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Cedrane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedSF-96150.1463.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedSF-96150.1465.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedSF-96150.1455.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedSF-96150.1458.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedSF-96170.1479.Andersen and Falcone, 1969 
PackedSF-96170.1470.Andersen and Falcone, 1969 

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51424.Buchin, Salmon, et al., 200260. m/0.32 mm/1. «mu»m, He, 40. C @ 5. min, 3. K/min, 230. C @ 2. min
CapillaryDB-51471.Buchin, Salmon, et al., 200260. m/0.32 mm/1. «mu»m, He, 40. C @ 5. min, 3. K/min, 230. C @ 2. min

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedCarbowax 20M130.1625.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedCarbowax 20M130.1627.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedCarbowax 20M130.1617.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedCarbowax 20M130.1617.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedCarbowax 20M165.1662.Andersen and Falcone, 1969 
PackedCarbowax 20M165.1651.Andersen and Falcone, 1969 

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51425.Sati and Mathela, 200530. m/0.25 mm/0.26 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 210. C
CapillaryHP-51435.Isidorov, Krajewska, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 40. C; Tend: 250. C
CapillaryRTX-51438.Shellie, Marriott, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 45. C @ 6. min, 3. K/min; Tend: 250. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-51441.Isidorov, Krajewska, et al., 200030. m/0.25 mm/0.25 «mu»m; Program: 40C(1min) => 3C/min => 120C => 5C/min => 280C
CapillaryHP-51437.Isidorov, Krajewska, et al., 200030. m/0.25 mm/0.25 «mu»m; Program: 40C(1min) => 3C/min => 120C => 5C/min => 280C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51436.Letchamo, Ward, et al., 200430. m/0.25 mm/0.25 «mu»m, He; Program: 60C(4min) => 6C/min => 240 => 10C/min => 280C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-Wax1633.Giuseppe, Manuela, et al., 200530. m/0.25 mm/0.25 «mu»m, He; Program: 35C(5min) => 2C/min => 173C(1min) => 15C/min => 210C(5min)

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Maarse, 1975
Maarse, H., Hydrogenolysis of terpenes in the injection port of a gas chromatograph. II. Sesquiterpenes, J. Chromatogr., 1975, 106, 2, 369-384, https://doi.org/10.1016/S0021-9673(00)93846-9 . [all data]

Andersen and Falcone, 1969
Andersen, N.H.; Falcone, M.S., The identification of sesquiterpene hydrocarbons from gas-liquid chromatography retention data, J. Chromatogr., 1969, 44, 52-59, https://doi.org/10.1016/S0021-9673(01)92497-5 . [all data]

Buchin, Salmon, et al., 2002
Buchin, S.; Salmon, J.-C.; Carnat, A.-P.; Berger, T.; Bugaud, C.; Bosset, J.O., Identification de composés monoterpéniques, sesquiterpéniques et benzéniques dans un lait d'alpage très riche en ces substances, Mitt. Lebensmittelunters. Hyg., 2002, 93, 199-216. [all data]

Sati and Mathela, 2005
Sati, S.; Mathela, C.S., Essential oil composition of Valeriana hardwickii var. arnottiana from the Himalayas, Flavour Fragr. J., 2005, 20, 3, 299-301, https://doi.org/10.1002/ffj.1415 . [all data]

Isidorov, Krajewska, et al., 2004
Isidorov, V.A.; Krajewska, U.; Vinogorova, V.T.; Vetchinnikova, L.V.; Fuksman, I.L.; Bal, K., Gas chromatographic analysis of essential oil from buds of different birch species with preliminary partition of components, Biochem. Syst. Ecol., 2004, 32, 1, 1-13, https://doi.org/10.1016/S0305-1978(03)00175-3 . [all data]

Shellie, Marriott, et al., 2003
Shellie, R.; Marriott, P.; Zappia, G.; Mondello, L.; Dugo, G., Interactive use of linear retention indices on polar and apolar columns with an MS-Library for reliable characterization of Australian tea tree and other Melaleuca sp. oils, J. Essent. Oil Res., 2003, 15, 5, 305-312, https://doi.org/10.1080/10412905.2003.9698597 . [all data]

Isidorov, Krajewska, et al., 2000
Isidorov, V.; Krajewska, U.; Bal, K.; Jaroszynska, J.; Niesluchowska, A.; Fuksman, I., GC-MS identification of multicomponent organic compounds mixtures using extra column phase equilibrium, Chem. Anal. (Warsaw), 2000, 45, 513-520. [all data]

Letchamo, Ward, et al., 2004
Letchamo, W.; Ward, W.; Heard, B.; Heard, D., Essential oil of Valeriana officinalis L. cultivars and their antimicrobial activity as influenced by harvesting time under commercial organic cultivation, J. Agric. Food Chem., 2004, 52, 12, 3915-3919, https://doi.org/10.1021/jf0353990 . [all data]

Giuseppe, Manuela, et al., 2005
Giuseppe, Z.; Manuela, G.; Marta, B.; Vincenzo, G., Application of artificial neural network on mono- and sesquiterpenes compounds determined by headspace solid-phase microextraction-gas chromatography-mass spectrometry for the Piedmont ricotta cheese traceability, J. Chromatogr. A, 2005, 1071, 1-2, 247-253, https://doi.org/10.1016/j.chroma.2004.11.083 . [all data]


Notes

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