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Lidocaine

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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxane5 % Phenyl methyl siloxaneHP-1Polymethylsiloxane, (PMS-20000)Polymethylsiloxane, (PMS-20000)
Column length (m) 25.25. 12.12.
Carrier gas   HeliumHeHe
Substrate      
Column diameter (mm) 0.200.20 0.200.20
Phase thickness (mum) 0.330.33 0.330.33
Program 50 0C (0.5 min) 99 0C/min -> 100 0C (1 min) 15 0C/min -> 280 0C (20 min)50 0C (0.5 min) 99 0C/min -> 100 0C (1 min) 15 0C/min -> 280 0C (20 min)not specifiednot specifiednot specified
I 1924.1924.1875.1841.1842.
ReferenceGrigoriev and Savchuk, 2010Grigoriev and Savchuk, 2010Grigor'ev, Bozhko, et al., 2009Gambaro, Saligari, et al., 1997Gambaro, Saligari, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1BP-1BP-1BP-1
Column length (m) 12.12.12.12.12.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.220.220.22
Phase thickness (mum) 0.250.250.250.250.25
Program 120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)
I 1856.1857.1857.1858.1858.
ReferenceStowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryOther
Active phase BP-1Methyl Silicone
Column length (m) 12. 
Carrier gas He 
Substrate   
Column diameter (mm) 0.22 
Phase thickness (mum) 0.25 
Program not specifiednot specified
I 1860.1870.
ReferenceStowell and Wilson, 1985Ardrey and Moffat, 1981
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Grigoriev and Savchuk, 2010
Grigoriev, A.M.; Savchuk, S.A., Correlation of the parameters of screening libraries of the gas-chromatographic retention data, Rus. J. Anal. Chem. (Engl. Transl.), 2010, 65, 4, 388-397. [all data]

Grigor'ev, Bozhko, et al., 2009
Grigor'ev, A.M.; Bozhko, E.S.; Rudakova, L.V., Use of correlation between retention indices on low-polarity phases for screening comp-lex mixtures by gas chromatography-mass spectrometry, Rus. J. Anal. Chem., 2009, 64, 2, 140-143, https://doi.org/10.1134/S1061934809020087 . [all data]

Gambaro, Saligari, et al., 1997
Gambaro, V.; Saligari, E.; Froldi, R.; Bianchi, L., Analysis of street drugs by means of HRGC, Bollettino Chimico Farmaceutica, 1997, 36, 4, 359-367. [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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