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Fenchone


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5 MSVF-5 MSCP-Sil 5 CBDB-1-MS
Column length (m) 30.60.60.30.60.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (mum) 0.250.250.250.260.25
Tstart (C) 35.30.30.45.30.
Tend (C) 300.260.260.280.200.
Heat rate (K/min) 3.2.2.3.2.
Initial hold (min) 5.   4.
Final hold (min) 15.28.28.22.35.
I 1084.1090.1091.1069.1063.
ReferenceKotowska, Zalikowski, et al., 2012Leffingwell and Alford, 2011Leffingwell and Alford, 2011Mothana, Hasson, et al., 2011Takeoka, Hobbs, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-5 MSZB-5DB-1
Column length (m) 25.30.30.30.50.
Carrier gas HeliumHeliumHelium He
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (mum) 0.330.250.250.250.25
Tstart (C) 60.50.60.60.95.
Tend (C) 240.230.200.220.240.
Heat rate (K/min) 3.3.4.4.4.
Initial hold (min)  10. 5. 
Final hold (min) 7.10.20.20. 
I 1088.1088.1085.1090.1074.
ReferenceMaridass, 2009Adams, Beauchamp, et al., 2007Araque, Rojas, et al., 2007Mohottalage, Tabacchi, et al., 2007Pala-Paul, Brophy, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-52DB-1HP-5MSHP-5MS
Column length (m) 60.50.50.30.30.
Carrier gas  HeliumN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.50.95.60.60.
Tend (C) 250.240.240.280.280.
Heat rate (K/min) 5.3.4.3.4.
Initial hold (min)      
Final hold (min)      
I 1075.1087.1081.1052.1089.
ReferenceSalehi, Asghari, et al., 2007Ozcan, Chalchat, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pitarokili, Tzakou, et al., 2006Sajjadi, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1HP-1DB-1HP-5MS
Column length (m) 60.30.50.50.30.
Carrier gas HeliumHeHe He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.50.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 250.250.250.240.280.
Heat rate (K/min) 5.4.2.3.3.
Initial hold (min)  1.   
Final hold (min) 10.10.60.  
I 1073.1057.1075.1060.1087.
ReferenceSonboli, Mirjalili, et al., 2006Wong, Sivasothy, et al., 2006Bendimerad and Bendiab, 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Malencic, Couladis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5RSL-200RSL-200CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas  HeH2H2He
Substrate      
Column diameter (mm) 0.320.2490.320.320.25
Phase thickness (mum) 0.250.250.250.250.39
Tstart (C) 50.60.40.40.60.
Tend (C) 200.300.280.280.220.
Heat rate (K/min) 5.3.6.6.5.
Initial hold (min) 5. 5.5. 
Final hold (min)   5.5. 
I 1093.1085.1078.1080.1071.
ReferenceWang, Guo, et al., 2004Woerdenbag, Windono, et al., 2004Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Khanavi, Hadjiakhoondi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5HP-5HP-5
Column length (m) 30.50.25.30.30.
Carrier gas HeliumN2N2He 
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum)  0.250.250.25 
Tstart (C) 70.95.50.60.50.
Tend (C) 210.240.250.275.200.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min)      
Final hold (min) 60. 10.  
I 1087.1076.1088.1087.1090.
ReferenceMookdasanit, Tamura, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Zrira, Elamrani, et al., 2003Ghannadi, Sajjadi, et al., 2002Isidorov and Jdanova, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5OV-101DB-1DB-5MSDB-5MS
Column length (m) 60.50.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.50.250.250.25
Tstart (C) 50.50.50.60.60.
Tend (C) 240.250.250.270.240.
Heat rate (K/min) 5.2.4.3.3.
Initial hold (min) 3. 5.  
Final hold (min) 10.    
I 1099.1066.1070.1086.1086.
ReferenceKim and Lee, 2002Orav, Kailas, et al., 2002Yamini, Sefidkon, et al., 2002Zoghbi, Andrade, et al., 2002Cherchi, Deidda, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101HP-5 MSSPB-1HP-5DB-1
Column length (m) 50.30.30.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.20.250.20.250.25
Phase thickness (mum)  0.250.2 0.25
Tstart (C) 50.50.80.80.40.
Tend (C) 250.250.300.200.260.
Heat rate (K/min) 2.5.5.9.2.
Initial hold (min)  2.3. 5.
Final hold (min)  5. 10.2.
I 1064.1078.1088.1083.1067.
ReferenceOrav and Kann, 2001Shang, Hu, et al., 2001Fraternale, Giamperi, et al., 2000Lis-Balchin and Roth, 2000Senatore, Napolitano, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5HP-1OV-101DB-1
Column length (m) 25.30.60.25.60.
Carrier gas H2HeHe He
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (mum) 0.170.250.25 0.25
Tstart (C) 40.40.50.50.50.
Tend (C) 260.250.280.200.250.
Heat rate (K/min) 3.2.4.5.2.5
Initial hold (min) 5.5.5. 5.
Final hold (min)  60.   
I 1058.1069.1086.1080.1076.
ReferenceLopes, Koketsu, et al., 1999Porta, Porcedda, et al., 1999Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998Stashenko, Puertas, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1Methyl SiliconeOV-101OV-101SE-54
Column length (m) 50.25.50.50.30.
Carrier gas N2   Hydrogen
Substrate      
Column diameter (mm) 0.270.500.250.250.25
Phase thickness (mum) 0.2   0.25
Tstart (C) 80.60.80.80.60.
Tend (C) 240.220.200.200.250.
Heat rate (K/min) 3.5.2.2.2.
Initial hold (min)     5.
Final hold (min)     2.
I 1072.1075.1072.1072.1083.
ReferenceRamanoelina, Viano, et al., 1994Mallavarapu, Ramesh, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase BP-1
Column length (m) 25.
Carrier gas  
Substrate  
Column diameter (mm) 0.33
Phase thickness (mum)  
Tstart (C) 45.
Tend (C) 180.
Heat rate (K/min) 3.
Initial hold (min) 3.
Final hold (min)  
I 1067.
ReferenceWyllie, Brophy, et al., 1990
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kotowska, Zalikowski, et al., 2012
Kotowska, U.; Zalikowski, M.; Isidorov, V.A., HS-SPME/GC-MS analysis of volatile and semi-volatile organic compounds emitted from municipal sewage sludge, Environ. Monit. Asses., 2012, 184, 5, 2893-2907, https://doi.org/10.1007/s10661-011-2158-8 . [all data]

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Mothana, Hasson, et al., 2011
Mothana, R.A.A.; Hasson, S.S.; Schultze, W.; Mowitz, A.; Lindequist, U., Phytochemical composition and in vitro antimicrobial and antioxidant activities of essential oils of three endemic Soqotraen Boswellia species, Food Chem., 2011, 126, 3, 1149-1154, https://doi.org/10.1016/j.foodchem.2010.11.150 . [all data]

Takeoka, Hobbs, et al., 2010
Takeoka, G.R.; Hobbs, C.; Byeoung-Soo, P., Volatile constituents of the aerial parts of Salvia apiana Jepson, J. Essential Oil. Res., 2010, 22, 3, 241-244, https://doi.org/10.1080/10412905.2010.9700314 . [all data]

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Sonboli, Mirjalili, et al., 2006
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Wong, Sivasothy, et al., 2006
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Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

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Woerdenbag, Windono, et al., 2004
Woerdenbag, H.J.; Windono, T.; Bos, R.; Riswan, S.; Quax, W.J., Composition of the essential oils of Kaempferia rotunda L. and Kaempferia angustifolia Roscoe rhizomes from Indonesia, Flavour Fragr. J., 2004, 19, 2, 145-148, https://doi.org/10.1002/ffj.1284 . [all data]

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Yamini, Sefidkon, et al., 2002
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Zoghbi, Andrade, et al., 2002
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Cherchi, Deidda, et al., 2001
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Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

Shang, Hu, et al., 2001
Shang, C.; Hu, Y.; Deng, C.; Hu, K., Rapid determination of volatile constituents of Michelia alba flowers by gas chromatography - mass spectrometry with solid-phase microextraction, J. Chromatogr. A, 2001, 942, 1-2, 283-288, https://doi.org/10.1016/S0021-9673(01)01382-6 . [all data]

Fraternale, Giamperi, et al., 2000
Fraternale, D.; Giamperi, L.; Ricci, D.; Manunta, A., Composition of the essential oil of Peucedanum verticillare, Biochem. Syst. Ecol., 2000, 28, 2, 143-147, https://doi.org/10.1016/S0305-1978(99)00049-6 . [all data]

Lis-Balchin and Roth, 2000
Lis-Balchin, M.; Roth, G., Composition of the essential oils of Pelargonium odoratissimum, P. exstipulatum, and P. x fragrans (Geraniaceae) and their bioactivity, Flavour Fragr. J., 2000, 15, 6, 391-394, https://doi.org/10.1002/1099-1026(200011/12)15:6<391::AID-FFJ929>3.0.CO;2-W . [all data]

Senatore, Napolitano, et al., 2000
Senatore, F.; Napolitano, F.; Ozcan, M., Composition and antibacterial activity of the essential oil from Crithmum maritimum L. (Apiaceae) growing wild in Turkey, Flavour Fragr. J., 2000, 15, 3, 186-189, https://doi.org/10.1002/1099-1026(200005/06)15:3<186::AID-FFJ889>3.0.CO;2-I . [all data]

Lopes, Koketsu, et al., 1999
Lopes, D.; Koketsu, M.; Carauta, J.P.P.; de Oliveira, R.R.; Kaplan, M.A.C., Chemical composition of Pourouma guianensis Aublet essential oils, Flavour Fragr. J., 1999, 14, 4, 233-236, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<233::AID-FFJ813>3.0.CO;2-L . [all data]

Porta, Porcedda, et al., 1999
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Stashenko, Cervantes, et al., 1998
Stashenko, E.E.; Cervantes, M.; Combariza, Y.; Martínez, J.R., HRGC-FID-MSD Analysis of the Secondary Metabolites Obtained by Different Extraction Methods from Lepechinia schiedeana, and Evaluation of its Antioxidant Activity in vitro in 20th International Symposium on Capillary Chromatography, 1998, 1-11. [all data]

Zollo, Biyiti, et al., 1998
Zollo, P.H.A.; Biyiti, L.; Tchoumbougnang, F.; Menut, C.; Lamaty, G.; Bouchet, Ph., Aromatic plants of tropical central Africa. Part XXXII. Chemical composition and antifungal activity of thirteen essential oils from aromatic plants of Cameroon, Flavour Fragr. J., 1998, 13, 2, 107-114, https://doi.org/10.1002/(SICI)1099-1026(199803/04)13:2<107::AID-FFJ701>3.0.CO;2-G . [all data]

Stashenko, Puertas, et al., 1996
Stashenko, E.E.; Puertas, M.A.; Combariza, M.Y., Volatile secondary metabolites from Spilanthes americana obtained by simultaneous steam distillation--solvent extraction and supercritical fluid extraction, J. Chromatogr. A, 1996, 752, 1-2, 223-232, https://doi.org/10.1016/S0021-9673(96)00480-3 . [all data]

Ramanoelina, Viano, et al., 1994
Ramanoelina, P.A.R.; Viano, J.; Bianchini, J.-P.; Gaydou, E.M., Occurrence of various chemotypes in Niaouli (Melaleuca quinquenervia) essential oils from Madagascar using multivariate statistical analysis, J. Agric. Food Chem., 1994, 42, 5, 1177-1182, https://doi.org/10.1021/jf00041a024 . [all data]

Mallavarapu, Ramesh, et al., 1993
Mallavarapu, G.R.; Ramesh, S.; Kaul, P.N.; Battacharya, A.K.; Rao, B.R.R., The essential oil of Hyptis suaveolens (L.) Poit., J. Essent. Oil Res., 1993, 5, 3, 321-323, https://doi.org/10.1080/10412905.1993.9698230 . [all data]

Tamura, Yang, et al., 1993
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Kollmannsberger, Nitz, et al., 1992
Kollmannsberger, H.; Nitz, S.; Drawert, F., UBer die Aromastoffzusammensetzung von Hochdruckextrakten. I. Pfeffer (Piper nigrum, Var. muntok), Z. Lebensm. Unters Forsch., 1992, 194, 6, 545-551, https://doi.org/10.1007/BF01185481 . [all data]

Wyllie, Brophy, et al., 1990
Wyllie, S.G.; Brophy, J.J.; Sarafis, V.; Hobbs, M., Volatile Components of the Fruit of Pistacia Lentiscus, J. Food. Sci., 1990, 55, 5, 1325-1326, https://doi.org/10.1111/j.1365-2621.1990.tb03926.x . [all data]


Notes

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