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Dimethyl phthalate

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryPackedPackedPacked
Active phase DB-5 MSHP-5SE-30SE-30SE-30
Column length (m) 30.60.2.2.2.
Carrier gas HeliumHeNitrogenNitrogenNitrogen
Substrate   Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)
Column diameter (mm) 0.250.32   
Phase thickness (mum) 0.250.25   
Tstart (C) 40.30.100.100.100.
Tend (C) 250.260.290.290.290.
Heat rate (K/min) 4.2.8.8.8.
Initial hold (min) 2.2.   
Final hold (min) 2.28.   
I 1454.1460.71417.1417.1417.
ReferenceSu, Wang, et al., 2009Leffingwell and Alford, 2005Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedCapillary
Active phase SE-30SE-30SE-30SE-30Ultra-1
Column length (m) 2.2.2.2.25.
Carrier gas NitrogenNitrogenNitrogenNitrogenHe
Substrate Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh) 
Column diameter (mm)     0.32
Phase thickness (mum)     0.25
Tstart (C) 100.100.100.100.80.
Tend (C) 290.290.290.290.260.
Heat rate (K/min) 8.8.8.8.3.
Initial hold (min)      
Final hold (min)      
I 1417.1417.1418.1426.1400.
ReferenceLourici, Souici, et al., 1999Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999Okumura, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-1SE-54DB-1OV-101OV-101
Column length (m) 25.25.60.30.25.
Carrier gas HeHe H2He
Substrate      
Column diameter (mm) 0.320.320.320.3 
Phase thickness (mum) 0.25    
Tstart (C) 80.50.50.80.75.
Tend (C) 260.250.250.275.280.
Heat rate (K/min) 3.8.4.2.2.
Initial hold (min)  2.0.17.7.
Final hold (min)  12.5.  
I 1405.1456.1406.1414.1414.
ReferenceOkumura, 1991Harland, Cumming, et al., 1986Flath, Mon, et al., 1983Pinkston, Spiteller, et al., 1981Spiteller and Spiteller, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-101
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 75.
Tend (C) 280.
Heat rate (K/min) 2.
Initial hold (min) 7.
Final hold (min)  
I 1481.
ReferenceSpiteller and Spiteller, 1979
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Su, Wang, et al., 2009
Su, Y.; Wang, C.; Yinlong, G., Analysis of volatile compounds from Mentha hapioealyx Briq. by GC-MS based on accurate mass measurements and retention indices, Acta Chem. Sinica, 2009, 67, 6, 546-554. [all data]

Leffingwell and Alford, 2005
Leffingwell, J.C.; Alford, E.D., Volatile constituents of Perique tobacco, Electron. J. Environ. Agric. Food Chem., 2005, 4, 2, 899-915. [all data]

Lourici, Souici, et al., 1999
Lourici, L.; Souici, M.-L.; Rebbani, N.; Messadi, D., Independent of local properties mathematical models for the calculation of retention indices in programmed temperature gas chromatography, Analusis, 1999, 27, 3, 249-254, https://doi.org/10.1051/analusis:1999114 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Harland, Cumming, et al., 1986
Harland, B.J.; Cumming, R.I.; Gillings, E., The Kovats indexes of some organic micropollutants on an SE54 capillary column, EUR, I Org. Micropollut. Aquat. Environ., 1986, EUR 10388, 123-127. [all data]

Flath, Mon, et al., 1983
Flath, R.A.; Mon, T.R.; Lorenz, G.; Whitten, C.J.; Mackley, J.W., Volatile components of Acacia sp. blossoms, J. Agric. Food Chem., 1983, 31, 6, 1167-1170, https://doi.org/10.1021/jf00120a008 . [all data]

Pinkston, Spiteller, et al., 1981
Pinkston, D.; Spiteller, G.; von Henning, H.; Matthaei, D., High-resolution gas chromatography-mass spectrometry of the methyl esters of organic acids from uremic hemofiltrates, J. Chromatogr., 1981, 223, 1, 1-19, https://doi.org/10.1016/S0378-4347(00)80063-8 . [all data]

Spiteller and Spiteller, 1979
Spiteller, M.; Spiteller, G., Trennung und charakterisierung saurer harnbest and- teile, J. Chromatogr., 1979, 164, 3, 253-317, https://doi.org/10.1016/S0378-4347(00)81232-3 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References