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3-Carene

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-30PB-1SqualaneApiezon L
Column length (m) 28.40.42.50.45.
Carrier gas He  N2 
Substrate      
Column diameter (mm) 0.250.350.320.250.25
Phase thickness (mum) 0.250.35   
Temperature (C) 150.100.130.70.100.
I 1009.1011.01022.993.1026.
ReferenceViswanathan, Maridass, et al., 2002Tudor, 1997Engewald, Knobloch, et al., 1991Udarov, Manukov, et al., 1987Morishita, Okano, et al., 1980
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SF-96Apiezon L
Column length (m) 80.80.80.  
Carrier gas      
Substrate      
Column diameter (mm) 0.50.50.5  
Phase thickness (mum) 0.80.80.8  
Temperature (C) 100.110.130.100.100.
I 1011.51015.31021.51009.11020.9
ReferenceSaeed, Redant, et al., 1979Saeed, Redant, et al., 1979Saeed, Redant, et al., 1979Andersen and Syrdal, 1970Andersen and Syrdal, 1970
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillary
Active phase SqualaneSF-96
Column length (m) 15.152.
Carrier gas He 
Substrate Chromosorb P 
Column diameter (mm) 0.250.8
Phase thickness (mum)   
Temperature (C) 86.100.
I 999.1013.
ReferenceHively and Hinton, 1968Sakai, Maarse, et al., 1967
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Viswanathan, Maridass, et al., 2002
Viswanathan, M.B.; Maridass, M.; Thangadurai, D.; Ramesh, N., Chemical constituents of the fruit essential oil of Diospyros malabarica (Desr.) Kostel (Ebenaceae), Acta Pharmaceutica, 2002, 52, 207-211. [all data]

Tudor, 1997
Tudor, E., Temperature dependence of the retention index for perfumery compounds on a SE-30 glass capillary column. I. Linear equations, J. Chromatogr. A, 1997, 779, 1-2, 287-297, https://doi.org/10.1016/S0021-9673(97)00453-6 . [all data]

Engewald, Knobloch, et al., 1991
Engewald, W.; Knobloch, T.; Haufe, G.; Muller, M.; Pohris, V., A Novel Method for Terpene Pattern Determination of Essential Oils by Selectivity Tuning in GC, Fresenius' J. Anal. Chem., 1991, 341, 10, 641-643, https://doi.org/10.1007/BF00322279 . [all data]

Udarov, Manukov, et al., 1987
Udarov, B.G.; Manukov, E.N.; Vyglazov, O.G.; Chuiko, V.A.; Izotova, L.V., Gas-chromatographic analysis of alkylated derivatives of carane and of cyclohelptane in capillary columns, Chem. Nat. Compd. (Engl. Transl.), 1987, 22, 4, 398-403, https://doi.org/10.1007/BF00579809 . [all data]

Morishita, Okano, et al., 1980
Morishita, F.; Okano, T.; Kojima, T., Retention indices of monocyclic monoterpene hydrocarbons, Bunseki Kagaku, 1980, 29, 1, 48-53, https://doi.org/10.2116/bunsekikagaku.29.48 . [all data]

Saeed, Redant, et al., 1979
Saeed, T.; Redant, G.; Sandra, P., Kovats Indices of Monoterpene Hydrocarbons on Glass Capillary Columns, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1979, 2, 2, 75-76, https://doi.org/10.1002/jhrc.1240020208 . [all data]

Andersen and Syrdal, 1970
Andersen, N.H.; Syrdal, D.D., Terpenes and sesquiterpenes of chamaecyparis nootkatensis leaf oil, Phytochemistry, 1970, 9, 6, 1325-1340, https://doi.org/10.1016/S0031-9422(00)85326-1 . [all data]

Hively and Hinton, 1968
Hively, R.A.; Hinton, R.E., Variation of the retention index with temperature on squalane substrates, J. Gas Chromatogr., 1968, 6, 4, 203-217, https://doi.org/10.1093/chromsci/6.4.203 . [all data]

Sakai, Maarse, et al., 1967
Sakai, T.; Maarse, H.; Kepner, R.E.; Jennings, W.G.; Longhurst, W.M., Volatile components of Douglas fir needles, J. Agric. Food Chem., 1967, 15, 6, 1070-1072, https://doi.org/10.1021/jf60154a027 . [all data]


Notes

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