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Pyrene

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Lee's RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSHP-5MS5 % Phenyl methyl siloxane
Column length (m) 60.30.30.30. 
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm)  0.250.250.25 
Phase thickness (mum)  0.250.250.25 
Program not specified60C(2min) => 6C/min => 258C => 2C/min => 300C(4min)not specifiednot specified70 0C (2 min) 30 0C/min -> 150 0C 5 0C/min -> 200 0C 4 0C/min -> 310 0C (5 min)
I 351.352.41351.91352.41348.10
ReferenceFuentes, Font, et al., 2007Wang, Li, et al., 2007Wang, Li, et al., 2007, 2Wang, Li, et al., 2007, 2Skrbic and Onjia, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5MSLM-5LM-5Ultra-1
Column length (m) 60.30.30.30.50.
Carrier gas  HeHeHeNitrogen
Substrate      
Column diameter (mm) 0.250.300.250.250.32
Phase thickness (mum)  0.250.250.250.50
Program not specified50 0C (2 min) 8 0C/min -> 120 0C (3 min) 10 0C/min -> 230 0C60C(2min) => 15C/min => 180C => 5C/min => 280C (10min)60C(2min) => 15C/min => 180C => 5C/min => 280C (10min)40-100 0C 3-15 0C/min -> 290 0C
I 346.3400.00348.28348.46346.0
ReferenceAracil, Font, et al., 2005Cheng, Liu, et al., 2005Ré-Poppi and Santiago-Silva, 2005Ré-Poppi and Santiago-Silva, 2005Sremac, Skrbic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-1Ultra-1Ultra-1DB-5LM-5
Column length (m) 50.50.50.30.30.
Carrier gas NitrogenNitrogenNitrogen He
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.500.500.500.250.25
Program 40-100 0C 3-15 0C/min -> 290 0C40-100 0C 3-15 0C/min -> 290 0C40-100 0C 3-15 0C/min -> 290 0Cnot specified60C(2min) => 15C/min => 180C => 5C/min => 280C(5min)
I 348.1350.3351.2352.8348.43
ReferenceSremac, Skrbic, et al., 2005Sremac, Skrbic, et al., 2005Sremac, Skrbic, et al., 2005Lundstedt, Haglund, et al., 2003Ré-Poppi and Santiago-Silva, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase LM-5HP-5SE-52DB-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.20.300.250.25
Phase thickness (mum) 0.250.11 0.250.25
Program 60C(2min) => 15C/min => 180C => 5C/min => 280C(5min)106C(0.2min) => 40C/min => 120C => 3C/min => 310C(10min)not specified90C (1min) => 10C/min => 120C => 4C/min => 310C (20min)90C (1min) => 10C/min => 120C => 4C/min => 310C (20min)
I 348.46350.71351.22350.52350.79
ReferenceRé-Poppi and Santiago-Silva, 2002Reckendorf, 1997Wang, Peng, et al., 1997Zamperlini, Silva, et al., 1997Zamperlini, Silva, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54SE-52CP Sil 8 CBXTI-5SE-54
Column length (m) 30.30.25.15. 
Carrier gas      
Substrate      
Column diameter (mm) 0.250.250.320.28 
Phase thickness (mum)      
Program not specifiednot specified140C (2min) => (rapidly) => 200C(2min) => 5C/min => 370C140C (2min) => (rapidly) => 200C(2min) => 5C/min => 370Cnot specified
I 351.22351.51351.47351.88350.83
ReferenceChen, 1996Shaogang and Xiaobai, 1994Bemgard, Colmsjo, et al., 1992Bemgard, Colmsjo, et al., 1992Guillen, Iglesias, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-54DB-5DB-5DB-5
Column length (m) 30.15. 30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.25 0.320.32
Phase thickness (mum) 0.250.25   
Program 60 0C (3 min) 10 0C/min -> 100 0C (3 min) 5 0C/min -> 300 0C125 0C (15 min) 1 0C/min -> 131 0C 4 0C/min -> 247 0C 8 0C/min -> 280 0C (15 min)70C(2min) => 30C/min => 150C => 5C/min => 200C => 4C/min => 310Cnot specifiednot specified
I 353.2352.3348.09351.22351.22
ReferencePaschke, Herbel, et al., 1992Peterman and Delfino, 1990Takada, Onda, et al., 1990Naikwadi, Charbonneau, et al., 1987Naikwadi, Charbonneau, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-5SE-52
Column length (m) 30.30. 30. 
Carrier gas    He 
Substrate      
Column diameter (mm) 0.320.32 0.25 
Phase thickness (mum)      
Program not specifiednot specifiednot specifiednot specifiednot specified
I 351.98352.88351.8351.22347.32
ReferenceNaikwadi, Charbonneau, et al., 1987Naikwadi, Charbonneau, et al., 1987Tucminen, Wickstrom, et al., 1986Tong, Centen, et al., 1985Shlyakhov, 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52SE-52
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Program not specifiednot specifiednot specifiednot specifiednot specified
I 347.87348.49349.15350.66351.22
ReferenceShlyakhov, 1984Shlyakhov, 1984Shlyakhov, 1984Shlyakhov, 1984Shlyakhov, 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase SE-52SE-52
Column length (m)   
Carrier gas   
Substrate   
Column diameter (mm)   
Phase thickness (mum)   
Program not specifiednot specified
I 352.30353.34
ReferenceShlyakhov, 1984Shlyakhov, 1984
Comment MSDC-RI MSDC-RI

References

Go To: Top, Lee's RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Fuentes, Font, et al., 2007
Fuentes, M.J.; Font, R.; Gomez-Rico, M.F.; Martin-Gullon, I., Pyrolysis and combustion of waste lubricant oil from diesel cars: Decomposition and pollutants, J. Anal. Appl. Pyrolysis, 2007, 79, 1-2, 215-226, https://doi.org/10.1016/j.jaap.2006.12.004 . [all data]

Wang, Li, et al., 2007
Wang, Z.; Li, K.; Lambert, P.; Yang, C., Identification, characterization and quantitation of pyrogenic polycylic aromatic hydrocarbons and other organic compounds in tire fire products, J. Chromatogr. A, 2007, 1139, 1, 14-26, https://doi.org/10.1016/j.chroma.2006.10.085 . [all data]

Wang, Li, et al., 2007, 2
Wang, Z.; Li, K.; Lambert, P.; Brown, C.E.; Yang, C.; Hollebone, B.P., Identification and characterization of polycyclic aromatic compounds in tire fire products and differentiation of pyrogenic PAHs from petrogenic PAHs in Proceedings of the 30th Arctic and Marine Oilspill (AMOP) Technical Seminar. Vol.1, 2007, 61-85. [all data]

Skrbic and Onjia, 2006
Skrbic, B.; Onjia, A., Prediction of Lee Retention Indices of Polycyclic Aromatic Hydrocarbons by Artificial Neural Networks, J. Chromatorg. A, 2006, 1108, 2, 279-284, https://doi.org/10.1016/j.chroma.2006.01.080 . [all data]

Aracil, Font, et al., 2005
Aracil, I.; Font, R.; Conesa, J.A., Semivolatile and volatile compounds from the pyrolysis and combustion of polyvinyl chloride, J. Anal. Appl. Pyrolysis, 2005, 74, 1-2, 465-478, https://doi.org/10.1016/j.jaap.2004.09.008 . [all data]

Cheng, Liu, et al., 2005
Cheng, D.-X.; Liu, B.-X.; Sun, Y.-A.; Xie, B.; Zhang, H.-L., rapid analysis of pyrolysis products of cholesterol by GC-MS assited with boiling point - Lee retention index, journal of Instrumental Analysis - Fenxi ceshi xuebao, 2005, 24, 6, 85-88. [all data]

Ré-Poppi and Santiago-Silva, 2005
Ré-Poppi, N.; Santiago-Silva, M., Polycyclic aromatic hydrocarbons and other selected organic compounds in ambient air of Campo Grande City, Brazil, Atmos. Environ., 2005, 39, 16, 2839-2850, https://doi.org/10.1016/j.atmosenv.2004.10.006 . [all data]

Sremac, Skrbic, et al., 2005
Sremac, S.; Skrbic, B.; Onjia, A., Artificial neural network prediction of quantitative structure-retention relationships of polycyclic aromatic hydrocarbons in gas chromatography, J. Serb. Chem. Soc., 2005, 70, 11, 1291-1300, https://doi.org/10.2298/JSC0511291S . [all data]

Lundstedt, Haglund, et al., 2003
Lundstedt, S.; Haglund, P.; Öberg, L., Degradation and formation of polycyclic aromatic compounds during bioslurry treatment of an aged gasworks soil, Environ. Toxicol. Chem., 2003, 22, 7, 1413-1420, https://doi.org/10.1002/etc.5620220701 . [all data]

Ré-Poppi and Santiago-Silva, 2002
Ré-Poppi, N.; Santiago-Silva, M.R., Identification of polycyclic aromatic hydrocarbons and methoxylated phenols in wood smoke emitted during production of charcoal, Chromatographia, 2002, 55, 7/8, 475-481, https://doi.org/10.1007/BF02492280 . [all data]

Reckendorf, 1997
Reckendorf, R.M., Identification of phenyl-substituted polycyclic aromatic compounds in ring furnace gases using GC-MS and GC-AED, Chromatographia, 1997, 45, 1, 173-182, https://doi.org/10.1007/BF02505557 . [all data]

Wang, Peng, et al., 1997
Wang, Y.; Peng, P.; Cui, S.; Zhang, Y., Identification of PAH in the Suzhou River bed sediments by GC/MS and PAH retention index system, J. Nanjing Norm. Univ. (Nat. Sci.), 1997, 20, 2, 47-68. [all data]

Zamperlini, Silva, et al., 1997
Zamperlini, G.C.M.; Silva, M.R.S.; Vilegas, W., Identification of polycyclic aromatic hydrocarbons in sugar cane soot by gas chromatography-mass spectrometry, Chromatographia, 1997, 46, 11/12, 655-663, https://doi.org/10.1007/BF02490527 . [all data]

Chen, 1996
Chen, J., GC and GC/MS methods for the analysis of polycyclic aromatic hydrocarbon (PAH) in sediment of the grand canal of China, Toxicol. Environ. Chem., 1996, 54, 1-4, 69-73, https://doi.org/10.1080/02772249609358297 . [all data]

Shaogang and Xiaobai, 1994
Shaogang, C.; Xiaobai, X., System for calculating the linear temperature-programmed retention indices of polycylic aromatic compounds, J. Hi. Res. Chromatogr., 1994, 17, 5, 339-342, https://doi.org/10.1002/jhrc.1240170511 . [all data]

Bemgard, Colmsjo, et al., 1992
Bemgard, A.; Colmsjo, A.; Lundmark, B.-O., Gas chromatographic analysis of high-molecular-weight polynuclear aromatic hydrocarbons. I. Molecular weight 328, J. Chromatogr., 1992, 595, 1-2, 247-258, https://doi.org/10.1016/0021-9673(92)85167-R . [all data]

Guillen, Iglesias, et al., 1992
Guillen, M.D.; Iglesias, M.J.; Dominguez, A.; Blanco, C.G., Polynuclear aromatic hydrocarbon retention indices on SE-54 stationary phase of the volatile components of a coal tar pitch. Relationships between chromatographic retention and thermal reactivity, J. Chromatogr., 1992, 591, 1-2, 287-295, https://doi.org/10.1016/0021-9673(92)80246-Q . [all data]

Paschke, Herbel, et al., 1992
Paschke, A.; Herbel, W.; Steinhart, H.; Franke, S.; Francke, W., Determination of mono- to tetracyclic aromatic hydrocarbons in lubricating oil, J. Hi. Res. Chromatogr., 1992, 15, 12, 827-833, https://doi.org/10.1002/jhrc.1240151211 . [all data]

Peterman and Delfino, 1990
Peterman, P.H.; Delfino, J.J., Identification of isopropylbiphenyl, alkyl diphenylmethanes, diisopropylnaphthalene, linear alkyl benzenes and other polychlorinated biphenyl replacement compounds in effluents, sediments and fish in the Fox River system, Wisconsin, Biomed. Environ. Mass Spectrom., 1990, 19, 12, 755-770, https://doi.org/10.1002/bms.1200191203 . [all data]

Takada, Onda, et al., 1990
Takada, H.; Onda, T.; Ogura, N., Determination of polycyclic aromatic hydrocarbons in urban street dusts and their source materials by capillary gas chromatography, Environ. Sci. Technol., 1990, 24, 8, 1179-1186, https://doi.org/10.1021/es00078a005 . [all data]

Naikwadi, Charbonneau, et al., 1987
Naikwadi, K.P.; Charbonneau, G.M.; Karasek, F.W.; Clement, R.E., Separation and Identification of Organic Compounds in Air Particulate Extracts by High-Performance Liquid Chromatography and Gas Chromatography-Mass Spectrometry, J. Chromatogr., 1987, 398, 227-237, https://doi.org/10.1016/S0021-9673(01)96508-2 . [all data]

Tucminen, Wickstrom, et al., 1986
Tucminen, A.; Wickstrom, K.; Pyysalo, H., Determination of Polycyclic Aromatic Compounds by GLC-Selected Ion Monitoring (SIM) Technique, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 8, 469-471, https://doi.org/10.1002/jhrc.1240090813 . [all data]

Tong, Centen, et al., 1985
Tong, H.Y.; Centen, J.D.; Karasek, F.W.; Jellum, E.; Helland, P., Identification of Trace Organic Compounds in Dimethyl Sulphoxide Solution Using High-Performance Liquid Chromatography and Gas Chromatography-Mass Spectrometry, J. Chromatogr., 1985, 324, 373-383, https://doi.org/10.1016/S0021-9673(01)81336-4 . [all data]

Shlyakhov, 1984
Shlyakhov, A.F., Gas chromatography in organic geochemistry, Nedra, Moscow, 1984, 221. [all data]


Notes

Go To: Top, Lee's RI, non-polar column, custom temperature program, References