DB-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	Helium	N2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	40.	70.
T_end (C)	280.	280.	240.	220.	310.
Heat rate (K/min)	3.	4.	5.	3.	3.
Initial hold (min)		5.	1.		5.
Final hold (min)			4.		20.
I	1032.	1027.	1031.	1043.	995.
Reference	Bozin B., Mlmica-Dukic N., et al., 2007	Capetanos, Saroglou, et al., 2007	Cheraif, Ben Jannet, et al., 2007	Chyau, Tsai, et al., 2007	Coelho, Grosso, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	HP-1	DB-5	HP-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.26	0.25
T_start (C)	60.	70.	60.	60.	60.
T_end (C)	240.	200.	290.	240.	250.
Heat rate (K/min)	3.	10.	3.	4.	2.
Initial hold (min)				2.	8.
Final hold (min)				20.	15.
I	1029.	1026.	1026.	1027.	1030.
Reference	Da Silva J.K.R., Sousa P.J.C., et al., 2007	Dongmo, Tatsadjieu, et al., 2007	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Ferhat, Meklati, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	ZP-5	VF-5MS	5 % Phenyl methyl siloxane	DB-5
Column length (m)	30.	60.	30.	60.	60.
Carrier gas	He	He		He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	1.0
T_start (C)	60.	40.	40.	90.	35.
T_end (C)	250.	260.	250.	225.	240.
Heat rate (K/min)	2.	6.	7.	3.	15.
Initial hold (min)	8.	7.			7.
Final hold (min)	15.	1.		15.	10.
I	1028.	1045.	1026.	1016.	1033.
Reference	Ferhat, Tigrine-Kordjani, et al., 2007	Füssel, Dötterl, et al., 2007	Ghiasvand, Setkova, et al., 2007	Gil A., Van Baren C.M., et al., 2007	Gogus, Ozel, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Col-Elite 5MS	HP-1	DBP-5	CP Sil 5 CB	RTX-5 MS
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	Helium	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	30.	60.	40.	50.	45.
T_end (C)	246.	240.	250.	200.	210.
Heat rate (K/min)	3.	2.	3.	5.	3.
Initial hold (min)			1.
Final hold (min)		20.	10.
I	1027.	1016.	1003.	1026.	1028.
Reference	Gudaityte and Venskutonis R.P., 2007	Hachicha, Skanji, et al., 2007	Heravi and Sereshti, 2007	Hnawia, Cabalion, et al., 2007	Hudaib and Aburjai, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	SE-30	HP-5	AT-5
Column length (m)		30.	30.	30.	60.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)		0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	40.	60.
T_end (C)	220.	300.	250.	250.	260.
Heat rate (K/min)	5.	3.	5.	5.	4.
Initial hold (min)			5.	5.
Final hold (min)	6.		10.	10.
I	1024.	1021.	1032.	1028.	1034.
Reference	Kiran, Devi, et al., 2007	Limberger, Scopel, et al., 2007	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Meccia, Rojas, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.32	0.33
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	260.	300.	220.	250.	240.
Heat rate (K/min)	2.5	3.	4.	5.	3.
Initial hold (min)	1.
Final hold (min)	20.
I	1018.	1006.	1031.	1020.	1032.
Reference	Monser-Esfahani, Karamkhani, et al., 2007	Moreno, Lima, et al., 2007	Morteza-Semnani, Saeedi, et al., 2007	Nori-Shargh, Raftari, et al., 2007	Oliveira, Leitão, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	DB-1	HP-5	SPB-1	DB-5
Column length (m)	50.	50.	25.	30.	30.
Carrier gas	Helium	He	Helium	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.2	0.25
Phase thickness (μm)		0.25	0.52	0.2	0.25
T_start (C)	50.	95.	40.	70.	50.
T_end (C)	240.	240.	280.	220.	250.
Heat rate (K/min)	3.	4.	4.	3.	4.
Initial hold (min)
Final hold (min)				15.
I	1031.	1026.	1026.	1020.	1027.
Reference	Ozcan and Chalchat, 2007	Pala-Paul, Brophy, et al., 2007	Pavlovic, Petrovic, et al., 2007	Pinto, Salgueiro, et al., 2007	Pontes, de Olivera, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	BPX-5	BPX-5	BPX-5	5 % Phenyl methyl siloxane
Column length (m)	30.	50.	50.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.22	0.25
Phase thickness (μm)	0.25		1.	1.	1.
T_start (C)	50.	50.	50.	50.	40.
T_end (C)	250.	300.	300.	300.	250.
Heat rate (K/min)	2.	4.	4.	4.	7.
Initial hold (min)		1.	1.	1.	10.
Final hold (min)		10.	10.	10.	5.
I	1026.	1050.	1049.	1050.	1039.
Reference	Raal, Orav, et al., 2007	Rali, Wossa, et al., 2007	Rali, Wossa, et al., 2007, 2	Rali, Wossa, et al., 2007, 2	Ramirez R. and Cava R., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	SPB-1	HP-5	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	Helium	Helium	Hydrogen	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	250.	220.	260.	260.	220.
Heat rate (K/min)	7.	2.	4.	4.	5.
Initial hold (min)	10.	2.			3.
Final hold (min)	5.			20.	3.
I	1039.	1014.	1023.	1019.	1027.
Reference	Ramirez R. and Cava R., 2007	Rao, Nagender, et al., 2007	Ristic, Krivokuca-Dokic, et al., 2007	Rojas, Velasco, et al., 2007	Safaei-Ghomi, Bamoniri, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DBP-5	DB-5	DB-5
Column length (m)	60.	30.	25.	30.	30.
Carrier gas		He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	60.	50.	40.	60.	40.
T_end (C)	250.	240.	250.	320.	210.
Heat rate (K/min)	5.	4.	3.	10.	2.
Initial hold (min)			1.
Final hold (min)			10.	4.	33.
I	1048.	1028.	1003.	1034.	1031.
Reference	Salehi, Asghari, et al., 2007	Sefidkon, Abbasi, et al., 2007	Sereshti and Samadi, 2007	Smelcerovic, Spiteller, et al., 2007	Sylvestre, Longtin, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	Elite-5MS	DB-5
Column length (m)	30.	25.	25.	30.	30.
Carrier gas				He	Helium
Substrate
Column diameter (mm)	0.25	0.2	0.2	0.32	0.25
Phase thickness (μm)	0.25	0.32	0.32	0.5
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	250.	250.	250.	280.	200.
Heat rate (K/min)	2.	5.	5.	4.	2.
Initial hold (min)		1.	1.	5.
Final hold (min)	33.			10.	20.
I	1030.	1030.	1032.	1029.	1020.
Reference	Sylvestre, Pichette, et al., 2007	Tapia, Perich, et al., 2007	Tapia, Perich, et al., 2007	Tava, Pecetti, et al., 2007	Tiwary, Nail, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5 MS	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	200.	280.	280.	250.	240.
Heat rate (K/min)	2.	3.	3.	3.	5.
Initial hold (min)				5.	3.
Final hold (min)	20.			10.	10.
I	1031.	1032.	1029.	1025.	1023.
Reference	Tiwary, Nail, et al., 2007	Tsokou, Georgopoulos, et al., 2007	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Wenguang, Wenlai, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	40.	60.	50.	50.	60.
T_end (C)	250.	250.	280.	280.	300.
Heat rate (K/min)	4.	5.	9.	9.	3.
Initial hold (min)	2.	30.	3.	3.
Final hold (min)	5.		3.	3.
I	1036.	1030.	1030.	1032.	1022.
Reference	Xu, Fan, et al., 2007	Yassa and Akhani, 2007	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Apel, Sobral, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	DB-5	HP-5	HP-1
Column length (m)	30.	25.	30.	60.	50.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25		0.25	0.25	0.2
Phase thickness (μm)	0.25		0.25	0.25	0.33
T_start (C)	40.	80.	50.	60.	60.
T_end (C)	260.	270.	265.	250.	250.
Heat rate (K/min)	4.	10.	2.5	3.	2.
Initial hold (min)	5.		1.
Final hold (min)			20.		20.
I	1029.	1025.	1032.	1026.	1020.
Reference	Askari and Sefidkon, 2006	Ayoub, Al-Azizi, et al., 2006	Bazargani, Almasirad, et al., 2006	Bertrand, Comte, et al., 2006	Berlioz, Cordella, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	BP-1	BP-1	HP-5MS	HP-1
Column length (m)	30.	50.	50.	30.	50.
Carrier gas		He		He	He
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	300.	220.	220.	280.	250.
Heat rate (K/min)	2.	2.	2.	3.	2.
Initial hold (min)					4.
Final hold (min)		20.	20.		30.
I	1030.	1020.	1022.	1032.	1015.
Reference	Biondi, Sari, et al., 2006	Boti, Muselli, et al., 2006	Boti, Yao, et al., 2006	Bozin, Mimicá-Dukic, et al., 2006	Castel, Fernandez, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-1	HP-1	HP-1	SPB-1
Column length (m)	50.	50.	50.	50.	30.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.2	0.2	0.2	0.2	0.20
Phase thickness (μm)	0.33	0.33	0.5	0.33	0.20
T_start (C)	60.	60.	60.	60.	70.
T_end (C)	250.	250.	250.	250.	220.
Heat rate (K/min)	2.	2.	2.	2.	3.
Initial hold (min)	4.	4.		4.
Final hold (min)	30.	30.	120.	30.	15.
I	1021.	1023.	1018.	1018.	1020.
Reference	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006, 2	Castel, Fernandez, et al., 2006, 2	Cavaleiro, Pinto, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Ultra-2	DB-1	DB-5	HP-5	DB-5
Column length (m)	25.	60.	30.	30.	30.
Carrier gas	H2	Nitrogen	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.33		0.25	0.25	0.25
T_start (C)	40.	40.	70.	60.	60.
T_end (C)	280.	200.	230.	246.	230.
Heat rate (K/min)	3.	2.	2.	3.	3.
Initial hold (min)	2.	1.	2.
Final hold (min)	10.	9.	20.		15.
I	1029.	1021.	1039.	1028.	1029.
Reference	Ceva-Antunes, Bizzo, et al., 2006	Chen, Sheu, et al., 2006	Choi, 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	BP-1	BP-1	HP-5MS
Column length (m)	30.	30.	50.	50.	30.
Carrier gas		Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.26	0.22	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	280.	290.	220.	220.	250.
Heat rate (K/min)	4.	3.	2.	2.	2.
Initial hold (min)
Final hold (min)			20.	20.
I	1033.	1026.	1021.	1021.	1031.
Reference	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006	Fanciullino, Tomi, et al., 2006	Fanciullino, Tomi, et al., 2006	Farah, Afifi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-1	BPX-5	DB-5	CP Sil 5 CB
Column length (m)	30.	50.	25.	30.	30.
Carrier gas	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.2	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.13	0.25	0.25
T_start (C)	50.	60.	50.	50.	40.
T_end (C)	300.	250.	230.	250.	220.
Heat rate (K/min)	5.	2.	3.	3.	3.
Initial hold (min)	5.		2.
Final hold (min)	5.	40.		10.	3.
I	1031.	1019.	1020.	1029.	1029.
Reference	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Fons, Rapior, et al., 2006	Havlik, Kokoska, et al., 2006	Hymete, Rohloff, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	CP Sil 5 CB	HP-5MS
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	Helium		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	240.	260.	260.	230.	280.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)					4.
Final hold (min)					10.
I	1031.	1031.	1031.	1024.	1032.
Reference	Ibañez and Usubillaga, 2006	Ibanez and Usubillaga, 2006	Javidnia, Miri, et al., 2006	Kasali, Ekundayo, et al., 2006	Kim, Abd El-Aty, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	BP-1	Methyl Silicone	RTX-1
Column length (m)	30.	30.		25.	30.
Carrier gas	He	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.32
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	50.	60.	90.	60.
T_end (C)	280.	280.	220.	220.	300.
Heat rate (K/min)	5.	5.	5.	7.	4.
Initial hold (min)	4.	4.		2.
Final hold (min)	10.	10.	6.
I	1036.	1032.	1024.	1020.	1023.
Reference	Kim, Abd El-Aty, et al., 2006	Kim, El-Aty, et al., 2006	Kiran, Bhavani, et al., 2006	Kitchlu, Bakshi, et al., 2006	Kula, Izydorczyk, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	BP-1	CP Sil 8 CB	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	60.	50.	30.	30.	30.
Carrier gas		He		N2	N2
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	40.	50.	50.
T_end (C)	230.	220.	250.	300.	200.
Heat rate (K/min)	2.	2.	3.	4.	5.
Initial hold (min)	2.		5.
Final hold (min)	20.	20.	20.
I	1032.	1021.	1032.	1030.	1031.
Reference	Lan Phi N.T., Nishiyama C., et al., 2006	Lesueur, Ban, et al., 2006	Li, Lee, et al., 2006	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	DB-5MS	DB-5	BP-1
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Nitrogen	N2	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.3
Phase thickness (μm)	0.25	0.52	0.25	0.25
T_start (C)	50.	50.	60.	50.	70.
T_end (C)	280.	280.	280.	250.	220.
Heat rate (K/min)	5.	5.	3.	3.	4.
Initial hold (min)				5.	2.
Final hold (min)	5.	5.	30.		10.
I	1033.	1033.	1007.	1029.	1028.
Reference	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Maronigiu, Piras, et al., 2006	Mirza, Navaei, et al., 2006	Moody, Gundidza, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	220.	220.	250.	265.
Heat rate (K/min)	4.	4.	4.	3.	2.5
Initial hold (min)		5.	5.	5.	0.5
Final hold (min)
I	1030.	1031.	1031.	1031.	1018.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Navaei and Mirza, 2006	Nickavar B., Kamalinejad M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	SE-52	DB-5	PE-5
Column length (m)	30.	25.	50.	30.	50.
Carrier gas	He	N2	Helium	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.15		0.25	0.25
T_start (C)	50.	50.	50.	60.	100.
T_end (C)	250.	200.	240.	280.	280.
Heat rate (K/min)	2.	4.	3.	5.	3.
Initial hold (min)		3.		0.5	1.
Final hold (min)				2.
I	1024.	1025.	1031.	1033.	1030.
Reference	Orav, Raal, et al., 2006	Ouamba, Ouabonzi, et al., 2006	Ozcan, Chalchat, et al., 2006	Ozel, Gogus, et al., 2006	Pandey-Rai S., Mallavarapu G.R., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	SPB-5	DB-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	Hydrogen	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	70.	70.	70.
T_end (C)	260.	250.	280.	280.	280.
Heat rate (K/min)	4.	4.	4.	4.	4.
Initial hold (min)		2.	4.	4.	4.
Final hold (min)		20.
I	1029.	1032.	1031.	1030.	1032.
Reference	Petrovic, Ristic, et al., 2006	Pino, Marquez, et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	HP-5	HP-5MS	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	H2	He	H2		He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	280.	280.	240.	250.	200.
Heat rate (K/min)	4.	3.	3.	10.	2.
Initial hold (min)	2.			5.
Final hold (min)	10.				60.
I	1031.	998.	1032.	1028.	1030.
Reference	Pino, Sauri-Duch, et al., 2006	Pitarokili, Tzakou, et al., 2006	Potzernheim, Bizzo, et al., 2006	Robinson, 2006	Rout, Naik, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	ZB-5	DB-1	Ultra-2
Column length (m)	30.	30.	30.	60.	50.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.32
T_start (C)	60.	60.	40.	70.	50.
T_end (C)	260.	243.	300.	230.	270.
Heat rate (K/min)	5.	3.	2.	2.	2.
Initial hold (min)				2.
Final hold (min)				20.
I	1033.	1025.	1030.	1029.	1033.
Reference	Sabulal, Dan, et al., 2006	Sabulal, Dan, et al., 2006, 2	Sari M., Biondi D.M., et al., 2006	Sawamura, Onishi, et al., 2006	Schlumpberger B.O., Clery R.A., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	FSOT-RSL-200	DB-5	DB-5	DB-5	DB-5
Column length (m)	30.	15.	30.	30.	30.
Carrier gas	Hydrogen	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	50.	40.
T_end (C)	280.	305.	240.	240.	240.
Heat rate (K/min)	6.	15.	4.	4.	4.
Initial hold (min)	5.	2.
Final hold (min)	5.
I	1026.	1033.	1033.	1033.	1030.
Reference	Schmidt, Jirovetz, et al., 2006	Sebastián, Urzúa, et al., 2006	Sefidkon, Abbasi, et al., 2006	Sefidkon, Abbasi, et al., 2006	Sefidkon and Jamzad, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-1	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	30.	25.	60.	25.	25.
Carrier gas	He	N2	Helium	H2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25
T_start (C)	40.	30.	60.	50.	50.
T_end (C)	260.	280.	250.	230.	230.
Heat rate (K/min)	2.	3.	5.	3.	3.
Initial hold (min)	5.
Final hold (min)	20.		10.
I	1030.	1033.	1023.	1031.	1029.
Reference	Senatore, Landolfi, et al., 2006	Shafi, Jose, et al., 2006	Sonboli, Mirjalili, et al., 2006	Tesso, König, et al., 2006	Tesso, Kubeczka, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	Methyl Silicone	SPB-5	DB-5	DB-1
Column length (m)	30.	25.	60.	30.	50.
Carrier gas	Helium	N2	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.3	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.15	1.	0.25	0.25
T_start (C)	60.	50.	40.	60.	90.
T_end (C)	250.	210.	230.	240.	240.
Heat rate (K/min)	2.	2.	3.	4.	4.
Initial hold (min)	8.	5.	5.
Final hold (min)	15.		2.
I	1028.	1038.	1040.	1030.	1012.
Reference	Tigrine-Kordiani, Meklati, et al., 2006	Tonzibo, Coffy, et al., 2006	Tornambe, Cornu, et al., 2006	Trilles, Bombarda, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	SPB-1	SPB-1	DB-5
Column length (m)	25.	30.	50.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.52	0.25	0.33	0.25	0.25
T_start (C)	50.	60.	50.	50.	40.
T_end (C)	280.	250.	220.	250.	250.
Heat rate (K/min)	2.5	10.	4.	4.	4.
Initial hold (min)	5.	2.	1.	1.
Final hold (min)		10.	10.	10.
I	1031.	1035.	1019.	1017.	1031.
Reference	Wang, Kong, et al., 2006	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006	Wong, Sivasothy, et al., 2006	Yadegarinia, Gachkar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-30	DB-5	HP-5MS	HP-1
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25		0.25	0.25	0.2
Phase thickness (μm)	0.25		0.25	0.25	0.5
T_start (C)	40.	90.	60.	60.	60.
T_end (C)	250.	220.	210.	280.	250.
Heat rate (K/min)	4.	7.	3.	3.	2.
Initial hold (min)		2.	5.
Final hold (min)					60.
I	1025.	1020.	1029.	1024.	1025.
Reference	Yadegarinia, Gachkar, et al., 2006	Ahuja, Bakshi, et al., 2005	Askari and Sefidkon, 2005	Basta, Tzakou, et al., 2005	Bendimerad and Bendiab, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-1	DB-5	DB-5	DB-5
Column length (m)	30.	25.	50.	25.	30.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.25	0.3	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.25
T_start (C)	60.	50.	60.	40.	60.
T_end (C)	240.	250.	240.	220.	240.
Heat rate (K/min)	3.	3.	2.	3.	3.
Initial hold (min)		3.		5.
Final hold (min)
I	1032.	1027.	1031.	1027.	1031.
Reference	Busman, Zoghbi, et al., 2005	Cégiéla-Carlioz, Bessière, et al., 2005	Chagonda and Chalchat, 2005	Chagonda and Chalchat, 2005, 2	Chaverri and Cicció, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	SPB-5	HP-5	DB-1	DB-1
Column length (m)	60.	60.	25.	30.	60.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.3	0.32	0.2	0.25	0.25
Phase thickness (μm)		1.	0.33	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	240.	230.	240.	250.	250.
Heat rate (K/min)	3.	3.	3.	5.	5.
Initial hold (min)		5.		5.
Final hold (min)			7.	15.	10.
I	1024.	1038.	1026.	1035.	1029.
Reference	Chalchat and Özcan, 2005	Cornu, Kondjoyan, et al., 2005	Duarte, Figueira, et al., 2005	Facundo, Pinto, et al., 2005	Fakhari A.R., Sonboli A., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	HP-5	HP-5	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	300.	250.	30.	300.	200.
Heat rate (K/min)	3.	2.	4.	5.	4.
Initial hold (min)	3.	60.	3.	5.	30.
Final hold (min)			15.	5.
I	1022.	1020.	1029.	1031.	1024.
Reference	Ferraz, Limberger, et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005	Ferretti, Maggi, et al., 2005	Figuérédo, Cabassu, et al., 2005	Gauvin and Smadja, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RSL-200	DB-1	DB-1	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.25	0.25	0.25
T_start (C)	50.	40.	50.	50.	60.
T_end (C)	250.	280.	265.	265.	240.
Heat rate (K/min)	3.	6.	2.5	2.5	3.
Initial hold (min)	3.	2.	1.	1.
Final hold (min)	10.	10.	20.	30.
I	1032.	1027.	1014.	1017.	1028.
Reference	Ghasemi Y., Faridi P., et al., 2005	Jirovetz, Buchbauer, et al., 2005	Khanavi, Ghasemian, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005	Khayyat and Karimi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	HP-5MS	HP-5
Column length (m)	60.	30.	30.	30.	60.
Carrier gas	He		Helium		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	35.	35.	38.	30.
T_end (C)	250.	280.	280.	220.	260.
Heat rate (K/min)	4.	4.	4.	5.	2.
Initial hold (min)	5.	2.	2.	1.	2.
Final hold (min)				2.	28.
I	1030.	1029.	1029.	1031.	1030.9
Reference	Khajeh, Yamini, et al., 2005	Kowalski and Wolski, 2005	Kowalski, 2005	Krist, Stuebiger, et al., 2005	Leffingwell and Alford, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	MDN-5	DB-5	DB-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	230.	270.	220.	220.	220.
Heat rate (K/min)	3.	4.	4.	4.	4.
Initial hold (min)		4.	5.	4.	4.
Final hold (min)		5.
I	1027.	1034.	1029.	1029.	1030.
Reference	Limberger, Sobral, et al., 2005	van Loon, Linssen, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Morteza-Semnani and Saeedi, 2005	Morteza-Semnani and Saeedi, 2005, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	HP-5	DB-5	DB-1
Column length (m)	30.	25.	30.	30.	50.
Carrier gas	He		He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.15	0.25	0.25	0.25
T_start (C)	50.	50.	70.	40.	95.
T_end (C)	250.	230.	240.	250.	240.
Heat rate (K/min)	3.	3.	5.	5.	4.
Initial hold (min)	5.			0.5
Final hold (min)				2.
I	1030.	1024.	1032.	1030.	1026.
Reference	Najafpour Navaei, Mirza, et al., 2005	Olawore, Ogunwande, et al., 2005	Oyedeji, Yani, et al., 2005	Özel, Gögüs, et al., 2005	Palá-Paúl, Pérez-Alonso, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	RTX-5 MS	HP-5MS	SPB-5	HP-5MS
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.32
T_start (C)	95.	50.	60.	60.	60.
T_end (C)	240.	280.	280.	250.	250.
Heat rate (K/min)	4.	8.	3.	4.	5.
Initial hold (min)		2.		2.	3.
Final hold (min)		2.		20.
I	1026.	1034.	1029.	1031.	1031.
Reference	Pala-Paul, Perez-Alonso, et al., 2005	Pellati, Benvenuti, et al., 2005	Petrakis, Roussis, et al., 2005	Pino, Marbot, et al., 2005	Pourmortazavi, Ghadiri, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB	DB-5
Column length (m)	12.5	30.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	40.	40.	60.
T_end (C)	270.	220.	220.	220.	200.
Heat rate (K/min)	4.	4.	4.	4.	2.
Initial hold (min)		1.	1.	1.
Final hold (min)					80.
I	1025.	1029.	1029.	1029.	1033.
Reference	Ricci, Fraternale, et al., 2005	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Rout, Misra, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5MS	DB-5	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	220.	280.	275.	220.	265.
Heat rate (K/min)	6.	4.	4.	3.	2.5
Initial hold (min)	3.			4.	1.
Final hold (min)					20.
I	1037.	1030.	1031.	1027.	1013.
Reference	Safaei-Ghomi, Bamoniri, et al., 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005	Salehi, Sefidkon, et al., 2005	Sarkhail, Amin, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	240.	280.	240.	300.	300.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)		5.
Final hold (min)
I	1030.	1027.	1030.	1023.	1023.
Reference	Sefidkon and Jamzad, 2005	Setzer, Noletto, et al., 2005	da Silva, Andrade, et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	PE-5	DB-5	HP-5MS	RTX-1	RTX-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	230.	230.	280.	250.	25.
Heat rate (K/min)	5.	3.	3.	5.	5.
Initial hold (min)	2.
Final hold (min)	4.	20.		10.	10.
I	1038.	1039.	1029.	1027.	1025.
Reference	Singh, Raina, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005	Sonboli A., Fakhari A.R., et al., 2005	Sonboli, Salehi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 8 CB	HP-5MS	HP-5 MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.50	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	210.	290.	285.	260.	280.
Heat rate (K/min)	2.	3.	4.3	3.	3.
Initial hold (min)	2.	5.
Final hold (min)	33.			20.
I	1032.	1038.	1031.	1030.	998.
Reference	Stevanovic, Garneau, et al., 2005	Suárez, Vásquez, et al., 2005	Tesevic, Nikicevic, et al., 2005	Topçu, Barla, et al., 2005	Tzakou, Bazos, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	DB-1	DB-1	HP-5MS
Column length (m)	30.	30.	50.	50.	30.
Carrier gas	He	Helium	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	90.	60.	40.
T_end (C)	280.	240.	240.	240.	220.
Heat rate (K/min)	3.	3.	4.	3.	3.
Initial hold (min)					5.
Final hold (min)					10.
I	1002.	1029.	1012.	1016.	1025.
Reference	Tzakou and Constantinidis, 2005	Urdampilleta, Amat, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2	Vichi, Riu-Aumatell, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	250.	250.	250.	250.	260.
Heat rate (K/min)	5.	5.	5.	5.	5.
Initial hold (min)	2.	2.	2.	2.	2.
Final hold (min)	5.	5.	5.	10.	13.
I	1021.	1021.	1023.	1021.	1032.
Reference	N/A	N/A	N/A	Wu, Krings, et al., 2005	Yayli, Yasar, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	BP-1	SE-52	HP-1
Column length (m)	30.	30.	50.	25.	50.
Carrier gas	He	He		N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.32	0.2
Phase thickness (μm)	0.32	0.25	0.25	0.15	0.33
T_start (C)	60.	90.	60.	45.	60.
T_end (C)	250.	220.	220.	200.	250.
Heat rate (K/min)	5.	7.	2.	3.	2.
Initial hold (min)	3.	2.		5.
Final hold (min)		5.	20.	30.	20.
I	1021.	1019.	1020.	1040.	1017.
Reference	Aghel, Yamini, et al., 2004	Agnihotri, Thappa, et al., 2004	Blanc, Muselli, et al., 2004	Cakir, Kordali, et al., 2004	Cavalli, Fernandez, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-1	DB-5	SPB-5	HP-5 MS
Column length (m)	60.	60.	30.	60.	30.
Carrier gas	He	N2	He	He	Helium
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	1.	0.25
T_start (C)	60.	70.	60.	60.	60.
T_end (C)	230.	230.	240.	200.	275.
Heat rate (K/min)	2.	2.	2.	4.	4.
Initial hold (min)		2.
Final hold (min)	45.	20.		30.
I	1023.	1039.	1029.	1033.	1030.
Reference	Cavalli, Tomi, et al., 2004	Choi, 2004	Cicció, 2004	Gauvin, Ravaomanarivo, et al., 2004	Ghannadi, Sajjadi, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	ZB-5	DB-5	RTX-1
Column length (m)	30.	25.	60.	60.	30.
Carrier gas	N2		He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	40.	40.	60.
T_end (C)	230.	180.	260.	280.	300.
Heat rate (K/min)	2.	3.	6.	4.	4.
Initial hold (min)		10.	4.6	4.
Final hold (min)		10.	1.
I	1031.	1029.	1040.	1027.	1025.
Reference	González, Guerra, et al., 2004	bin Jantan, Ayop, et al., 2004	Jürgens and Dötterl, 2004	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	HP-5MS	DB-5MS	DB-5	RTX-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	260.	230.	240.	300.	300.
Heat rate (K/min)	2.	5.	3.	3.	4.
Initial hold (min)	5.	2.
Final hold (min)		10.
I	1029.	1028.	1031.	1025.	1025.
Reference	Kilic, Hafizoglu, et al., 2004	Li and Jiang, 2004	paz Lima, Silva, et al., 2004	Limberger, Sobral, et al., 2004	Lis, Boczek, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	DB-5MS	DB-5MS	HP-5MS
Column length (m)	30.	25.	30.	30.	30.
Carrier gas		N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	210.	220.	280.	280.	275.
Heat rate (K/min)	2.	5.	3.	3.	4.
Initial hold (min)	2.
Final hold (min)	33.		30.	30.
I	1031.	1025.	1000.	1001.	1033.
Reference	Lopez Arze, Collin, et al., 2004	Mallavarapu, Kulkarni, et al., 2004	Marongiu, Piras, et al., 2004	Marongiu, Porcedda, et al., 2004	Mehrabani, Asadipour, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	DB-1	NB-30
Column length (m)	30.	30.	50.	60.	50.
Carrier gas	He	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25			0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	280.	240.	240.	270.	250.
Heat rate (K/min)	3.	2.	2.	4.	2.
Initial hold (min)
Final hold (min)		999.	999.
I	1032.	1031.	1031.	1030.	1024.
Reference	Mimica-Dukic, Bozin, et al., 2004	Miyazawa, Fuhita, et al., 2004	Miyazawa, Fujita, et al., 2004	Nik, Mirza, et al., 2004	Orav, Stulova, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-1	DB-1	DB-1	DB-1
Column length (m)	50.	50.	50.	60.	60.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.2	0.22	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	70.	95.	35.	35.
T_end (C)	250.	220.	240.	230.	230.
Heat rate (K/min)	2.	4.	4.	2.	2.
Initial hold (min)				4.	4.
Final hold (min)				25.	25.
I	1026.	1022.	1015.	1015.	1017.
Reference	Orav, Stulova, et al., 2004	Palá-Paúl, García-Jiménez, et al., 2004	Palá-Paúl, Velasco-Negueruela, et al., 2004	Park, Lee, et al., 2004	Park, Lee, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	NB-30	NB-30	HP-5MS
Column length (m)	60.	60.	50.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.2	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	35.	50.	50.	60.
T_end (C)	230.	230.	250.	250.	280.
Heat rate (K/min)	2.	2.	2.	2.	4.
Initial hold (min)	4.	4.
Final hold (min)	25.	25.
I	1020.	1020.	1024.	1024.	1026.
Reference	Park, Lee, et al., 2004	Park, Lee, et al., 2004	Raal, Arak, et al., 2004	Raal, Paaver, et al., 2004	Sadeghpour, Asghari, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	DB-5	HP-1
Column length (m)	30.	60.	60.	30.	30.
Carrier gas	He		Nitrogen		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	50.	70.	70.	50.	40.
T_end (C)	265.	230.	230.	250.	260.
Heat rate (K/min)	2.5	2.	2.	3.	2.
Initial hold (min)	1.	2.	2.	5.	5.
Final hold (min)	20.	20.			20.
I	1013.	1033.	1033.	1030.	1023.
Reference	Sarkhail, Amin, et al., 2004	Sawamura, Son, et al., 2004	Sawamura, Sou, et al., 2004	Sefidkon, Jamzad, et al., 2004	Senatore, Napolitano, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	DB-5	DB-5
Column length (m)	30.	25.	25.	30.	30.
Carrier gas	He	N2	H2		He
Substrate
Column diameter (mm)	0.25	0.2	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.5	0.52	0.25	0.25
T_start (C)	40.	30.	40.	60.	60.
T_end (C)	250.	280.	240.	300.	240.
Heat rate (K/min)	2.	3.	4.	3.	3.
Initial hold (min)	5.
Final hold (min)	20.
I	1029.	1033.	1031.	1022.	1028.
Reference	Senatore, Rigano, et al., 2004	Shafi, Nambiar, et al., 2004	Simic, Sokovic, et al., 2004	Suyenaga, Apel, et al., 2004	Tellez, Khan, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	BPX-5	CP Sil 8 CB	CP Sil 8 CB
Column length (m)	20.	30.	25.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.32
Phase thickness (μm)	0.25	0.25	1.	0.25	0.25
T_start (C)	100.	60.	60.	50.	50.
T_end (C)	270.	300.	250.	200.	200.
Heat rate (K/min)	8.	3.	3.	10.	5.
Initial hold (min)	2.		5.	3.	5.
Final hold (min)			10.	2.
I	1020.	1029.	1040.	1030.	1031.
Reference	Thappa, Bakshi, et al., 2004	Tirillini, Pellegrino, et al., 2004	Vilaseca, Guy, et al., 2004	Wang and Guo-Y. -L., 2004	Wang, Guo, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-5	DB-1	HP-5MS
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.249	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	70.	60.
T_end (C)	300.	220.	240.	230.	280.
Heat rate (K/min)	3.	5.	4.	2.	3.
Initial hold (min)		10.		2.
Final hold (min)				20.
I	1026.	1030.	1031.	1039.	1028.
Reference	Woerdenbag, Windono, et al., 2004	Bertoli, Menichini, et al., 2003	Cabanillas, Lopez, et al., 2003	Choi, 2003	Couladis, Özcan, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	RTX-5Sil	DB-5	DB-5	DB-5
Column length (m)	12.5	30.	60.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)		0.25
T_start (C)	50.	70.	50.	50.	50.
T_end (C)	270.	200.	220.	220.	200.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)
Final hold (min)		10.
I	1025.	1030.	1029.	1029.	1029.
Reference	Curini, Bianchi, et al., 2003	Dudai, Larkov, et al., 2003	Edris and Farrag, 2003	Edris and Farrag, 2003	Edris, Shalaby, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	HP-5MS	HP-5	RSL-200
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He	H2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	50.	70.	60.	60.	40.
T_end (C)	220.	200.	280.	275.	280.
Heat rate (K/min)	3.	10.	4.	4.	6.
Initial hold (min)					5.
Final hold (min)					5.
I	1034.	1024.	1031.	1028.	1026.
Reference	Edris, Shalaby, et al., 2003, 2	Fekam Boyom, Amvam Zollo, et al., 2003	Ghasemi, Asghari, et al., 2003	Ghannadi and Zolfaghari, 2003	Jirovetz, Buchbauer, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RSL-200	SE-30	CP Sil 5 CB	DB-5
Column length (m)	30.	30.	12.	25.	30.
Carrier gas	H2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.3	0.25	0.25
T_start (C)	40.	40.	70.	35.	60.
T_end (C)	280.	280.	220.	280.	280.
Heat rate (K/min)	6.	6.	3.	5.	5.
Initial hold (min)	2.	5.		2.5
Final hold (min)	10.	5.
I	1027.	1025.	1017.	1019.	1025.
Reference	Jirovetz, Buchbauer, et al., 2003, 2	Jirovetz, Buchbauer, et al., 2003, 3	Kambouche and El-Abed, 2003	Kanjilal, Kotoky, et al., 2003	Lago, de Ávila, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	CP Sil 5 CB	ZB-1
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He		N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.39	0.25
T_start (C)	60.	60.	60.	60.	45.
T_end (C)	240.	280.	280.	220.	230.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)
Final hold (min)		30.	30.
I	1029.	1020.	1017.	1028.	1015.
Reference	Machado, Zoghbi, et al., 2003	Marongiu, Porcedda, et al., 2003	Marongiu, Porcedda, et al., 2003	Mazloomifar, Saber-Tehrani, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	OV-101	CP Sil 5 CB	DB-1
Column length (m)	60.	30.	50.	25.	50.
Carrier gas	He	Helium	He	H2	N2
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.25	0.25
Phase thickness (μm)	0.25		0.5	0.15	0.25
T_start (C)	50.	70.	50.	50.	95.
T_end (C)	270.	210.	250.	230.	240.
Heat rate (K/min)	4.	2.	2.	3.	4.
Initial hold (min)
Final hold (min)		60.
I	1032.	1030.	1020.	1021.	1033.
Reference	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003	Orav, Kailas, et al., 2003	Oyedeji, Ekundayo, et al., 2003	Perez-Alonso, Velasco-Negueruela, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	DB-1	DB-1
Column length (m)	30.	60.	30.	60.	60.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	75.	40.	40.
T_end (C)	280.	250.	220.	220.	220.
Heat rate (K/min)	4.	4.	3.	4.	4.
Initial hold (min)	10.		4.
Final hold (min)	40.
I	1030.	1022.	1030.	1019.	1027.
Reference	Pino, Marbot, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Priestap, van Baren, et al., 2003	Rasooli and Mirmostafa, 2003	Rasooli and Mirmostafa, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	Methyl Silicone	SPB-5	DB-1
Column length (m)	30.	30.		60.	60.
Carrier gas	N2	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25		0.32	0.25
Phase thickness (μm)	0.25	0.25		1.0	0.25
T_start (C)	40.	60.	35.	30.	40.
T_end (C)	230.	275.	180.	230.	260.
Heat rate (K/min)	2.	4.	4.	3.	4.
Initial hold (min)					5.
Final hold (min)
I	1031.	1033.	1006.	1036.	1021.
Reference	Rotman, Ahumada, et al., 2003	Sadraei, Ghannadi, et al., 2003	Santos and Cordeiro, 2003	Sebastian, Viallon-Fernandez, et al., 2003	Sefidkon, Naderi Nik, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	HP-5	HP-5
Column length (m)	60.	30.	60.	60.	60.
Carrier gas	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	40.	40.	40.
T_end (C)	280.	240.	250.	250.	250.
Heat rate (K/min)	4.	3.	5.	5.	5.
Initial hold (min)			15.	15.	15.
Final hold (min)
I	1021.	1029.	1033.	1033.	1033.
Reference	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-1	DB-1	HP-1	HP-5
Column length (m)	30.	60.	60.	50.	25.
Carrier gas	He	N2	N2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.5	0.53
T_start (C)	60.	70.	70.	60.	40.
T_end (C)	240.	230.	230.	220.	280.
Heat rate (K/min)	3.	2.	2.	2.	4.
Initial hold (min)		2.	2.
Final hold (min)		20.	20.	40.
I	1029.	1040.	1041.	1017.	1029.
Reference	Taveira, de Lima, et al., 2003	Tu, Onishi, et al., 2003	Tu, Onishi, et al., 2003, 2	Valette, Fernandez, et al., 2003	Velickovic, Randjelovic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	SPB-1
Column length (m)	25.	25.	25.	25.	30.
Carrier gas	H2	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.53	0.25
T_start (C)	40.	40.	40.	40.	40.
T_end (C)	280.	280.	280.	280.	200.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)					10.
Final hold (min)
I	1033.	1024.	1024.	1029.	1015.
Reference	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Vichi, Castellote, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5	DB-5	DB-5	DB-1
Column length (m)	30.	30.	30.	25.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	50.
T_end (C)	200.	250.	240.	250.	280.
Heat rate (K/min)	3.	5.	3.	4.	4.
Initial hold (min)	10.	30.
Final hold (min)				10.
I	1016.	1040.	1030.	1031.	1022.
Reference	Vichi, Pizzale, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003	Zrira, Elamrani, et al., 2003	Ahmadi, Mirza, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	OV-101	DB-5	HP-1
Column length (m)	25.	60.	25.	30.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.4	0.25		0.25	0.25
T_start (C)	60.	60.	50.	60.	70.
T_end (C)	260.	220.	200.	280.	220.
Heat rate (K/min)	5.	4.	5.	3.	3.
Initial hold (min)
Final hold (min)	40.			30.	15.
I	1022.	1022.	1024.	1020.	1020.
Reference	Azaz. D., Demirci, et al., 2002	Baher, Mirza, et al., 2002	Boyom, Keumedjio, et al., 2002	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	DB-1	DB-5MS	DB-5MS	DB-5MS
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	75.	50.	60.	60.	50.
T_end (C)	200.	200.	280.	280.	280.
Heat rate (K/min)	3.	3.	3.	3.	15.
Initial hold (min)	4.	6.			2.
Final hold (min)	8.				10.
I	1029.	1024.	1030.	1030.	1027.
Reference	Cicció and Gómez-Laurito, 2002	Cimanga, Apers, et al., 2002	Congiu, Falconieri, et al., 2002	Congiu, Falconieri, et al., 2002	Damon, Hernández, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BPX-5	HP-5	DB-5	DB-1
Column length (m)	25.		30.	30.	30.
Carrier gas	N2		N2	He	H2
Substrate
Column diameter (mm)	0.50		0.25	0.25	0.32
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	40.	50.	60.	40.
T_end (C)	220.	260.	250.	240.	245.
Heat rate (K/min)	5.	5.	4.	3.	3.
Initial hold (min)			5.		20.
Final hold (min)	10.
I	1024.	1035.	1031.	1033.	1010.
Reference	Das, Ram, et al., 2002	Diaz and Kite, 2002	Farah, Fechtal. M., et al., 2002	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	PTE-5	HP-5	RSL-200	RSL-200
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	H2		H2	H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.30		0.25	0.25
T_start (C)	60.	60.	50.	40.	50.
T_end (C)	275.	285.	200.	280.	280.
Heat rate (K/min)	4.	4.3	3.	6.	6.
Initial hold (min)				5.	5.
Final hold (min)				5.	5.
I	1027.	1031.	1031.	1027.	1031.
Reference	Ghannadi, Sajjadi, et al., 2002	Gudzic, Djokovic, et al., 2002	Isidorov and Jdanova, 2002	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	CP Sil 8 CB	DB-1	SPB-5	DB-5
Column length (m)	30.	30.	25.	60.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.23	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.20	0.25	0.25
T_start (C)	40.	50.	50.	50.	60.
T_end (C)	280.	220.	200.	240.	240.
Heat rate (K/min)	6.	3.	3.	5.	3.
Initial hold (min)	2.	2.	3.	3.
Final hold (min)	10.		30.	10.
I	1027.	1028.	1030.	1036.	1032.
Reference	Jirovetz, Smith, et al., 2002	Juteau, Masotti, et al., 2002	Khallouki, Younos, et al., 2002	Kim and Lee, 2002	Kobaisy, Tellez, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	DB-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.32
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	35.	35.	50.	60.	40.
T_end (C)	280.	280.	200.	250.	290.
Heat rate (K/min)	3.	4.	5.	3.	7.
Initial hold (min)	2.	2.
Final hold (min)	15.	15.
I	1029.	1030.	1028.	1027.	1038.
Reference	Krauze-Baranowska, Mardarowicz, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002, 2	Kuiate, Bessière, et al., 2002	Limberger, Simões-Pires, et al., 2002	Lin, Rouseff, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-5	DB-5MS	OV-101
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	50.
T_end (C)	290.	275.	240.	240.	200.
Heat rate (K/min)	7.	4.	3.	3.	5.
Initial hold (min)		4.
Final hold (min)
I	1033.	1015.	1030.	1030.	1024.
Reference	Lin, Rouseff, et al., 2002	Lockwood, Asghari, et al., 2002	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Menut, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	OV-101	DB-1	DB-5MS
Column length (m)	25.	30.	50.	50.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.32
Phase thickness (μm)		0.25	0.5	0.25	0.25
T_start (C)	60.	60.	50.	80.	40.
T_end (C)	220.	250.	250.	225.	280.
Heat rate (K/min)	5.	4.	2.	4.	4.
Initial hold (min)		10.
Final hold (min)					5.
I	1028.	1030.	1020.	1014.	1030.
Reference	Monfared, Davarani, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002	Orav, Kailas, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Phutdhawong, Korth, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	HP-1	DB-5	DB-5	DB-1
Column length (m)	30.	50.	30.	25.	60.
Carrier gas	Helium	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25
T_start (C)	60.	90.	60.	60.	40.
T_end (C)	250.	220.	300.	220.	250.
Heat rate (K/min)	4.	3.	2.	3.	4.
Initial hold (min)	2.
Final hold (min)	20.
I	1030.	1024.	1027.	1028.	1022.
Reference	Pino, Marbot, et al., 2002	Priestap, van Baren, et al., 2002	Ruberto, Biondi, et al., 2002	Schwob, Bessière, et al., 2002	Sefidkon, Dabiri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-1	DB-1	HP-5
Column length (m)	60.	30.	50.	50.	30.
Carrier gas	He	He	N2	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	95.	60.	40.
T_end (C)	280.	240.	240.	240.	280.
Heat rate (K/min)	4.	3.	4.	3.	4.
Initial hold (min)	5.
Final hold (min)
I	1020.	1032.	1012.	1016.	1031.
Reference	Sefidkon, 2002	Tellez, Khan, et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002, 2	Velickovic, Randjelovic, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5MS	DB-5	DB-1	DB-5MS
Column length (m)	60.	30.	30.	60.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.248	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	250.	270.	240.	220.	240.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)	5.			5.
Final hold (min)				22.
I	1025.	1028.	1014.	1022.	1022.
Reference	Yamini, Sefidkon, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Bailac, Dellacasa, et al., 2001	Cherchi, Deidda, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	DB-1	DB-5MS	DB-5MS
Column length (m)	60.	60.	60.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	40.	35.	35.
T_end (C)	220.	280.	280.	250.	250.
Heat rate (K/min)	3.	4.	4.	3.	3.
Initial hold (min)	5.	5.	5.	5.	5.
Final hold (min)	15.
I	1029.	1019.	1024.	1033.	1034.
Reference	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Fernando and Grün, 2001	Fernando and Grün, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	OV-1	HP-5	BP-1	Optima-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	H2	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.3	0.25	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	220.	250.	220.	220.	250.
Heat rate (K/min)	5.	3.	5.	5.	3.
Initial hold (min)	10.	1.	10.		3.
Final hold (min)		20.
I	1032.	1019.	1032.	1023.	1027.
Reference	Flamini, Cioni, et al., 2001	Gallori, Bilia, et al., 2001	Gallori, Flamini, et al., 2001	Gupta, Mallavarapu, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RTX-1	SPB-1	SPB-5	BP-1
Column length (m)	30.	30.	30.	60.	50.
Carrier gas	H2	N2	N2	Helium	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	70.	50.	60.
T_end (C)	280.	300.	180.	240.	230.
Heat rate (K/min)	6.	4.	2.	3.	2.
Initial hold (min)	5.		2.	3.
Final hold (min)	5.		1.	10.	35.
I	1020.	1025.	1024.	1039.	1021.
Reference	Jirovetz L., Buchbauer G., et al., 2001	Kalemba, Marschall, et al., 2001	Kamath, Asha, et al., 2001	Kim and Lee, 2001	Lota, de Rocca Serra, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CBP-1	DB-5MS	DB-5MS	RSL-200	OV-101
Column length (m)	25.	30.	30.	30.	50.
Carrier gas	Nitrogen	He	He	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.5
T_start (C)	50.	60.	60.	40.	50.
T_end (C)	210.	240.	240.	280.	250.
Heat rate (K/min)	3.	3.	3.	6.	2.
Initial hold (min)	2.			5.
Final hold (min)		30.	30.	5.
I	1019.	1033.	999.	1020.	1020.
Reference	Ly, Yamauchi, et al., 2001	Marongiu, Porcedda, et al., 2001	Marongiu, Porcedda, et al., 2001	Ngassoum, Jirovetz, et al., 2001	Orav, Kailas, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-1	DB-5	DB-5
Column length (m)	50.	50.	30.	30.	60.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.2	0.2	0.25	0.32	0.25
Phase thickness (μm)			0.25	0.5
T_start (C)	50.	50.	80.	35.	50.
T_end (C)	250.	250.	225.	275.	250.
Heat rate (K/min)	2.	2.	4.	6.	3.
Initial hold (min)					5.
Final hold (min)
I	1020.	1020.	1015.	1030.	1030.
Reference	Orav and Kann, 2001	Orav and Kann, 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Rouseff, Jella, et al., 2001	Rousis, Papadogianni, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5 MS	DB-5	OV-101
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	H2	He	Helium	He	N2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25
T_start (C)	60.	60.	50.	60.	80.
T_end (C)	285.	240.	250.	240.	200.
Heat rate (K/min)	3.	3.	5.	3.	2.
Initial hold (min)			2.
Final hold (min)			5.
I	1024.	1026.0	1022.	1032.	1030.
Reference	Santos-Gomes and Fernandes-Ferreira, 2001	Santos, Moreira, et al., 2001	Shang, Hu, et al., 2001	Tellez M., Estell R., et al., 2001	Yang, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CP Sil 5 CB	DB-1	CP Sil 5 CB	HP-5
Column length (m)	50.	25.	60.	25.	30.
Carrier gas	N2		N2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.15	0.25	0.4	0.25
T_start (C)	80.	50.	60.	60.	40.
T_end (C)	200.	230.	220.	260.	280.
Heat rate (K/min)	2.	3.	3.	5.	3.
Initial hold (min)			5.	40.	10.
Final hold (min)			22.		10.
I	1030.	1021.	1028.	1016.	1027.
Reference	Yang, 2001, 2	Asekun and Ekundayo, 2000	Bailac, Dellacasa, et al., 2000	Baser, Özek, et al., 2000	Bicalho, Pereira, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RSL-200	SPB-5	HP-5	DB-5
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25		0.25
T_start (C)	40.	40.	70.	80.	60.
T_end (C)	240.	250.	240.	200.	240.
Heat rate (K/min)	3.	6.	5.	9.	3.
Initial hold (min)			8.
Final hold (min)			20.	10.
I	1040.	1025.	1049.	1032.	1030.
Reference	García, Martín, et al., 2000	Jirovetz, Puschmann, et al., 2000	Kim, Kim, et al., 2000	Lis-Balchin and Roth, 2000	Maia, Zoghbi, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	BP-1	HP-5	DB-1
Column length (m)	25.	30.	25.	30.	30.
Carrier gas	Nitrogen	N2	N2	He	He
Substrate
Column diameter (mm)	0.50	0.22	0.33	0.25	0.25
Phase thickness (μm)	0.25	0.25	1.0	0.25	0.25
T_start (C)	60.	70.	60.	60.	40.
T_end (C)	220.	230.	275.	275.	260.
Heat rate (K/min)	5.	4.	4.	4.	2.
Initial hold (min)		2.			5.
Final hold (min)		20.			2.
I	1027.	1036.	1031.	1030.	1024.
Reference	Mallavarapu, Rao, et al., 2000	Mitiku, Sawamura, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2	Senatore, Napolitano, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	Methyl Silicone	CP Sil 5 CB	OV-101
Column length (m)	50.	30.	50.	25.	25.
Carrier gas	Nitrogen	He	H2	H2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.5	0.15
T_start (C)	40.	60.	40.	50.	50.
T_end (C)	200.	240.	260.	320.	200.
Heat rate (K/min)	2.	3.	4.	3.	5.
Initial hold (min)	10.		0.5
Final hold (min)
I	1025.	1032.	1026.	1026.	1027.
Reference	Tamura, Boonbumrung, et al., 2000	Tellez, Dayan, et al., 2000	Vendramini and Trugo, 2000	Asekun and Ekundayo, 1999	Ayedoun, Adéoti, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	SPB-1	OV-101	RTX-1	OV-101
Column length (m)	60.	50.	52.	30.	25.
Carrier gas			Helium	N2
Substrate
Column diameter (mm)	0.25	0.2	0.26	0.25	0.32
Phase thickness (μm)	0.25	0.33	0.13	0.25
T_start (C)	40.	60.	50.	60.	50.
T_end (C)	220.	260.	220.	300.	200.
Heat rate (K/min)	5.	4.	3.	4.	5.
Initial hold (min)	10.		0.
Final hold (min)			0.
I	1022.10	1021.	1020.	1026.	1024.
Reference	Baraldi, Rapparini, et al., 1999	Choo, Wong, et al., 1999	Dzumayev, Tkachenko, et al., 1999	Kalemba, 1999	Kuiate, Zollo, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	DB-5	OV-1	OV-1	OV-101
Column length (m)	25.	30.	25.		50.
Carrier gas	H2		H2		Helium
Substrate
Column diameter (mm)	0.32	0.32	0.25		0.20
Phase thickness (μm)	0.17	1.	0.25		0.50
T_start (C)	40.	40.	40.	50.	30.
T_end (C)	260.	200.	220.	160.	100.
Heat rate (K/min)	3.	3.	3.	2.	1.
Initial hold (min)	5.	5.	5.		6.
Final hold (min)			5.
I	1012.	1030.	1024.	1025.	1018.
Reference	Lopes, Koketsu, et al., 1999	Meynier, Novelli, et al., 1999	Oberhofer, Nikiforov, et al., 1999	Orav, Kailas, et al., 1999	Orav, Kailas, et al., 1999, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	OV-101	DB-5	SE-30
Column length (m)	25.	50.	50.	30.	30.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.20
T_start (C)	50.	70.	70.	40.	60.
T_end (C)	230.	240.	220.	250.	200.
Heat rate (K/min)	3.	4.	2.	2.	3.
Initial hold (min)			5.	5.	4.
Final hold (min)				60.
I	1020.	1015.	1022.	1028.	1026.
Reference	Oyedeji, Olawore, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Pateira, Nogueira, et al., 1999	Porta, Porcedda, et al., 1999	Prikhod'ko, Klyuev, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Ultra-2	BP-1	CP Sil 5 CB	DB-1	DB-1
Column length (m)	25.	25.	25.		60.
Carrier gas		N2	He		He
Substrate
Column diameter (mm)	0.2	0.5	0.25		0.25
Phase thickness (μm)			0.39		0.25
T_start (C)	40.	60.	60.	50.	40.
T_end (C)	300.	220.	220.	260.	280.
Heat rate (K/min)	5.	5.	5.	4.	4.
Initial hold (min)	4.		5.		5.
Final hold (min)		10.	20.
I	1030.	1024.	1022.	1020.	1022.
Reference	Quiroz, Fuentes-Contreras, et al., 1999	Rao, Bhattacharya, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Schultz, Kaiser, et al., 1999	Sefidkon, Dabiri, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	OV-101	SPB-5
Column length (m)	30.	60.	30.	25.	60.
Carrier gas	He	He	H2	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.20	0.32
Phase thickness (μm)	0.25				1.
T_start (C)	40.	60.	32.	60.	40.
T_end (C)	220.	230.	260.	220.	200.
Heat rate (K/min)	4.	3.	7.	4.	3.
Initial hold (min)	5.		5.	0.	5.
Final hold (min)		5.	5.	0.	2.
I	1026.	1025.	1039.	1021.	1038.
Reference	Sefidkon and Khajavi, 1999	Shafiee, Javidnia, et al., 1999	Sun and Petracek, 1999	Tropnikova, Zenkevich, et al., 1999	Viallon C., Verdier-Metz I., et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5MS	HP-5	SPB-5	DB-5
Column length (m)	25.	30.	50.	50.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)		0.25	0.32	0.32	0.25
Phase thickness (μm)	0.39	0.25	0.52	0.25	0.25
T_start (C)	60.	60.	35.	60.	60.
T_end (C)	220.	240.	250.	240.	240.
Heat rate (K/min)	5.	3.	2.	3.	3.
Initial hold (min)			15.
Final hold (min)			45.	20.
I	1028.	1029.	1030.	1030.	1024.
Reference	Weyerstahl, Marschall, et al., 1999	Zoghbi, Andrade, et al., 1999	Boylston and Viniyard, 1998	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	OV-1	CBP-1	DB-5	HP-101
Column length (m)	25.	50.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.32	0.25	0.25	0.2
Phase thickness (μm)		0.25		0.25	0.2
T_start (C)	60.	50.	60.	60.	70.
T_end (C)	180.	250.	240.	240.	200.
Heat rate (K/min)	3.	10.	4.	3.	3.
Initial hold (min)	10.	5.			2.
Final hold (min)		20.			10.
I	1026.	1018.	1031.	1030.	1025.
Reference	Jantan, Ahmad, et al., 1998	Kökdil, Kurucu, et al., 1998	Lamarque, Maestri, et al., 1998	Maia, Zohhbi, et al., 1998	Milso, Mastelic, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-5	HP-1	OV-101	HP-1
Column length (m)	25.	25.	60.	25.	30.
Carrier gas		He	He		He
Substrate
Column diameter (mm)	0.32	0.2	0.25	0.32	0.25
Phase thickness (μm)		0.33	0.25		0.1
T_start (C)	35.	70.	50.	50.	50.
T_end (C)	250.	290.	280.	200.	300.
Heat rate (K/min)	4.	3.	4.	5.	5.
Initial hold (min)		8.	5.		2.
Final hold (min)		20.			3.
I	1021.	1032.	1021.	1027.	1029.
Reference	Ong, Acree, et al., 1998	Poiana, Sicari, et al., 1998	Stashenko, Cervantes, et al., 1998	Zollo, Biyiti, et al., 1998	Boatright and Crum, 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB	OV-1	SPB-Sulfur
Column length (m)	25.	25.	25.	30.	30.
Carrier gas	N2	N2	He		He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	4.
T_start (C)	50.	50.	60.	40.	45.
T_end (C)	290.	290.	300.	270.	240.
Heat rate (K/min)	4.	4.	6.	2.	5.
Initial hold (min)				4.	13.
Final hold (min)					5.
I	1017.	1017.	1017.	1024.	1038.
Reference	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997, 2	Kökdil, Tanker, et al., 1997	Mariaca, Berger, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-Sulfur	DB-5	DB-1	DB-5	DB-5
Column length (m)	30.	30.		30.	30.
Carrier gas	He	He		Helium	He
Substrate
Column diameter (mm)	0.32	0.25		0.25	0.25
Phase thickness (μm)	4.	0.25		0.25
T_start (C)	45.	50.	80.	60.	60.
T_end (C)	240.	250.	220.	240.	240.
Heat rate (K/min)	5.	2.	6.	3.	4.
Initial hold (min)	13.	5.
Final hold (min)	5.
I	1039.	1028.	1009.	1031.	1030.
Reference	Mariaca, Berger, et al., 1997	Reverchon, Porta, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Zunino, Novillo-Newton, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CBP-1	HP-1	OV-101	HP-1	OV-101
Column length (m)	25.	23.	50.	30.	50.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.22	0.32	0.25	0.53	0.25
Phase thickness (μm)		0.17	0.17	0.88
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	240.	250.	220.	300.	250.
Heat rate (K/min)	5.	5.	5.	8.	2.
Initial hold (min)		3.
Final hold (min)		30.		15.
I	1029.	1019.	1033.	1022.	1020.
Reference	Zygadlo, Ariza-Espinar, et al., 1997	Ayedoun, Adeoti, et al., 1996	Chacko, Jayalekshmy, et al., 1996	Malizia, Molli, et al., 1996	Orav, Kailas, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	BP-1	DB-1	DB-5
Column length (m)	25.	25.	25.	60.	30.
Carrier gas	N2	N2	N2	He
Substrate
Column diameter (mm)	0.50	0.50	0.50	0.32	0.25
Phase thickness (μm)				0.50
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	220.	220.	220.	250.	210.
Heat rate (K/min)	5.	5.	5.	8.	2.
Initial hold (min)				1.	2.
Final hold (min)				6.	33.
I	1022.	1024.	1025.	1031.	1031.
Reference	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Sagrero-Nieves and Bartley, 1996	Sohounhloue, Dangou, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	SE-54	SPB-1	DB-1	OV-101
Column length (m)	25.	50.	50.	60.	52.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.2	0.25	0.26
Phase thickness (μm)	0.25	1.05	0.33
T_start (C)	60.	40.	40.	30.	50.
T_end (C)	220.	300.	200.	200.	220.
Heat rate (K/min)	4.	2.	3.	4.	3.
Initial hold (min)	2.		3.	25.
Final hold (min)	20.		30.	20.
I	1019.	1039.	1024.	1020.	1021.
Reference	Thanh, Dung, et al., 1996	Weenen, Koolhaas, et al., 1996	Wong and Lai, 1996	Buttery and Ling, 1995	Dzumayev, Tsibulskaya, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	OV-101	DB-1	OV-101
Column length (m)			50.	60.	50.
Carrier gas			He	He	N2
Substrate
Column diameter (mm)			0.2	0.25	0.25
Phase thickness (μm)			0.5	0.25
T_start (C)	35.	35.	70.	50.	80.
T_end (C)	200.	200.	180.	250.	200.
Heat rate (K/min)	6.	6.	1.	3.5	2.
Initial hold (min)	2.	2.		5.
Final hold (min)
I	1038.	1038.	1020.	1020.	1024.
Reference	Larsen and Frisvad, 1995	Larsen and Frisvad, 1995, 2	Orav, Kuningas, et al., 1995	Stashenko, Torres, et al., 1995	Tamura, Nakamoto, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-1	DB-1	DB-5 MS
Column length (m)	50.	60.	60.	60.	30.
Carrier gas	N2	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)		0.25	0.25
T_start (C)	80.	70.	70.	30.	50.
T_end (C)	200.	270.	270.	200.	250.
Heat rate (K/min)	2.	2.5	2.5	4.	4.
Initial hold (min)		5.	5.	25.
Final hold (min)				20.
I	1025.	1026.	1026.	1020.	1031.
Reference	Tamura, Nakamoto, et al., 1995	Tirado, Stashenko, et al., 1995	Tirado, Stashenko, et al., 1995	Buttery, Stern, et al., 1994	Gomez and Ledbetter, 1994
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	HP-5	HP-5	HP-101	OV-101
Column length (m)	50.			50.	50.
Carrier gas	N2			H2
Substrate
Column diameter (mm)	0.27			0.32	0.22
Phase thickness (μm)	0.2			0.3
T_start (C)	80.	40.	40.	65.	80.
T_end (C)	240.	210.	210.	300.	200.
Heat rate (K/min)	3.	2.	2.	2.	2.
Initial hold (min)				5.
Final hold (min)
I	1027.	1031.	1033.	1019.	1030.
Reference	Ramanoelina, Viano, et al., 1994	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Demarne and van der Walt, 1993	Egolf and Jurs, 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	Methyl Silicone	CP Sil 5 CB	DB-5	DB-1
Column length (m)	50.	50.	25.	60.	30.
Carrier gas	N2	N2		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.17	0.17		0.25	0.25
T_start (C)	80.	80.	60.	40.	50.
T_end (C)	200.	200.	280.	200.	240.
Heat rate (K/min)	2.	3.	5.	3.	5.
Initial hold (min)				2.	3.
Final hold (min)
I	1030.	1039.	1025.	1057.	1022.
Reference	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Kaul, Singh, et al., 1993	Shimoda, Shibamoto, et al., 1993	Shiota, 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	DB-1	SPB-5	SE-54
Column length (m)	30.	54.	60.	30.	30.
Carrier gas	He	He	He		Hydrogen
Substrate
Column diameter (mm)	0.25	0.26	0.32		0.25
Phase thickness (μm)	0.25		1.2	1.0	0.25
T_start (C)	50.	50.	30.	50.	60.
T_end (C)	240.	230.	240.	250.	250.
Heat rate (K/min)	5.	3.	3.	8.	2.
Initial hold (min)	3.		10.		5.
Final hold (min)					2.
I	1024.	1012.	1029.	1029.	1029.
Reference	Shiota, 1993	Zenkevich and Kulikova, 1993	Ciccioli, Cecinato, et al., 1992	King and Knight, 1992	Kollmannsberger, Nitz, et al., 1992
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5	OV-101	DB-1
Column length (m)	30.	30.	60.	50.	60.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	1.0	1.0	0.25	0.5	0.25
T_start (C)	40.	40.	40.	50.	50.
T_end (C)	250.	250.	250.	250.	240.
Heat rate (K/min)	3.	3.	2.	4.	3.
Initial hold (min)			5.
Final hold (min)	30.	30.
I	1023.	1030.	1031.	1019.	1024.
Reference	Peppard, 1992	Peppard, 1992	Lee, Macku, et al., 1991	Misharina, Golovnya, et al., 1991	Shiota, 1991
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	DB-1	CP Sil 8 CB
Column length (m)	60.	30.	60.	60.	25.
Carrier gas	He	N2
Substrate
Column diameter (mm)	0.25		0.32	0.32	0.20
Phase thickness (μm)	0.25
T_start (C)	50.	80.	50.	50.	60.
T_end (C)	240.	220.	230.	230.	230.
Heat rate (K/min)	3.	4.	4.	4.	3.
Initial hold (min)					10.
Final hold (min)			10.	10.
I	1029.	1019.	1020.	1020.	1037.
Reference	Shiota, 1991	Velasco-Negueruela, Pérez Alonso, et al., 1991	Binder, Benson, et al., 1990	Binder, Turner, et al., 1990	Jantan and Goh, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	BP-1	OV-101	OV-101
Column length (m)	50.	50.	25.	50.	50.
Carrier gas	Nitrogen	Nitrogen		N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.33	0.25	0.25
Phase thickness (μm)
T_start (C)	70.	80.	45.	80.	80.
T_end (C)	200.	200.	180.	200.	200.
Heat rate (K/min)	2.	2.	3.	2.	2.
Initial hold (min)			3.
Final hold (min)
I	1027.	1028.	1022.	1029.	1032.
Reference	Sugisawa, Nakamura, et al., 1990	Sugisawa, Nakamura, et al., 1990	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-1	HP-1	HP-1	HP-1
Column length (m)	12.	12.	12.	25.	50.
Carrier gas
Substrate
Column diameter (mm)	0.2	0.2	0.2	0.32	0.2
Phase thickness (μm)	0.33	0.33	0.33	0.52	0.11
T_start (C)	40.	40.	40.	40.	40.
T_end (C)
Heat rate (K/min)	16.	4.	8.	8.	6.
Initial hold (min)	0.395	0.4	0.801	0.8	3.194
Final hold (min)
I	1020.3	1014.4	1020.3	1021.1	1021.4
Reference	Yin and Sun, 1990	Yin and Sun, 1990	Yin and Sun, 1990	Yin and Sun, 1990	Yin and Sun, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	SE-30	OV-101	OV-101	OV-101
Column length (m)	50.	40.	50.	50.	50.
Carrier gas	H2	He	N2	N2	N2
Substrate
Column diameter (mm)	0.30	0.50	0.25	0.25	0.25
Phase thickness (μm)		0.75
T_start (C)	40.	30.	80.	80.	80.
T_end (C)	250.	220.	200.	200.	200.
Heat rate (K/min)	10.	3.	2.	2.	2.
Initial hold (min)	1.
Final hold (min)
I	1021.	1020.	1029.	1024.	1027.
Reference	Brophy, Davies, et al., 1989	de Pooter, de Buyck, et al., 1989	Sugisawa, Yamamoto, et al., 1989	Sugisawa, Yang, et al., 1989	Sugisawa, Yang, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	OV-1	OV-1	OV-3
Column length (m)	30.	25.	50.	60.	150.
Carrier gas	Hydrogen	Hydrogen	He	Helium	He
Substrate
Column diameter (mm)	0.35	0.20	0.20	0.50	0.66
Phase thickness (μm)	1.0		0.20	1.2
T_start (C)	45.	70.	30.	40.	30.
T_end (C)	220.	180.	220.	220.	170.
Heat rate (K/min)	2.	3.	2.	2.	1.
Initial hold (min)		5.
Final hold (min)
I	1044.	1030.	1019.	1020.	1030.
Reference	Georgilopoulos and Gallois, 1988	MacLeod, MacLeod, et al., 1988	de Pooter, Nicolai, et al., 1988	Wahab, Aboutabl, et al., 1987	Buttery, Flath, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-1	OV-1	OV-1
Column length (m)	50.	50.	10.	40.
Carrier gas			H2	He	He
Substrate
Column diameter (mm)	0.30	0.30	0.25	0.5
Phase thickness (μm)			0.25	0.75
T_start (C)	40.	40.	50.	30.	40.
T_end (C)	230.	230.	250.	220.	220.
Heat rate (K/min)	3.5	3.5	5.	3.	2.
Initial hold (min)	5.	5.
Final hold (min)
I	1021.	1032.	1019.	1019.	1020.
Reference	Nykanen, 1986	Nykanen, 1986	Perry, Baxter, et al., 1986	de Pooter, de Buyck, et al., 1986	De Pooter, De Buyck, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-101	DB-1	DB-1
Column length (m)	30.	30.	30.	50.	50.
Carrier gas	He	He	He
Substrate
Column diameter (mm)	0.5	0.5	0.5	0.32	0.32
Phase thickness (μm)	0.8	0.8	0.8
T_start (C)	40.	40.	40.	0.	50.
T_end (C)	220.	220.	220.	250.	250.
Heat rate (K/min)	2.	2.	2.	3.	3.
Initial hold (min)
Final hold (min)
I	1019.	1019.	1019.	1019.	1016.
Reference	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986	Habu, Flath, et al., 1985	Habu, Flath, et al., 1985
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-1	SE-30	OV-1
Column length (m)	50.	50.	60.	50.	183.
Carrier gas		He		He	N2
Substrate
Column diameter (mm)	0.32	0.31	0.32	0.5	0.762
Phase thickness (μm)
T_start (C)	50.	0.	50.	40.	0.
T_end (C)	225.	225.	250.	170.	230.
Heat rate (K/min)	4.	3.	4.	3.	1.
Initial hold (min)	0.1	1.	0.1	3.
Final hold (min)	30.		5.
I	1020.	1013.	1019.	1021.	1024.
Reference	Stern, Flath, et al., 1985	del Rosario, de Lumen, et al., 1984	Flath, Mon, et al., 1983	Heydanek and McGorrin, 1981	Schreyen, Dirinck, et al., 1979
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary
Active phase	SF-96	SF-96
Column length (m)	111.	111.
Carrier gas	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.76	0.76
Phase thickness (μm)
T_start (C)
T_end (C)	130.	130.
Heat rate (K/min)	3.	3.
Initial hold (min)	8.	8.
Final hold (min)	40.	40.
I	1008.	1020.
Reference	Donetzhuber, Johansson, et al., 1976	Donetzhuber, Johansson, et al., 1976
Comment	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Edris, A.E.; Farrag, E.S., Antifungal activity of peppermint and sweet basil essential oils and their major aroma constituents on some plant pathogenic fungi from the vapor phase, Nahrung/Food, 2003, 47, 2, 117-121, https://doi.org/10.1002/food.200390021 . [all data]

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Kim and Lee, 2002
Kim, N.-S.; Lee, D.-S., Comparison of different extraction methods for the analysis of fragrances from Lavandula species by gas chromatography-mass spectrometry, J. Chromatogr. A, 2002, 982, 1, 31-47, https://doi.org/10.1016/S0021-9673(02)01445-0 . [all data]

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Fernando and Grün, 2001
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Asekun and Ekundayo, 2000
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Kim, H.-J.; Kim, K.; Kim, N.-S.; Lee, D.-S., Determination of floral fragrances of Rosa hybrida using solid-phase trapping-solvent extraction and gas chromatography-mass spectrometry, J. Chromatogr. A, 2000, 902, 2, 389-404, https://doi.org/10.1016/S0021-9673(00)00863-3 . [all data]

Lis-Balchin and Roth, 2000
Lis-Balchin, M.; Roth, G., Composition of the essential oils of Pelargonium odoratissimum, P. exstipulatum, and P. x fragrans (Geraniaceae) and their bioactivity, Flavour Fragr. J., 2000, 15, 6, 391-394, https://doi.org/10.1002/1099-1026(200011/12)15:6<391::AID-FFJ929>3.0.CO;2-W . [all data]

Maia, Zoghbi, et al., 2000
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Vendramini and Trugo, 2000
Vendramini, A.L.; Trugo, L.C., Chemical composition of acerola fruit (Malpighia punicifolia L.) at three stages of maturity, Food Chem., 2000, 71, 2, 195-198, https://doi.org/10.1016/S0308-8146(00)00152-7 . [all data]

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Kalemba, 1999
Kalemba, D., Constituents of the essential oil of Artemisia asiatica Nakai, Flavour Fragr. J., 1999, 14, 3, 173-176, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<173::AID-FFJ805>3.0.CO;2-Q . [all data]

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Rustaiyan, A.; Masoudi, S.; Monfared, A.; Komeilizadeh, H., Volatile constituents of three Salvia species grown wild in Iran, Flavour Fragr. J., 1999, 14, 5, 276-278, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<276::AID-FFJ825>3.0.CO;2-Y . [all data]

Schultz, Kaiser, et al., 1999
Schultz, K.; Kaiser, R.; Knudsen, J.T., Cyclanthone and derivatives, new natural products in the flower scent of Cyclanthus bipartitus Poit., Flavour Fragr. J., 1999, 14, 3, 185-190, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<185::AID-FFJ809>3.0.CO;2-7 . [all data]

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de Pooter, de Buyck, et al., 1989
de Pooter, H.L.; de Buyck, L.F.; Schamp, N.M.; Billiet, F.; De Bruyn, A., The volatile fraction of Otacanthus coeruleus Lindl. Containing the new copaene derivative β-copaen-4α-ol, Flavour Fragr. J., 1989, 4, 2, 47-51, https://doi.org/10.1002/ffj.2730040202 . [all data]

Sugisawa, Yamamoto, et al., 1989
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Sugisawa, Yang, et al., 1989
Sugisawa, H.; Yang, R.H.; Kawabata, C.; Tamura, H., Volatile constituents in the peel oil of sudachi (Citrus sudachi), Agric. Biol. Chem., 1989, 53, 6, 1721-1723, https://doi.org/10.1271/bbb1961.53.1721 . [all data]

Georgilopoulos and Gallois, 1988
Georgilopoulos, D.N.; Gallois, A.N., Flavour compounds of a commercial concentrated blackberry juice, Food Chem., 1988, 28, 2, 141-148, https://doi.org/10.1016/0308-8146(88)90143-4 . [all data]

MacLeod, MacLeod, et al., 1988
MacLeod, A.J.; MacLeod, G.; Subramanian, G., Volatile aroma constitutents of celery, Phytochemistry, 1988, 27, 2, 373-375, https://doi.org/10.1016/0031-9422(88)83101-7 . [all data]

de Pooter, Nicolai, et al., 1988
de Pooter, H.L.; Nicolai, B.; De Laet, J.; De Buyck, L.F.; Schamp, N.M.; Goetghebeur, P., The Essential Oils of Five Nepeta Species. A Preliminary Evaluation of their Use in Chemotaxonomy by Cluster Analysis, Flavour Fragr. J., 1988, 3, 4, 155-159, https://doi.org/10.1002/ffj.2730030404 . [all data]

Wahab, Aboutabl, et al., 1987
Wahab, S.M.A.; Aboutabl, E.A.; El-Zalabani, S.M.; DePooter, H.L.; Al-Fallaha, B., The essential oil of olibanum, Planta Medica, 1987, 53, 04, 382-384, https://doi.org/10.1055/s-2006-962745 . [all data]

Buttery, Flath, et al., 1986
Buttery, R.G.; Flath, R.A.; Mon, T.R.; Ling, L.C., Identification of germacrene D in walnut and fig leaf volatiles, J. Agric. Food Chem., 1986, 34, 5, 820-822, https://doi.org/10.1021/jf00071a013 . [all data]

Nykanen, 1986
Nykanen, I., High Resolution Gas Chromatographic - Mass Spectrometric determination of the Flavour Composition of Wild Majoram (Origanum vulgare L.) Cultivated in Finland, Z. Lebensm Unters Forsch, 1986, 183, 4, 267-272, https://doi.org/10.1007/BF01087742 . [all data]

Perry, Baxter, et al., 1986
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de Pooter, H.L.; de Buyck, L.F.; Schamp, N.M.; Aboutabl, E.; De Bruyn, A.; Husain, S.Z., The Volatile Fraction of Senecio glaucus subsp. coronopifolius, Flavour Fragr. J., 1986, 1, 4-5, 159-163, https://doi.org/10.1002/ffj.2730010406 . [all data]

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De Pooter and Schamp, 1986
De Pooter, H.L.; Schamp, N.M., Comparison of the Volatile Composition of Some Calamintha/Satureja Species, Prog. Essnt. Oil. Res., 1986, 139-150. [all data]

Habu, Flath, et al., 1985
Habu, T.; Flath, R.A.; Mon, T.R.; Morton, J.F., Volatile components of Rooibos tea (Aspalathus linearis), J. Agric. Food Chem., 1985, 33, 2, 249-254, https://doi.org/10.1021/jf00062a024 . [all data]

Stern, Flath, et al., 1985
Stern, D.J.; Flath, R.A.; Mon, T.R.; Teranishi, R.; Lundin, R.E.; Benson, M.E., Crude oleic acid volatiles, J. Agric. Food Chem., 1985, 33, 2, 180-184, https://doi.org/10.1021/jf00062a005 . [all data]

del Rosario, de Lumen, et al., 1984
del Rosario, R.; de Lumen, B.O.; Habu, T.; Flath, R.A.; Mon, T.R.; Teranishi, R., Comparison of headspace volatiles from winged beans and soybeans, J. Agric. Food Chem., 1984, 32, 5, 1011-1015, https://doi.org/10.1021/jf00125a015 . [all data]

Flath, Mon, et al., 1983
Flath, R.A.; Mon, T.R.; Lorenz, G.; Whitten, C.J.; Mackley, J.W., Volatile components of Acacia sp. blossoms, J. Agric. Food Chem., 1983, 31, 6, 1167-1170, https://doi.org/10.1021/jf00120a008 . [all data]

Heydanek and McGorrin, 1981
Heydanek, M.G.; McGorrin, R.J., Gas chromatography-mass spectroscopy investigations on the flavor chemistry of oat groats, J. Agric. Food Chem., 1981, 29, 5, 950-954, https://doi.org/10.1021/jf00107a016 . [all data]

Schreyen, Dirinck, et al., 1979
Schreyen, L.; Dirinck, P.; Sandra, P.; Schamp, N., Flavor analysis of quince, J. Agric. Food Chem., 1979, 27, 4, 872-876, https://doi.org/10.1021/jf60224a058 . [all data]

Donetzhuber, Johansson, et al., 1976
Donetzhuber, A.; Johansson, K.; Sandstroem, C., Gas phase characterization of wood, pulp, and paper, Appl. Polymer Symp., 1976, 28, 889-901. [all data]

Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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