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Pyrene

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.50.50.
Tend (C) 310.310.310.310.310.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min) 2.2.2.2.2.
Final hold (min)      
I 2103.2104.2109.2109.2112.
ReferenceMiao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5Ultra-1SE-54
Column length (m) 30.30.30.50.25.
Carrier gas    H2He
Substrate      
Column diameter (mm) 0.320.320.320.20.32
Phase thickness (mum) 0.250.250.250.33 
Tstart (C) 50.50.50.60.50.
Tend (C) 310.310.310.300.250.
Heat rate (K/min) 5.5.5.3.8.
Initial hold (min) 2.2.2. 2.
Final hold (min)    35.12.
I 2114.2134.2135.2085.2096.
ReferenceMiao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999Elizalde-González, Hutfliess, et al., 1996Harland, Cumming, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-5
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum) 0.1
Tstart (C) 60.
Tend (C) 290.
Heat rate (K/min) 10.
Initial hold (min)  
Final hold (min)  
I 2103.
ReferenceQuilliam, Lant, et al., 1985
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Miao and Wu, 1999
Miao, X.; Wu, F., Study on retention behaviors of polycyclic aromatic hydrocarbons by gas chromatography in different operation models, J. Instrumental Anal., 1999, 15, 4, 288-292. [all data]

Elizalde-González, Hutfliess, et al., 1996
Elizalde-González, M.P.; Hutfliess, M.; Hedden, K., Retention index system, adsorption characteristics, and sructure correlations of polycyclic aromatic hydrocarbons in fuels, J. Hi. Res. Chromatogr., 1996, 19, 6, 345-352, https://doi.org/10.1002/jhrc.1240190608 . [all data]

Harland, Cumming, et al., 1986
Harland, B.J.; Cumming, R.I.; Gillings, E., The Kovats indexes of some organic micropollutants on an SE54 capillary column, EUR, I Org. Micropollut. Aquat. Environ., 1986, EUR 10388, 123-127. [all data]

Quilliam, Lant, et al., 1985
Quilliam, M.A.; Lant, M.S.; Kaiser-Farrell, C.; McCalla, D.R.; Sheldrake, C.P.; Kerr, A.A.; Lockington, J.N.; Gibson, E.S., Identification of polycyclic aromatic compounds in of poly-mutagenic emissions from steel casting, Biomed. Mass Spectrom., 1985, 12, 4, 143-150, https://doi.org/10.1002/bms.1200120402 . [all data]


Notes

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