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Dimethyl phthalate

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase VF-5MSDB-1DB-15 % Phenyl methyl siloxaneSE-30
Column length (m) 30.30.30.25.2.
Carrier gas HeHe   
Substrate     Chromosorb Q
Column diameter (mm) 0.250.250.20.31 
Phase thickness (mum) 0.250.250.250.31 
Tstart (C) 60.40.50.50.100.
Tend (C) 270.325.300.250. 
Heat rate (K/min)  3.5.5.10.
Initial hold (min)   2.1. 
Final hold (min)   5.10. 
I 1476.1400.01457.1454.1400.
ReferenceZheng, 2011Sun and Stremple, 2003Johnson, Urso, et al., 1997Guisto, Smith, et al., 1993Helaimia and Messadi, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillaryCapillaryCapillaryCapillary
Active phase SE-30SP-2100SP-2100SP-2100SP-2100
Column length (m) 2.    
Carrier gas  H2H2H2H2
Substrate Chromosorb Q    
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 100.170.170.170.170.
Tend (C)      
Heat rate (K/min) 10.2.4.6.2.
Initial hold (min)      
Final hold (min)      
I 1425.1429.291431.471429.441440.94
ReferenceHelaimia and Messadi, 1989Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-2100SP-2100CP Sil 5 CBSE-54SE-54
Column length (m)    25.25.
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)    0.310.31
Phase thickness (mum)    0.170.17
Tstart (C) 170.170.170.35.35.
Tend (C)      
Heat rate (K/min) 4.6.4.2.2.
Initial hold (min)      
Final hold (min)      
I 1441.551433.141431.251449.1457.
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Weber, 1986Weber, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m)  
Carrier gas N2
Substrate Chromosorb Q
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 100.
Tend (C) 340.
Heat rate (K/min) 10.
Initial hold (min)  
Final hold (min)  
I 1425.
ReferenceMessadi and Vergnaud, 1979
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zheng, 2011
Zheng, Yufang, Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2011. [all data]

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

Johnson, Urso, et al., 1997
Johnson, C.I.; Urso, A.; Geleta, L., Broad spectrum analysis of municipal and industrial effluents discharged into the Peace, Athabasca and Slave river basins: characterization of effluent samples, 1994 - Volume 1 of 2, Northern River Basins Study Project Report No. 121, Norther River Basins Study, Edmonton, Alberta, 1997, 27. [all data]

Guisto, Smith, et al., 1993
Guisto, R.; Smith, S.R.; Stuart, J.D., Gas chromatographic retention indices, mass, and infrared spectra of industrially important adipate esters, J. Chromatogr. Sci., 1993, 31, 6, 225-230, https://doi.org/10.1093/chromsci/31.6.225 . [all data]

Helaimia and Messadi, 1989
Helaimia, F.; Messadi, D., Determination of linear programmed temperature gas chromatography retention indices for some plasticizers, C.R. Acad. Sci. Ser. 2:, 1989, 309, 37-42. [all data]

Podmaniczky, Szepesy, et al., 1986
Podmaniczky, L.; Szepesy, L.; Lakszner, K.; Schomburg, G., Determination of Retention Indices in LPTGC, Chromatographia, 1986, 21, 7, 387-391, https://doi.org/10.1007/BF02346137 . [all data]

Weber, 1986
Weber, L., Utilization of the Sadtler standard RI system in micropollution analyses, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 8, 446-451, https://doi.org/10.1002/jhrc.1240090806 . [all data]

Messadi and Vergnaud, 1979
Messadi, D.; Vergnaud, J.-M., Quick identification and analysis of plasticizers in PVC by programmed-temperature gas chromatography using the best stationary phases, J. Appl. Polym. Sci., 1979, 24, 5, 1215-1225, https://doi.org/10.1002/app.1979.070240507 . [all data]


Notes

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