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Tributyl phosphate

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-5DB-5
Column length (m) 30.30.15.15.15.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.20.320.530.530.53
Phase thickness (mum) 0.251.5   
Tstart (C) 50.40.50.50.50.
Tend (C) 300.280.   
Heat rate (K/min) 5.8.10.10.10.
Initial hold (min) 2.4.2.2.2.
Final hold (min) 5.    
I 1613.1622.1616.1638.71647.4
ReferenceJohnson, Urso, et al., 1997Peng, Hua, et al., 1992Hancock and Peters, 1991Hancock and Peters, 1991Hancock and Peters, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedCapillaryCapillary
Active phase DB-5SE-30SE-30DB-1DB-5
Column length (m) 15.2.2.15.15.
Carrier gas He  HeHe
Substrate  Chromosorb QChromosorb Q  
Column diameter (mm) 0.53  0.320.32
Phase thickness (mum)    0.250.25
Tstart (C) 50.100.100.50.50.
Tend (C)    300.300.
Heat rate (K/min) 10.10.10.10.10.
Initial hold (min) 2.  2.2.
Final hold (min)    5. 
I 1647.91623.1636.1615.71658.8
ReferenceHancock and Peters, 1991Helaimia and Messadi, 1989Helaimia and Messadi, 1989D'Agostino and Provost, 1985D'Agostino and Provost, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m)  
Carrier gas N2
Substrate Chromosorb Q
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 100.
Tend (C) 340.
Heat rate (K/min) 10.
Initial hold (min)  
Final hold (min)  
I 1623.
ReferenceMessadi and Vergnaud, 1979
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Johnson, Urso, et al., 1997
Johnson, C.I.; Urso, A.; Geleta, L., Broad spectrum analysis of municipal and industrial effluents discharged into the Peace, Athabasca and Slave river basins: characterization of effluent samples, 1994 - Volume 1 of 2, Northern River Basins Study Project Report No. 121, Norther River Basins Study, Edmonton, Alberta, 1997, 27. [all data]

Peng, Hua, et al., 1992
Peng, C.T.; Hua, R.L.; Maltby, D., Prediction of retention indexes. IV. Chain branching in alkylbenzene isomers with C10-13 alkyl chains identified in a scintillator solvent, J. Chromatogr., 1992, 589, 1-2, 231-239, https://doi.org/10.1016/0021-9673(92)80027-R . [all data]

Hancock and Peters, 1991
Hancock, J.R.; Peters, G.R., Retention index monitoring of compounds of chemical defence interest using thermal desorption gas chromatography, J. Chromatogr., 1991, 538, 2, 249-257, https://doi.org/10.1016/S0021-9673(01)88845-2 . [all data]

Helaimia and Messadi, 1989
Helaimia, F.; Messadi, D., Determination of linear programmed temperature gas chromatography retention indices for some plasticizers, C.R. Acad. Sci. Ser. 2:, 1989, 309, 37-42. [all data]

D'Agostino and Provost, 1985
D'Agostino, P.A.; Provost, L.R., Gas chromatographic retention indices of chemical warfare agents and simulants, J. Chromatogr., 1985, 331, 47-54, https://doi.org/10.1016/0021-9673(85)80005-4 . [all data]

Messadi and Vergnaud, 1979
Messadi, D.; Vergnaud, J.-M., Quick identification and analysis of plasticizers in PVC by programmed-temperature gas chromatography using the best stationary phases, J. Appl. Polym. Sci., 1979, 24, 5, 1215-1225, https://doi.org/10.1002/app.1979.070240507 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References