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Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxDB-WaxSupelcowax-10DB-WaxDB-Wax
Column length (m) 30.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25  0.250.25
Tstart (C) 40.40.35.40.40.
Tend (C) 190.200.200.200.200.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min)  2.5.5.5.
Final hold (min) 5. 20.  
I 1382.1390.1397.1396.1400.
ReferenceMahmood, Kaul, et al., 2004Umano, Hagi, et al., 1994Wong and Teng, 1994Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedCapillaryCapillaryCapillary
Active phase DB-WaxPEG-20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 60.5.559.150.150.
Carrier gas HeN2 He 
Substrate  Celite   
Column diameter (mm) 0.25 0.250.640.64
Phase thickness (mum)      
Tstart (C) 40.70.70.50.50.
Tend (C) 200.175.190.170.170.
Heat rate (K/min) 2.10.1.1.1.
Initial hold (min) 10.9. 30.30.
Final hold (min)      
I 1392.1382.1400.1390.1390.
ReferenceUmano and Shibamoto, 1987Galt and MacLeod, 1984Palma-Fleming and Kepner, 1983Buttery, Kamm, et al., 1982Buttery, Ling, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 150.50.50.70.70.
Carrier gas He  N2N2
Substrate      
Column diameter (mm) 0.640.280.280.280.28
Phase thickness (mum)      
Tstart (C) 50.80.80.80.80.
Tend (C) 170.200.200.200.200.
Heat rate (K/min) 1.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1390.1367.1369.1374.1380.
ReferenceButtery, Seifert, et al., 1982Toda, Yamaguchi, et al., 1982Toda, Yamaguchi, et al., 1982Yamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 50.50.30.30.50.
Carrier gas N2N2N2N2He
Substrate      
Column diameter (mm) 0.280.280.260.260.28
Phase thickness (mum)      
Tstart (C) 80.80.70.70.70.
Tend (C) 200.200.170.170.190.
Heat rate (K/min) 2.2.3.3.2.
Initial hold (min)      
Final hold (min)      
I 1348.1350.1393.1400.1386.
ReferenceYamaguchi and Shibamoto, 1979Yamaguchi and Shibamoto, 1979Spencer, Pangborn, et al., 1978Spencer, Pangborn, et al., 1978Tressl, Friese, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mahmood, Kaul, et al., 2004
Mahmood, U.; Kaul, V.K.; Acharya, R., Volatile constituents of Capillipedium parviflorum, Phytochemistry, 2004, 65, 14, 2163-2166, https://doi.org/10.1016/j.phytochem.2004.04.003 . [all data]

Umano, Hagi, et al., 1994
Umano, K.; Hagi, Y.; Tamura, T.; Shoji, A.; Shibamoto, T., Identification of volatile compounds isolated from round kumquat (Fortunella japonica Swingle), J. Agric. Food Chem., 1994, 42, 9, 1888-1890, https://doi.org/10.1021/jf00045a011 . [all data]

Wong and Teng, 1994
Wong, K.C.; Teng, Y.E., Volatile Components of Mimusops elengi L. Flowers, J. Essent. Oil Res., 1994, 6, 5, 453-458, https://doi.org/10.1080/10412905.1994.9698425 . [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

Umano and Shibamoto, 1987
Umano, K.; Shibamoto, T., Analysis of headspace volatiles from overheated beef fat, J. Agric. Food Chem., 1987, 35, 1, 14-18, https://doi.org/10.1021/jf00073a004 . [all data]

Galt and MacLeod, 1984
Galt, A.M.; MacLeod, G., Headspace sampling of cooked beef aroma using Tenax GC, J. Agric. Food Chem., 1984, 32, 1, 59-64, https://doi.org/10.1021/jf00121a016 . [all data]

Palma-Fleming and Kepner, 1983
Palma-Fleming, H.A.; Kepner, R.E., Volatile components of California live oak, Quercus agrifolia, Phytochemistry, 1983, 22, 6, 1503-1505, https://doi.org/10.1016/S0031-9422(00)84047-9 . [all data]

Buttery, Kamm, et al., 1982
Buttery, R.G.; Kamm, J.A.; Ling, L.C., Volatile components of alfalfa flowers and pods, J. Agric. Food Chem., 1982, 30, 4, 739-742, https://doi.org/10.1021/jf00112a028 . [all data]

Buttery, Ling, et al., 1982
Buttery, R.G.; Ling, L.C.; Wellso, S.G., Oat leaf volatiles: possible insect attractants, J. Agric. Food Chem., 1982, 30, 4, 791-792, https://doi.org/10.1021/jf00112a045 . [all data]

Buttery, Seifert, et al., 1982
Buttery, R.G.; Seifert, R.M.; Ling, L.C.; Soderstrom, E.L.; Ogawa, J.M.; Turnbaugh, J.G., Additional aroma components of honeydew melon, J. Agric. Food Chem., 1982, 30, 6, 1208-1211, https://doi.org/10.1021/jf00114a051 . [all data]

Toda, Yamaguchi, et al., 1982
Toda, H.; Yamaguchi, K.; Shibamoto, T., Isolation and identification of banana-like aroma from banana shrub (Michellia figo Spreng), J. Agric. Food Chem., 1982, 30, 1, 81-84, https://doi.org/10.1021/jf00109a017 . [all data]

Yamaguchi and Shibamoto, 1981
Yamaguchi, K.; Shibamoto, T., Volatile constituents of green tea, Gyokuro (Camellia sinensis L. var Yabukita), J. Agric. Food Chem., 1981, 29, 2, 366-370, https://doi.org/10.1021/jf00104a035 . [all data]

Yamaguchi and Shibamoto, 1979
Yamaguchi, K.; Shibamoto, T., Volatile constituents of Castanopsis flower, J. Agric. Food Chem., 1979, 27, 4, 847-850, https://doi.org/10.1021/jf60224a025 . [all data]

Spencer, Pangborn, et al., 1978
Spencer, M.D.; Pangborn, R.M.; Jennings, W.G., Gas chromatographic and sensory analysis of volatiles from cling peaches, J. Agric. Food Chem., 1978, 26, 3, 725-732, https://doi.org/10.1021/jf60217a052 . [all data]

Tressl, Friese, et al., 1978
Tressl, R.; Friese, L.; Fendesack, F.; Köppler, H., Studies of the volatile composition of hops during storage, J. Agric. Food Chem., 1978, 26, 6, 1426-1430, https://doi.org/10.1021/jf60220a036 . [all data]


Notes

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