Limonene oxide, cis-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSDB-5HP-5 MSZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.50.50.60.
Tend (C) 200.200.250.230.220.
Heat rate (K/min) 3.3.5.3.4.
Initial hold (min) 2.2.2.10.5.
Final hold (min) 18.18. 10.20.
I 1091.1091.1087.1132.1140.
ReferenceJerkovic, Hegic, et al., 2010Jerkovic and Marijanovic, 2010Ho, Wang, et al., 2009Adams, Beauchamp, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1CP Sil 5 CBDB-1RSL-200
Column length (m) 30.50.30.60.30.
Carrier gas HeHeN2  
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.50.70.40.
Tend (C) 260.220.300.230.280.
Heat rate (K/min) 4.2.4.2.6.
Initial hold (min) 5.  2.2.
Final hold (min)  20. 20.10.
I 1133.1118.1114.1118.1137.
ReferenceAskari and Sefidkon, 2006Boti, Muselli, et al., 2006Lis and Milczarek, 2006Sawamura, Onishi, et al., 2006Jirovetz, Buchbauer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-1DB-1DB-1
Column length (m) 30.30.60.60.60.
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 40.60.60.70.70.
Tend (C) 240.240.250.230.230.
Heat rate (K/min) 4.3.5.2.2.
Initial hold (min)    2.2.
Final hold (min)   10.20.20.
I 1133.1134.1119.1126.1121.
ReferenceSefidkon and Jamzad, 2005da Silva, Andrade, et al., 2005Sonboli, Salehi, et al., 2005Choi, 2004Sawamura, Son, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200HP-5DB-1HP-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas H2HeliumN2 He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.25 0.25 0.25
Tstart (C) 40.70.70.50.60.
Tend (C) 280.210.230.200.240.
Heat rate (K/min) 6.2.2.3.3.
Initial hold (min) 2. 2.  
Final hold (min) 10.60.20.  
I 1137.1134.1125.1129.1132.
ReferenceJirovetz, Buchbauer, et al., 2003Mookdasanit, Tamura, et al., 2003Tu, Onishi, et al., 2003Isidorov and Jdanova, 2002Maia, da Silva, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101OV-101DB-5SPB-Sulfur
Column length (m) 50.50.50.30.30.
Carrier gas N2N2N2N2He
Substrate      
Column diameter (mm) 0.250.250.250.220.32
Phase thickness (μm) 0.25  0.254.
Tstart (C) 80.80.80.70.45.
Tend (C) 225.200.200.230.240.
Heat rate (K/min) 4.2.2.4.5.
Initial hold (min)    2.13.
Final hold (min)    20.5.
I 1120.1123.1123.1133.1137.
ReferencePalá-Paúl, Pérez-Alonso, et al., 2002Yang, 2001Yang, 2001, 2Mitiku, Sawamura, et al., 2000Mariaca, Berger, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-SulfurDB-1DB-1OV-101OV-101
Column length (m) 30.60.60.50.50.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 4.0.250.25  
Tstart (C) 45.70.70.80.80.
Tend (C) 240.270.270.200.200.
Heat rate (K/min) 5.2.52.52.2.
Initial hold (min) 13.5.5.  
Final hold (min) 5.    
I 1138.1118.1118.1122.1123.
ReferenceMariaca, Berger, et al., 1997Tirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Sefidkon and Jamzad, 2005
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da Silva, Andrade, et al., 2005
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Sonboli, Salehi, et al., 2005
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Notes

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