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Fenchone


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxTC-FFAPDB-WaxBP-20Supelcowax-10
Column length (m) 30. 60.50.30.
Carrier gas HeliumHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.320.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.70.45.50.
Tend (C) 230.220.220.230.250.
Heat rate (K/min) 4.3.4.3.4.
Initial hold (min) 2.  1.1.
Final hold (min) 4.530. 15.10.
I 1426.1405.1392.1388.1398.
ReferenceZeng, Xie, et al., 2011Kurose, Okamura, et al., 2007Pala-Paul, Brophy, et al., 2007La Guerche S., Dauphin B., et al., 2006Wong, Sivasothy, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxDB-WaxCarbowax 20MSupelcowax-10Carbowax 20M
Column length (m) 50.60.25.60.30.
Carrier gas HeHeliumN2HeHe
Substrate      
Column diameter (mm) 0.20.250.250.20.25
Phase thickness (mum) 0.5 0.250.50.25
Tstart (C) 60.70.50.70.50.
Tend (C) 250.210.250.220.215.
Heat rate (K/min) 2.2.4.2.4.
Initial hold (min)      
Final hold (min) 60.60.10.  
I 1410.1414.1383.1397.1410.
ReferenceBendimerad and Bendiab, 2005Mookdasanit, Tamura, et al., 2003Zrira, Elamrani, et al., 2003Orav, Kailas, et al., 2002Kasali, Oyedeji, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20MHP-InnowaxTC-WaxDB-WaxCarbowax 20M
Column length (m) 50.60.60.60.45.
Carrier gas HeHe HeHydrogen
Substrate      
Column diameter (mm) 0.20.250.250.250.32
Phase thickness (mum)  0.25 0.251.0
Tstart (C) 70.50.80.50.60.
Tend (C) 220.220.240.180.200.
Heat rate (K/min) 2.5.3.2.52.
Initial hold (min)  5.5.5.5.
Final hold (min)      
I 1397.1410.1402.1391.1390.
ReferenceOrav and Kann, 2001Stashenko, Cervantes, et al., 1998Shuichi, Masazumi, et al., 1996Stashenko, Puertas, et al., 1996Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPacked
Active phase DB-WaxCarbowax 20MCarbowax 20M
Column length (m) 30.2.2.
Carrier gas  HydrogenHydrogen
Substrate  Gas-Chrom Z (80-100 mesh)Gas-Chrom Z (80-100 mesh)
Column diameter (mm) 0.32  
Phase thickness (mum)    
Tstart (C) 70.65.65.
Tend (C) 200.220.220.
Heat rate (K/min) 4.4.4.
Initial hold (min) 2.  
Final hold (min)    
I 1407.1432.1432.
ReferenceWyllie, Brophy, et al., 1990Stancher and Pertoldi, 1967Stancher and Pertoldi, 1967
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zeng, Xie, et al., 2011
Zeng, Z.; Xie, R.; Zhang, T.; Zhang, H.; Chen, J.Y., Analysis of volatile compositions of Magnolia biondii Pamp by steam distillation and Headspace solid phase micro-extraction, J. Oleo Sci., 2011, 60, 12, 591-596, https://doi.org/10.5650/jos.60.591 . [all data]

Kurose, Okamura, et al., 2007
Kurose, K.; Okamura, D.; Yatagai, M., Composition of the essential oils from the leaves of nine Pinus species and the cones of three of Pinus species, Flavour Fragr. J., 2007, 22, 1, 10-20, https://doi.org/10.1002/ffj.1609 . [all data]

Pala-Paul, Brophy, et al., 2007
Pala-Paul, J.; Brophy, J.J.; Perez-Alonso, M.J.; Usano, J.; Soria, S.C., Essential oil composition of the different parts of Eryngium corniculatum Lam. (Apiaceae) from Spain, J. Chromatogr. A, 2007, 1175, 2, 289-293, https://doi.org/10.1016/j.chroma.2007.10.061 . [all data]

La Guerche S., Dauphin B., et al., 2006
La Guerche S.; Dauphin B.; Pons M.; Blancard D.; Darriet P., Characterization of some mushroom and earthy off-odors microbially induced by the development of rot on grapes, J. Agric. Food Chem., 2006, 54, 24, 9193-9200, https://doi.org/10.1021/jf0615294 . [all data]

Wong, Sivasothy, et al., 2006
Wong, K.C.; Sivasothy, Y.; Boey, P.L., Essential oil of Elettariopsis elan C.K. Lim, Flavour Fragr. J., 2006, 21, 3, 562-564, https://doi.org/10.1002/ffj.1654 . [all data]

Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

Mookdasanit, Tamura, et al., 2003
Mookdasanit, J.; Tamura, H.; Yoshizawa T.; Tokunaga T.; Nakanishi, K., Trace Volatile Compounds in Essential Oil of Citrus Sudachi by Means of Modified Solvent Extraction Method, Food Sci Technol. Res., 2003, 9, 1, 54-61, https://doi.org/10.3136/fstr.9.54 . [all data]

Zrira, Elamrani, et al., 2003
Zrira, S.; Elamrani, A.; Benjilali, B., Chemical composition of the essential oil of Pistacia lentiscus L. from Morocco - a seasonal variation, Flavour Fragr. J., 2003, 18, 6, 475-480, https://doi.org/10.1002/ffj.1221 . [all data]

Orav, Kailas, et al., 2002
Orav, A.; Kailas, T.; Müürisepp, M., Composition of blackcurrant aroma isolated from leaves, buds, and berries of Ribes nigrum L., Proc. Est. Acad. Sci. Chem., 2002, 51, 4, 225-234. [all data]

Kasali, Oyedeji, et al., 2001
Kasali, A.A.; Oyedeji, A.O.; Ashilokun, A.O., Volatile leaf oil constituents of Cymbopogon citratus (DC) Stapf, Flavour Fragr. J., 2001, 16, 5, 377-378, https://doi.org/10.1002/ffj.1019 . [all data]

Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

Stashenko, Cervantes, et al., 1998
Stashenko, E.E.; Cervantes, M.; Combariza, Y.; Martínez, J.R., HRGC-FID-MSD Analysis of the Secondary Metabolites Obtained by Different Extraction Methods from Lepechinia schiedeana, and Evaluation of its Antioxidant Activity in vitro in 20th International Symposium on Capillary Chromatography, 1998, 1-11. [all data]

Shuichi, Masazumi, et al., 1996
Shuichi, H.; Masazumi, N.; Hiromu, K.; Kiyoshi, F., Comparison of volatile compounds berween the crude drugs, Onji-tsutsu and Onji-niki, Nippon nogei kagaku kaishi, 1996, 70, 2, 151-160. [all data]

Stashenko, Puertas, et al., 1996
Stashenko, E.E.; Puertas, M.A.; Combariza, M.Y., Volatile secondary metabolites from Spilanthes americana obtained by simultaneous steam distillation--solvent extraction and supercritical fluid extraction, J. Chromatogr. A, 1996, 752, 1-2, 223-232, https://doi.org/10.1016/S0021-9673(96)00480-3 . [all data]

Kollmannsberger, Nitz, et al., 1992
Kollmannsberger, H.; Nitz, S.; Drawert, F., UBer die Aromastoffzusammensetzung von Hochdruckextrakten. I. Pfeffer (Piper nigrum, Var. muntok), Z. Lebensm. Unters Forsch., 1992, 194, 6, 545-551, https://doi.org/10.1007/BF01185481 . [all data]

Wyllie, Brophy, et al., 1990
Wyllie, S.G.; Brophy, J.J.; Sarafis, V.; Hobbs, M., Volatile Components of the Fruit of Pistacia Lentiscus, J. Food. Sci., 1990, 55, 5, 1325-1326, https://doi.org/10.1111/j.1365-2621.1990.tb03926.x . [all data]

Stancher and Pertoldi, 1967
Stancher, B.; Pertoldi, M.G., Characterization of commercial materials used in synthetic essential oil production. Identification and gas-chromatographic determination of impurities, Rassegna chimica, 1967, 19, 3, 99-109. [all data]


Notes

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