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Decane, 5-methyl-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Petrocol DHOV-101Cross-Linked MethylsiliconeUltra-1Ultra-1
Column length (m) 50.80. 50.50.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.22 0.220.22
Phase thickness (mum) 0.5  0.330.33
Tstart (C) 35.30.40.-30.-30.
Tend (C) 200.130.300.240.240.
Heat rate (K/min) 3.1.5.1.2.
Initial hold (min) 10.    
Final hold (min) 10.    
I 1058.31057.41058.1059.031058.91
ReferenceCensullo, Jones, et al., 2003Yin, Liu, et al., 2001Khorasheh, Gray, et al., 1989Haynes and Pitzer, 1985Haynes and Pitzer, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase Ultra-1Ultra-2Ultra-2Ultra-2
Column length (m) 50.50.50.50.
Carrier gas HeHeHeHe
Substrate     
Column diameter (mm) 0.220.220.220.22
Phase thickness (mum) 0.330.330.330.33
Tstart (C) -30.-30.-30.-30.
Tend (C) 240.240.240.240.
Heat rate (K/min) 3.1.2.3.
Initial hold (min)     
Final hold (min)     
I 1059.061058.231058.151058.28
ReferenceHaynes and Pitzer, 1985Haynes and Pitzer, 1985Haynes and Pitzer, 1985Haynes and Pitzer, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Censullo, Jones, et al., 2003
Censullo, A.C.; Jones, D.R.; Wills, M.T., Speciation of the volatile organic compounds (VOCs) in solventborne aerosol coatings by solid phase microextraction-gas chromatography, J. Coat. Technol., 2003, 75, 936, 47-53, https://doi.org/10.1007/BF02697922 . [all data]

Yin, Liu, et al., 2001
Yin, C.; Liu, W.; Li, Z.; Pan, Z.; Lin, T.; Zhang, M., Chemometrics to chemical modeling: structural coding in hydrocarbons and retention indices of gas chromatography, J. Sep. Sci., 2001, 24, 3, 213-220, https://doi.org/10.1002/1615-9314(20010301)24:3<213::AID-JSSC213>3.0.CO;2-4 . [all data]

Khorasheh, Gray, et al., 1989
Khorasheh, F.; Gray, M.R.; Selucky, M.L., Correlation for Kováts retention index of C9-C26 monoalkyl and polymethyl alkanes and alkenes, J. Chromatogr., 1989, 481, 1-16, https://doi.org/10.1016/S0021-9673(01)96747-0 . [all data]

Haynes and Pitzer, 1985
Haynes, P.C., Jr.; Pitzer, E.W., Disengaging solutes in shale- and petroleum-derived jet fuels by altering GC programmed temperature rates, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1985, 8, 5, 230-242, https://doi.org/10.1002/jhrc.1240080504 . [all data]


Notes

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