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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5MSDB-5MSDB-5Equity-5MS
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.40.60.50.
Tend (C) 270.200.200.240.250.
Heat rate (K/min) 15.4.4.3.3.
Initial hold (min)  1.1.  
Final hold (min) 15.10.10. 10.
I 1081.1071.1071.1104.1105.
ReferenceZaikin, 2010Cho, Namgung, et al., 2008Cho, Namgung, et al., 2008Baccouri, Ben Temime, et al., 2007Belsito E.L., Carbone C., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5SPB-5DB-5HP-5
Column length (m) 30.25.60.30.30.
Carrier gas HeHe HeN2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.251.0.250.25
Tstart (C) 40.60.40.60.50.
Tend (C) 200.240.230.240.220.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min) 1.2.2. 10.
Final hold (min) 10. 10.  
I 1104.1095.1106.1103.1106.
ReferenceCho I.H., Lee S.M., et al., 2007Dehghan, Solaimanian, et al., 2007Engel and Ratel, 2007Flamini, Cioni, et al., 2007Flamini, Tebano, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSDB-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.35.35.60.60.
Tend (C) 225.225.225.240.240.
Heat rate (K/min) 10.10.10.3.3.
Initial hold (min) 5.5.5.  
Final hold (min) 25.25.25.  
I 1108.1108.1102.1104.1104.
ReferenceLozano P.R., Drake M., et al., 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Miracle E.R., et al., 2007Maccioni, Baldini, et al., 2007Maccioni, Baldini, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1HP-5ZB-5HP-5MS
Column length (m) 60.60.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.220.250.320.25
Phase thickness (mum) 1.0.250.250.50.25
Tstart (C) 40.60.50.40.60.
Tend (C) 260.230.250.265.280.
Heat rate (K/min) 4.2.4.7.4.
Initial hold (min) 2. 4. 5.
Final hold (min) 10.35.10.5. 
I 1107.1081.1103.1111.1102.
ReferenceMethven L., Tsoukka M., et al., 2007Paolini, Muselli, et al., 2007Quijano, Salamanca, et al., 2007Ruiz Perez-Cacho, Mahattanatawee, et al., 2007Saroglou, Marin, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.251.
Tstart (C) 60.50.80.60.50.
Tend (C) 240.250.300.220.290.
Heat rate (K/min) 3.3.4.3.10.
Initial hold (min)     1.
Final hold (min)  10.  10.
I 1098.1104.1105.31104.1112.
ReferenceTelascrea, de Araujo, et al., 2007Yu, Liao, et al., 2007Zeng, Zhao, et al., 2007Bastos, Ishimoto, et al., 2006Bylaite and Meyer, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSMega 5MSSPB-5DB-5
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.251.0.25
Tstart (C) 60.40.60.40.60.
Tend (C) 280.200.240.230.240.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)  1. 5.3.
Final hold (min)  10. 5.5.
I 1102.1104.1080.1105.1102.
ReferenceChorianopoulos N., Evergets E., et al., 2006Cho, Kim, et al., 2006Condurso, Verzera, et al., 2006Deport, Ratel, et al., 2006Dob, Dahmane, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5MSHP-5MS
Column length (m) 30.30.30.20.30.
Carrier gas N2HeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.260.260.240.280.
Heat rate (K/min) 5.3.3.5.3.
Initial hold (min) 10.  4. 
Final hold (min)    15. 
I 1105.1105.1104.1105.1100.
ReferenceFlamini, Tebano, et al., 2006Javidnia, Miri, et al., 2006Javidnia K., Miri R., et al., 2006Kallio, Jussila, et al., 2006Kukic J., Petrovic S., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5DB-1HP-5HP-5MS
Column length (m) 50.30.30.25.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.280.240.240.280.
Heat rate (K/min) 4.3.4.4.4.
Initial hold (min) 5.   5.
Final hold (min) 30.    
I 1097.1101.1128.1102.1107.
ReferenceMahadevan and Farmer, 2006Pavlovic, Tzakou, et al., 2006Rezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006Saroglou, Dorizas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5MSHP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.40.50.80.
Tend (C) 285.300.200.220.300.
Heat rate (K/min) 4.34.5.3.4.
Initial hold (min)  5.5.  
Final hold (min)   45.20. 
I 1090.1101.1100.1103.1106.5
ReferenceVujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006Whetstine M.E.C., Drake M.A., et al., 2006Xian Q., Chen H., et al., 2006Zhao C.X., Li, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBCP Sil 5 CBDB-5SE-54
Column length (m) 30.25.25.30.50.
Carrier gas HeH2HeH2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.40.250.27
Tstart (C) 60.80.80.35.50.
Tend (C) 250.270.270.270.300.
Heat rate (K/min) 10.10.10.5.5.
Initial hold (min) 2.    
Final hold (min) 10.  20. 
I 1110.1076.1076.1102.1099.
ReferenceZhao J.Y., Liu J.M., et al., 2006Ziegenbein, Hanssen, et al., 2006Ziegenbein, Hanssen, et al., 2006, 2Alves, Pinto, et al., 2005Brantner, Pfeifhofer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSHP-5MDN-5CP-Sil 8CB-MS
Column length (m) 30.30.30.30.0.
Carrier gas He N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.50.40.
Tend (C) 200.200.220.250.280.
Heat rate (K/min) 5.10.5.3.4.
Initial hold (min) 5.3.10. 2.
Final hold (min) 45.20.  5.
I 1098.1098.1104.1103.1109.
ReferenceCarunchia Whetstine, Croissant, et al., 2005Carunchia Whetstine, Croissant, et al., 2005Celik, Gokturk, et al., 2005Dugo, Mondello, et al., 2005Elmore, Cooper, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-1BP-1HP-5HP-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (mum) 1.0.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 250.250.220.220.220.
Heat rate (K/min) 7.3.2.5.5.
Initial hold (min) 10.  10.10.
Final hold (min) 5.20.20.  
I 1128.1083.1082.1104.1104.
ReferenceEstevez, Ventanas, et al., 2005Fanciullino, Gancel, et al., 2005Ferrari, Tomi, et al., 2005Flamini, Luigi Cioni, et al., 2005Flamini, Luigi Cioni, et al., 2005, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5HP-5HP-5
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.251.050.250.250.25
Tstart (C) 40.35.60.50.50.
Tend (C) 250.220.260.250.250.
Heat rate (K/min) 3.8.3.4.4.
Initial hold (min)  15. 5.5.
Final hold (min) 20.5. 15.15.
I 1083.1109.1105.1103.1101.
ReferenceGancel, Ollitrault, et al., 2005Insausti, Goñi, et al., 2005Javidnia, Miri, et al., 2005Mahattanatawee, Goodner, et al., 2005Mahattanatawee, Goodner, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5MSDB-5MSHP-5MSHP-5
Column length (m) 60.30.60.60.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.20.2
Phase thickness (mum) 0.250.250.250.251.
Tstart (C) 60.60.40.60.40.
Tend (C) 230.250.200.200.280.
Heat rate (K/min) 2.4.2.2.5.
Initial hold (min)  2.   
Final hold (min) 35.20.20.10.5.
I 1081.1103.1104.1094.1105.
ReferencePaolini, Costa, et al., 2005Pino, Mesa, et al., 2005Seo and Baek, 2005Smadja, Rondeau, et al., 2005Solina, Baumgartner, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Mega 5MSDB-5MSDB-5HP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.20.250.250.320.25
Phase thickness (mum) 1.0.250.250.250.25
Tstart (C) 40.40.40.40.80.
Tend (C) 280.240.200.250.290.
Heat rate (K/min) 5.3.10.5.2.
Initial hold (min)  2.3.2. 
Final hold (min) 5. 20.5. 
I 1105.1098.1100.1085.1105.9
ReferenceSolina, Baumgartner, et al., 2005Verzera, Trozzi, et al., 2005Whetstine, Cadwallader, et al., 2005Wu, Zorn, et al., 2005Zhao, Liang, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSSPB-1HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.80.60.70.60.
Tend (C) 290.290.280.220.220.
Heat rate (K/min) 4.6.3.3.5.
Initial hold (min)     10.
Final hold (min)    15. 
I 1104.81104.21103.1081.1107.
ReferenceZhao, Liang, et al., 2005Zhao, Liang, et al., 2005Aligiannis, Kalpoutzakis, et al., 2004Antunes, Sevinate-Pinto, et al., 2004Bertoli, Menichini, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5MSBPX-5RTX-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.220.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.50.45.60.
Tend (C) 220.280.300.300.240.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)   5.6. 
Final hold (min) 15.  10. 
I 1079.1102.1114.1103.1104.
ReferenceCavaleiro, Salgueiro, et al., 2004Chorianopoulos, Kalpoutzakis, et al., 2004Dickschat, Wenzel, et al., 2004Dugo, Mondello, et al., 2004Flamini, Bader, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5MSCP-Sil 8CB-MS
Column length (m) 30.30.30.30.60.
Carrier gas N2HeN2He 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.40.
Tend (C) 240.290.220.280.280.
Heat rate (K/min) 3.4.5.4.4.
Initial hold (min)   10.5.2.
Final hold (min)     5.
I 1104.1106.1103.1102.1105.
ReferenceFlamini, Cioni, et al., 2004Flach A., Dondon R.C., et al., 2004Flamini, Luigi Cioni, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Hierro, de la Hoz, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5MSSPB-5SPB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum)  1.0.250.250.25
Tstart (C) 60.40.40.60.60.
Tend (C) 260.230.280.250.250.
Heat rate (K/min) 3.5.4.4.4.
Initial hold (min)  4.2.2.2.
Final hold (min)  10. 20.20.
I 1105.1101.1106.1102.1102.
ReferenceJavidnia, Miri, et al., 2004Mahajan, Goddik, et al., 2004Mardarowicz, Wianowska, et al., 2004Pino, Marbot, et al., 2004Pino, Marbot, et al., 2004, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSOptima 5HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.10.250.250.250.25
Tstart (C) -30.50.60.60.50.
Tend (C) 250.310.280.280.200.
Heat rate (K/min) 10.4.3.3.6.
Initial hold (min) 1.   1.5
Final hold (min) 5.  20.5.
I 1105.1104.1092.1107.1106.
ReferenceSiegmund and Murkovic, 2004Singer, Flach, et al., 2004Tzakou, Vagias, et al., 2004Vérité, Nacer, et al., 2004Weissbecker, Holighaus, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-1CP-Sil 8CB-MSHP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.40.40.60.
Tend (C) 200.240.250.280.220.
Heat rate (K/min) 4.3.3.4.5.
Initial hold (min) 5.  2.10.
Final hold (min) 20.30.20.5. 
I 1104.1103.1081.1108.1103.
ReferenceZheng, Kim, et al., 2004Bader, Caponi, et al., 2003Brat, Rega, et al., 2003Bruna, Hierro, et al., 2003Campeol, Flamini, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-1HP-1HP-1SPB-1
Column length (m) 30.50.50.50.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.20.20.25
Phase thickness (mum) 0.250.330.330.330.25
Tstart (C) 60.60.60.60.35.
Tend (C) 220.250.250.250.225.
Heat rate (K/min) 5.2.2.2.4.
Initial hold (min) 10.5.5.5.5.
Final hold (min)  20.20.20.20.
I 1103.1071.1067.1074.1078.
ReferenceCampeol, Flamini, et al., 2003Cavalli, Fernandez, et al., 2003Cavalli, Fernandez, et al., 2003Cavalli, Fernandez, et al., 2003Chisholm, Jell, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1SPB-1SPB-1HP-5
Column length (m) 30.25.25.25.30.
Carrier gas He   N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.35.35.35.60.
Tend (C) 225.225.225.225.220.
Heat rate (K/min) 4.4.4.4.5.
Initial hold (min) 5.10.10.10.10.
Final hold (min) 20.    
I 1082.1084.1084.1086.1103.
ReferenceChisholm, Jell, et al., 2003Chisholm, Wilson, et al., 2003Chisholm, Wilson, et al., 2003Chisholm, Wilson, et al., 2003Dural, Bagci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2N2HeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.240.240.220.
Heat rate (K/min) 5.5.3.3.5.
Initial hold (min) 10.10.  10.
Final hold (min)      
I 1103.1103.1104.1104.1103.
ReferenceEmilio Tomei, Manganelli, et al., 2003Ertugrul, Dural, et al., 2003Flamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2N2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.5
Tstart (C) 60.60.60.40.40.
Tend (C) 220.220.280.250.265.
Heat rate (K/min) 5.5.3.3.7.
Initial hold (min) 10.10.   
Final hold (min)    20.5.
I 1103.1104.1103.1083.1103.
ReferenceFlamini, Luigi Cioni, et al., 2003, 3Flamini, Luigi Cioni, et al., 2003, 4Fokialakis, Melliou, et al., 2003Gancel, Ollitrault, et al., 2003Högnadóttir and Rouseff, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5CP Sil 5 CB
Column length (m) 30.25.30.30.60.
Carrier gas  He  He
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (mum) 0.5 0.250.250.25
Tstart (C) 40.60.35.35.60.
Tend (C) 265.260.250.250.280.
Heat rate (K/min) 7.4.4.4.3.
Initial hold (min)   2.2.10.
Final hold (min) 5. 4.4.60.
I 1109.1104.1102.1102.1089.
ReferenceHögnadóttir and Rouseff, 2003Javidnia, Miri, et al., 2003Peterson and Reineccius, 2003Peterson and Reineccius, 2003, 2Pino, Almora, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5DB-1Mega 5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.330.250.250.251.
Tstart (C) 40.60.40.40.50.
Tend (C) 260.280.325.240.200.
Heat rate (K/min) 2.4.3.3.2.5
Initial hold (min) 5.5. 2. 
Final hold (min) 20.    
I 1101.1102.1080.21098.1103.2
ReferenceSenatore, Rigano, et al., 2003Skaltsa, Demetzos, et al., 2003Sun and Stremple, 2003Verzera, Trozzi, et al., 2003Xu, van Stee, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBPX-5HP-5MSHP-5MSCP Sil 8 CB
Column length (m) 30.50.30.30.60.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.50.250.250.25
Tstart (C) 60.60.60.50.40.
Tend (C) 275.250.300.280.250.
Heat rate (K/min) 4.4.3.3.4.
Initial hold (min)  5. 5.8.
Final hold (min)  20.  10.
I 1103.1118.1104.1100.1114.
ReferenceAfsharypuor and Suleimany, 2002Bredie, Mottram, et al., 2002Couladis, Chinou, et al., 2002Demetzos, Angelopoulou, et al., 2002Duckham, Dodson, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5HP-5HP-5CP Sil 5 CB
Column length (m) 60.30.30.30.50.
Carrier gas HeHeN2 H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.15
Tstart (C) 40.60.60.60.40.
Tend (C) 250.240.220.280.300.
Heat rate (K/min) 4.3.5.3.4.
Initial hold (min) 8. 10.5.3.
Final hold (min) 10.    
I 1118.1103.1104.1097.1103.
ReferenceDuckham, Dodson, et al., 2002Flamini, Cioni, et al., 2002Flamini, Cioni, et al., 2002, 2Fokialakis, Magiatis, et al., 2002Heinrich, Pfeifhofer, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5RTX-5CP Sil 8 CB
Column length (m) 25.50.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 70.60.60.45.40.
Tend (C) 275.220.280.300.250.
Heat rate (K/min) 4.2.3.3.4.
Initial hold (min)   5.6.8.
Final hold (min)  20. 10.10.
I 1102.1082.1102.1105.1104.
ReferenceJavidnia, Miri, et al., 2002Lota, de Rocca Serra, et al., 2002Magiatis, Skaltsounis, et al., 2002Mondello, Zappia, et al., 2002Oruna-Concha, Ames, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5CP Sil 5 CBHP-5Petrocol DHCP-Sil 8CB-MS
Column length (m) 30.50.30.100.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.40.250.50.25
Tstart (C) 60.60.60.60.40.
Tend (C) 250.280.280.180.280.
Heat rate (K/min) 4.3.3.4.4.
Initial hold (min) 2.10.5.8.2.
Final hold (min) 20.60. 2. 
I 1102.1085.1101.1098.1108.
ReferencePino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Aligiannis, Kalpoutzakis, et al., 2001Alonzo, Saiano, et al., 2001Bruna, Hierro, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-1SPB-SulfurSPB-1
Column length (m) 30.30.60.30.30.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (mum) 0.250.251.4.4.
Tstart (C) 60.35.40.40.45.
Tend (C) 260.200.220.200.240.
Heat rate (K/min) 3.10.2.4.5.
Initial hold (min)  5.5.12.513.
Final hold (min) 10.30.  5.
I 1104.1099.1083.1084.81089.
ReferenceCouladis, Baziou, et al., 2001Karagül-Yüceer, Drake, et al., 2001Kim, 2001de Lacy Costello, Evans, et al., 2001Larráyoz, Addis, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1BP-1DB-5BPX-5
Column length (m) 30.50.50.30.50.
Carrier gas  HeHeH2He
Substrate      
Column diameter (mm) 0.320.220.220.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.35.
Tend (C) 240.220.220.240.250.
Heat rate (K/min) 7.2.2.3.4.
Initial hold (min)     3.
Final hold (min) 5.   10.
I 1130.1082.1082.1102.1116.
ReferenceLin and Rouseff, 2001Lota, Serra, et al., 2001Lota, Serra, et al., 2001Nogueira, Bittrich, et al., 2001Oruna-Concha, Duckham, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5BPX-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 50.50.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.250.250.250.40.4
Tstart (C) 35.35.35.60.60.
Tend (C) 250.250.250.280.280.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min) 3.3.3.10.10.
Final hold (min) 10.10.10.60.60.
I 1118.1108.1118.1089.1089.
ReferenceOruna-Concha, Duckham, et al., 2001Oruna-Concha, Duckham, et al., 2001Oruna-Concha, Duckham, et al., 2001Pino and Marbot, 2001Pino, Marbot, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5CP Sil 8 CBHP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 50.60.60.40.50.
Tend (C) 200.280.180.280.280.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 1.5.8.2.5.
Final hold (min)   2.  
I 1105.1102.1096.1108.1103.
ReferenceShalit, Katzir, et al., 2001Skaltsa, Mavrommati, et al., 2001Alonzo, Bosco, et al., 2000Elmore, Mottram, et al., 2000Lazari, Skaltsa, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-5SE-30HP-5HP-5
Column length (m) 30.10.50.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.10.20.250.25
Phase thickness (mum) 0.250.1 0.250.25
Tstart (C) 50.50.50.50.70.
Tend (C) 280.350.250.280.230.
Heat rate (K/min) 4.12.36.4.2.
Initial hold (min) 5.  5. 
Final hold (min)      
I 1103.1109.1088.1101.1107.
ReferenceLazari, Skaltsa, et al., 2000, 2Mondello, Zappia, et al., 2000Paramonov, Khalilova, et al., 2000Skaltsa, Lazari, et al., 2000Song, Sawamura, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Mega 5MSMega 5MSDB-1CP Sil 8 CB
Column length (m) 30.30.30.60.50.
Carrier gas N2HeHeN2 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.251. 
Tstart (C) 70.40.40.30.60.
Tend (C) 230.240.240.200.220.
Heat rate (K/min) 2.3.3.5.4.
Initial hold (min)  2.2. 5.
Final hold (min)    30.30.
I 1107.1098.1098.1088.1102.
ReferenceSong, Sawamura, et al., 2000, 2Verzera, la Rosa, et al., 2000Verzera, Trozzi, et al., 2000Wu, Wang, et al., 2000Chevance and Farmer, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5BP-1HP-1
Column length (m) 60.60.30.50.25.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.320.320.250.220.2
Phase thickness (mum) 1. 0.250.250.33
Tstart (C) -50.60.50.60.35.
Tend (C) 175.230.280.230.250.
Heat rate (K/min) 6.3.4.2.4.
Initial hold (min) 2. 5.  
Final hold (min)  5. 35.2.
I 1089.91084.1103.1082.1081.4
ReferenceHelmig, Klinger, et al., 1999Javidnia and Shafiee, 1999Lazari, Skaltsa, et al., 1999Lota, Serra, et al., 1999Siegmund and Pfannhauser, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5OV-1OV-1BPX-5SPB-1
Column length (m) 30.20.20.50.60.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (mum) 0.250.30.30.500.25
Tstart (C) 35.45.45.40.40.
Tend (C) 250.220.220.280.200.
Heat rate (K/min) 5.310.10.4.4.
Initial hold (min)  5.5.  
Final hold (min) 2.10.10. 20.
I 1104.21090.1092.1119.1075.
ReferenceSiegmund and Pfannhauser, 1999Valero, Sanz, et al., 1999Valero, Sanz, et al., 1999Aaslyng, Elmore, et al., 1998Chen, Huang, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5DB-5DB-5BP-1
Column length (m) 60.30.30.30.25.
Carrier gas HeH2H2H2He
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 1.1.1.1. 
Tstart (C) 40.40.40.40.5.
Tend (C) 200.210.210.210.250.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min) 5.   5.
Final hold (min) 2.   30.
I 1104.1104.1106.1106.1082.
ReferenceVerdier-Metz., Coulon, et al., 1998Moio and Addeo, 1998Moio and Addeo, 1998Moio and Addeo, 1998Sinyinda and Gramshaw, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1DB-5SE-30DB-5
Column length (m) 50.30.60.50.30.
Carrier gas He   H2
Substrate      
Column diameter (mm) 0.220.250.330.320.32
Phase thickness (mum) 0.251.0.250.251.
Tstart (C) 60.-50.-50.50.40.
Tend (C) 230.180.180.250.220.
Heat rate (K/min) 2.6.6.4.3.
Initial hold (min)      
Final hold (min) 35.    
I 1083.1082.51103.31080.1103.
ReferenceMariotti, Costa, et al., 1997Helmig, Pollock, et al., 1996Helmig, Pollock, et al., 1996Misharina and Golovnya, 1996Moio L., Rillo L., et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5Methyl SiliconeDB-1DB-1
Column length (m) 30.30.25.60.60.
Carrier gas H2H2HeH2 
Substrate      
Column diameter (mm) 0.320.320.20.250.25
Phase thickness (mum) 1.1.0.30.250.25
Tstart (C) 40.40.40.50.35.
Tend (C) 220.220.200.250.280.
Heat rate (K/min) 3.3.2.2.52.
Initial hold (min)    5.10.
Final hold (min)     10.
I 1104.1103.1085.1082.1084.
ReferenceMoio L., Rillo L., et al., 1996Moio L., Rillo L., et al., 1996Píry, Príbela, et al., 1995Stashenko, Villa, et al., 1995Specht and Baltes, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101OV-101OV-101OV-101
Column length (m) 30.50.50.50.50.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.310.250.250.32
Phase thickness (mum)  0.5  0.50
Tstart (C) 50.50.80.80.50.
Tend (C) 250.250.200.200.250.
Heat rate (K/min) 4.4.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1105.1083.1084.1085.1086.
ReferenceGómez, Ledbetter, et al., 1993Misharina, Golovnya, et al., 1992Yang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Misharina, Aerove, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase DB-1DB-5CP Sil 5 CBOV-101Apiezon M
Column length (m) 60.0.3225.2.51.5
Carrier gas  H2  N2
Substrate    Gas-Chrom QCelite 545
Column diameter (mm) 0.321.0.22  
Phase thickness (mum)      
Tstart (C) 50.30.70.50.75.
Tend (C) 250.180.205.220.200.
Heat rate (K/min) 4.1.54.2.6.
Initial hold (min) 0.15.   
Final hold (min)      
I 1082.1106.1091.1085.1072.
ReferenceFlath, Light, et al., 1990Guichard and Souty, 1988Hendriks and Bruins, 1983Nixon, Wong, et al., 1979Golovnya and Uraletz, 1971
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase Apiezon MApiezon MSE-30
Column length (m) 1.51.5 
Carrier gas N2N2 
Substrate Celite 545Celite 545Celite
Column diameter (mm)    
Phase thickness (mum)    
Tstart (C) 75.75.75.
Tend (C) 200.200.228.
Heat rate (K/min) 6.6. 
Initial hold (min)    
Final hold (min)    
I 1073.1076.1091.
ReferenceGolovnya and Uraletz, 1971Golovnya and Uraletz, 1971van den Dool and Kratz, 1963
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References