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Pyrene

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.40.
Tend (C) 310.310.310.310.310.
Heat rate (K/min) 4.4.2.4.6.
Initial hold (min)  5.   
Final hold (min)      
I 2113.42113.42082.62113.42132.5
ReferenceSong, Lai, et al., 2003Song, Lai, et al., 2003Song, Lai, et al., 2003Song, Lai, et al., 2003Song, Lai, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1DB-5DB-5
Column length (m) 25.25. 30.30.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.20.2 0.250.25
Phase thickness (mum) 0.330.33 0.250.25
Tstart (C) 100.100.35.40.40.
Tend (C) 180.180.300.310.310.
Heat rate (K/min) 5.5.8.2.4.
Initial hold (min)      
Final hold (min)      
I 2080.42126.42095.82082.62113.4
ReferenceZhang, Shen, et al., 2000Zhang, Shen, et al., 2000Gautzsch and Zinn, 1996Lai and Song, 1995Lai and Song, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5SP-2100SP-2100
Column length (m) 30.30.30.  
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.250.250.25  
Phase thickness (mum) 0.250.250.25  
Tstart (C) 40.40.40.170.170.
Tend (C) 310.310.310.  
Heat rate (K/min) 6.4.4.4.6.
Initial hold (min)   5.  
Final hold (min)      
I 2132.52113.42113.42049.682060.85
ReferenceLai and Song, 1995Lai and Song, 1995Lai and Song, 1995Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-2100SP-2100SP-2100CP Sil 5 CBSE-52
Column length (m)     33.3
Carrier gas H2H2H2H2He
Substrate      
Column diameter (mm)     0.50
Phase thickness (mum)      
Tstart (C) 170.170.170.170.50.
Tend (C)     320.
Heat rate (K/min) 2.4.6.4.6.
Initial hold (min)     5.
Final hold (min)      
I 2069.402069.262091.452073.472057.
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.616.616.616.616.6
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.500.500.500.500.50
Phase thickness (mum)      
Tstart (C) 50.50.50.50.50.
Tend (C) 320.320.320.320.320.
Heat rate (K/min) 6.6.6.6.6.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 2041.2054.2055.2055.2055.
ReferenceBeernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.616.616.616.616.6
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.500.500.500.500.50
Phase thickness (mum)      
Tstart (C) 50.50.50.50.50.
Tend (C) 320.320.320.320.320.
Heat rate (K/min) 6.6.6.6.6.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 2055.2070.2070.2070.2070.
ReferenceBeernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.616.616.616.616.6
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.500.500.500.500.50
Phase thickness (mum)      
Tstart (C) 50.50.50.50.50.
Tend (C) 320.320.320.320.320.
Heat rate (K/min) 6.6.6.6.6.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 2078.2079.2080.2086.2086.
ReferenceBeernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m) 16.612.12.65.50.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.500.30.280.3 
Phase thickness (mum)  0.340.17  
Tstart (C) 50.50.50.100.100.
Tend (C) 320.250.250.300.300.
Heat rate (K/min) 6.2.2.1.82.5
Initial hold (min) 5.    
Final hold (min)      
I 2093.2063.992048.562070.2040.
ReferenceBeernaert, 1979Lee, Vassilaros, et al., 1979Lee, Vassilaros, et al., 1979Carugno and Rossi, 1967Cantuti, Cartoni, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Song, Lai, et al., 2003
Song, C.; Lai, W.-C.; Madhusudan Reddy, K.; Wei, B., Chapter 7. Temperature-programmed retention indices for GC and GC-MS of hydrocarbon fuels and simulated distillation GC of heavy oils in Analytical advances for hydrocarbon research, Hsu,C.S., ed(s)., Kluwer Academic/Plenum Publishers, New York, 2003, 147-193. [all data]

Zhang, Shen, et al., 2000
Zhang, M.-J.; Shen, S.-D.; Chen, S.-Y.; Sun, Y.-H., Analysis of heavy oil fractions in high-temperature coal tar by capillary gas chromatography/fourier transform infrared spectrometry, Chin. J. Chromatogr., 2000, 18, 3, 241-246. [all data]

Gautzsch and Zinn, 1996
Gautzsch, R.; Zinn, P., Use of incremental models to estimate the retention indexes of aromatic compounds, Chromatographia, 1996, 43, 3/4, 163-176, https://doi.org/10.1007/BF02292946 . [all data]

Lai and Song, 1995
Lai, W.-C.; Song, C., Temperature-programmed retention indices for g.c. and g.c.-m.s. analysis of coal- and petroleum-derived liquid fuels, Fuel, 1995, 74, 10, 1436-1451, https://doi.org/10.1016/0016-2361(95)00108-H . [all data]

Podmaniczky, Szepesy, et al., 1986
Podmaniczky, L.; Szepesy, L.; Lakszner, K.; Schomburg, G., Determination of Retention Indices in LPTGC, Chromatographia, 1986, 21, 7, 387-391, https://doi.org/10.1007/BF02346137 . [all data]

Beernaert, 1979
Beernaert, H., Gas Chromatographic Analysis of Polyclylic Aromatic Hydrocarbons, J. Chromatogr., 1979, 173, 1, 109-118, https://doi.org/10.1016/S0021-9673(01)80450-7 . [all data]

Lee, Vassilaros, et al., 1979
Lee, M.L.; Vassilaros, D.L.; White, C.M.; Novotny, M., Retention Indices for Programmed-Temperature Capillary-Column Gas Chromatography of Polycyclic Aromatic Hydrocarbons, Anal. Chem., 1979, 51, 6, 768-773, https://doi.org/10.1021/ac50042a043 . [all data]

Carugno and Rossi, 1967
Carugno, N.; Rossi, S., Evaluation of polynuclear hydrocarbons in cigarette smoke by glass capillary columns, J. Gas Chromatogr., 1967, 5, 2, 103-106, https://doi.org/10.1093/chromsci/5.2.103 . [all data]

Cantuti, Cartoni, et al., 1965
Cantuti, V.; Cartoni, G.P.; Liberti, A.; Torri, A.G., Improved evaluation of polynuclear hydrocarbons in atmospheric dust by gas chromatography, J. Chromatogr., 1965, 17, 60-65, https://doi.org/10.1016/S0021-9673(00)99836-4 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References