Octanal

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSHP-5 MSVF-5 MSVF-5 MSVF-5 MS
Column length (m) 60.30.60.60.30.
Carrier gas Helium HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.30.30.40.
Tend (C) 250.300.260.260.250.
Heat rate (K/min) 4.15.2.2.5.
Initial hold (min) 2.2.  3.
Final hold (min)  10.28.28.3.
I 1001.1011.1006.1006.1007.
ReferenceSrisajjalerwaja, Apichartsrangkoon, et al., 2012Xu, Han, et al., 2012Leffingwell and Alford, 2011Leffingwell and Alford, 2011Liu, Lu, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.70.50.70.70.
Tend (C) 260.290.240.290.290.
Heat rate (K/min) 4.5.4.5.5.
Initial hold (min)   2.  
Final hold (min) 5. 10. 10.
I 1004.1004.1000.1005.1003.
ReferenceMiyazawa, Marumoto, et al., 2011Lazarevic, Radulovic, et al., 2010Pino, Marquez, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSSLB-5 MSDB-5 MSDB-5 MSVF-5
Column length (m) 10.10.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.100.100.320.320.25
Phase thickness (μm) 0.100.100.250.250.25
Tstart (C) 50.50.40.40.60.
Tend (C) 250.250.230.250.300.
Heat rate (K/min) 10.10.6.6.10.
Initial hold (min)   2.2.2.
Final hold (min)   20.20.10.
I 1003.1004.1004.1005.1008.
ReferenceScandinaro, Tranchida, et al., 2010Scandinaro, Tranchida, et al., 2010Chen, Song, et al., 2009Chen, Song, et al., 2009Li and Zhao, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1RTX-5 MSHP-5 MSHP-5 MS
Column length (m) 60.50.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.220.250.250.25
Phase thickness (μm) 0.250.250.500.250.25
Tstart (C)  60.35.60.50.
Tend (C) 240.220.225.300.280.
Heat rate (K/min) 6.2.6.15.4.
Initial hold (min)   5.2. 
Final hold (min) 5.20.10.10. 
I 1007.980.1002.1011.1002.
ReferenceMallia, Escher, et al., 2009Ottavioli, Bighelli, et al., 2009Watcharananun, Cadwallader, et al., 2009Xu, Han, et al., 2009Zhao, Zeng, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1HP-1SE-52HP-5
Column length (m) 30.50.50.50.30.
Carrier gas HeliumHeliumHeliumHeliumN2
Substrate      
Column diameter (mm) 0.250.200.200.250.25
Phase thickness (μm) 0.250.330.330.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.250.250.280.220.
Heat rate (K/min) 3.2.2.3.5.
Initial hold (min)     10.
Final hold (min)  20.20.20. 
I 1001.1002.983.1008.1003.
ReferenceBastos, Ishimoto, et al., 2008Breme, Langle, et al., 2008Breme, Langle, et al., 2008Djarri, Medjroubi, et al., 2008Flamini, Tebano, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1HP-5HP-5HP-5 MS
Column length (m) 30.30.10.30.30.
Carrier gas HeliumHeHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.100.250.25
Phase thickness (μm) 1.00.250.400.250.25
Tstart (C) 60.30.40.50.50.
Tend (C) 250.210.280.280.250.
Heat rate (K/min) 5.5.20.5.6.5
Initial hold (min) 5. 1.1.1.5
Final hold (min)   1.1.10.
I 984.980.1010.1010.1001.
ReferenceFrerot, Velluz, et al., 2008Kumazawa, Itobe, et al., 2008Mildner-Szkudlarz and Jelen, 2008Saidana, Mahjoub, et al., 2008Thakeow, Angeli, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1RTX-5HP-5 MSVF-5MS5 % Phenyl methyl siloxane
Column length (m) 30.60.30.30.30.
Carrier gas Helium Helium He
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.251.0.250.251.
Tstart (C) 65.40.60.40.40.
Tend (C) 260.205.280.250.250.
Heat rate (K/min) 6.4.4.7.7.
Initial hold (min)  5.5. 10.
Final hold (min)  5.  5.
I 994.1004.999.998.1004.
ReferenceWang, Yi, et al., 2008Berdague, Tournayre, et al., 2007Capetanos, Saroglou, et al., 2007Ghiasvand, Setkova, et al., 2007Ramirez R. and Cava R., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5SPB-5CP Sil 5 CBHP-1
Column length (m) 30.30.60.25.50.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.32 0.2
Phase thickness (μm) 1.0.251. 0.5
Tstart (C) 40.60.40.80.60.
Tend (C) 250.320.230.270.250.
Heat rate (K/min) 7.10.3.10.2.
Initial hold (min) 10. 5.  
Final hold (min) 5.4.5. 120.
I 1004.999.1003.977.977.
ReferenceRamirez R. and Cava R., 2007Smelcerovic, Spiteller, et al., 2007Vasta, Ratel, et al., 2007Ayoub, Al-Azizi, et al., 2006Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1DB-1DB-15 % Phenyl methyl siloxane
Column length (m) 30.50.60.60.30.
Carrier gas N2He  Helium
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 70.60.70.70.60.
Tend (C) 230.250.230.230.280.
Heat rate (K/min) 2.2.2.2.3.
Initial hold (min) 2. 2.2. 
Final hold (min) 20.60.20.20.30.
I 1002.979.979.980.977.
ReferenceChoi, 2006Fernandez, Pintaric, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Marongiu, Piras, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1Ultra-2DB-5HP-5
Column length (m) 30.60.50.30.25.
Carrier gas Helium HeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.320.250.33
Tstart (C) 60.70.50.40.30.
Tend (C) 250.230.270.260.280.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min) 2.2. 5. 
Final hold (min) 20.20. 20. 
I 1000.978.1003.1001.1003.
ReferencePino, Marquez, et al., 2006Sawamura, Onishi, et al., 2006Schlumpberger B.O., Clery R.A., et al., 2006Senatore, Landolfi, et al., 2006Shafi, Jose, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5HP-1DB-5
Column length (m) 30.30.30.50.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.320.320.20.3
Phase thickness (μm) 0.250.250.250.50.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.260.260.250.240.
Heat rate (K/min) 3.5.5.2.2.
Initial hold (min)  2.2.  
Final hold (min)  14.14.60. 
I 994.1001.998.983.1001.
ReferenceTzakou, Said, et al., 2006Yayli, Gülec, et al., 2006Yayli, Gülec, et al., 2006Bendimerad and Bendiab, 2005Chagonda and Chalchat, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RTX-5SilCP Sil 5 CBBPX-5MDN-5
Column length (m) 60.30.30.30.60.
Carrier gas N2HeN2 He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.45.60.40.40.
Tend (C) 250.200.250.200.270.
Heat rate (K/min) 5.3.5.5.4.
Initial hold (min)  5. 8.4.
Final hold (min) 10. 10.10.5.
I 985.1007.985.1029.1005.
ReferenceFakhari A.R., Sonboli A., et al., 2005Holland, Larkov, et al., 2005Jassbi, Mehrdad, et al., 2005Kalua, Allen, et al., 2005van Loon, Linssen, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase MDN-5CP Sil 5 CBCP Sil 5 CBDB-5HP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.60.
Tend (C) 270.220.220.260.280.
Heat rate (K/min) 4.4.4.2.3.
Initial hold (min) 4.1.1.5. 
Final hold (min) 5.  20. 
I 1005.999.999.1001.969.
Referencevan Loon, Linssen, et al., 2005Rohloff and Bones, 2005Rohloff and Bones, 2005Senatore, Apostolides Arnold, et al., 2005Tzakou, Bazos, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.60.
Tend (C) 250.250.250.250.260.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min) 2.2.2.2.2.
Final hold (min) 5.5.5.5.13.
I 1004.984.984.985.1008.
ReferenceN/AN/AN/AN/AYayli, Yasar, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1ZB-5DB-5SE-54DB-5MS
Column length (m) 50.60.60.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.0530.25
Phase thickness (μm) 0.330.250.251.50.25
Tstart (C) 60.40.40.100.60.
Tend (C) 250.260.280.250.280.
Heat rate (K/min) 2.6.4.5.3.
Initial hold (min)  4.64.  
Final hold (min) 20.1.  30.
I 977.1008.998.1005.975.
ReferenceCavalli, Fernandez, et al., 2004Jürgens and Dötterl, 2004Kalvandi, Sefidkon, et al., 2004Kilic, Hafizoglu, et al., 2004Marongiu, Piras, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneHP-1HP-5SE-54DB-5
Column length (m) 0.30.25.30.60.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 1.0.330.50.250.25
Tstart (C) 40.40.30.40.35.
Tend (C) 250.260.280.200.280.
Heat rate (K/min) 7.2.3.5.5.
Initial hold (min) 10.5. 4.2.
Final hold (min) 5.20. 10.4.
I 1004.981.1003.1009.998.
ReferenceRamírez, Estévez, et al., 2004Senatore, Napolitano, et al., 2004Shafi, Nambiar, et al., 2004Tura, Prenzler, et al., 2004Dhanda, Pegg, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase MDN-5HP-5SPB-5SPB-1SPB-1
Column length (m) 30.30.60.30.30.
Carrier gas HeHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.25 1.00.250.25
Tstart (C) 40.70.30.40.40.
Tend (C) 280.210.230.200.200.
Heat rate (K/min) 20.2.3.3.3.
Initial hold (min) 1.  10.10.
Final hold (min) 1.60.   
I 1010.1004.1003.981.981.
ReferenceMildner-Szkudlarz, Jelen, et al., 2003Mookdasanit, Tamura, et al., 2003Sebastian, Viallon-Fernandez, et al., 2003Vichi, Castellote, et al., 2003Vichi, Pizzale, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5HP-5DB-5DB-1
Column length (m) 30.50.30.30.30.
Carrier gas HeHeH2HeH2
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (μm) 0.251.050.250.250.25
Tstart (C) 40.40.45.60.40.
Tend (C) 200.200.230.240.245.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min) 10.10.1. 20.
Final hold (min)  5.10.  
I 984.1008.1008.1003.976.
ReferenceVichi, Pizzale, et al., 2003, 2Andrés, Cava, et al., 2002Darriet, Pons, et al., 2002Flamini, Ertugrul, et al., 2002Gancel, Ollé, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200DB-5HP-5DB-5RTX-5
Column length (m) 30.30.30.30.20.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.18
Phase thickness (μm) 0.250.250.250.250.4
Tstart (C) 40.40.60.60.20.
Tend (C) 280.290.275.300.290.
Heat rate (K/min) 6.7.4.2.40.
Initial hold (min) 2. 4. 3.5
Final hold (min) 10.   0.5
I 975.1004.999.998.1004.
ReferenceJirovetz, Smith, et al., 2002Lin, Rouseff, et al., 2002Lockwood, Asghari, et al., 2002Ruberto, Biondi, et al., 2002Sies A., Hirsch R., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-1DB-5MSHP-5DB-5MSOV-101
Column length (m) 25.30.30.60.50.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.200.530.250.250.2
Phase thickness (μm) 0.251.50.250.25 
Tstart (C) 50.40.60.40.50.
Tend (C) 250.225.220.200.250.
Heat rate (K/min) 3.6.5.2.2.
Initial hold (min) 3.5.10.5. 
Final hold (min)  30. 30. 
I 987.1005.1002.1005.985.
ReferenceBrun, Bessière, et al., 2001Cadwallader and Heo, 2001Campeol, Flamini, et al., 2001Lee, Suriyaphan, et al., 2001Orav and Kann, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5OV-101OV-101CP Sil 5 CB
Column length (m) 60.30.50.50.25.
Carrier gas He N2N2He
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 1.0.5  0.4
Tstart (C) 40.35.80.80.60.
Tend (C) 200.275.200.200.260.
Heat rate (K/min) 3.6.2.2.5.
Initial hold (min)     40.
Final hold (min)      
I 1003.1003.980.980.975.
ReferencePoligné, Collignan, et al., 2001Rouseff, Jella, et al., 2001Yang, 2001Yang, 2001, 2Baser, Özek, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-1HP-5DB-5SE-30Methyl Silicone
Column length (m) 25.60.30.30.60.
Carrier gas HeHeN2  
Substrate      
Column diameter (mm) 0.200.320.220.250.25
Phase thickness (μm) 0.251.0.25 0.25
Tstart (C) 50.40.70.50.40.
Tend (C) 250.240.230.300.220.
Heat rate (K/min) 3.3.4.10.5.
Initial hold (min) 3. 2. 10.
Final hold (min)   20.4. 
I 989.1004.1000.981.982.16
Referencede Beck, Bessière, et al., 2000García, Martín, et al., 2000Mitiku, Sawamura, et al., 2000Zhou, Robards, et al., 2000Baraldi, Rapparini, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5HP-1DB-5DB-5DB-5
Column length (m) 50.25.30. 30.
Carrier gas HeH2  H2
Substrate      
Column diameter (mm) 0.320.320.32 0.32
Phase thickness (μm) 1.0.171.0.25 
Tstart (C) 40.40.40.34.32.
Tend (C) 190.260.200.200.260.
Heat rate (K/min) 2.3.3.5.7.
Initial hold (min) 5.5.5.3.5.
Final hold (min)    10.5.
I 1010.981.1003.999.1004.
ReferenceLopez, Ferreira, et al., 1999Lopes, Koketsu, et al., 1999Meynier, Novelli, et al., 1999Schlüter, Steinhart, et al., 1999Sun and Petracek, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SE-54CBP-1HP-1HP-5
Column length (m) 50.25.30.25.25.
Carrier gas   He He
Substrate      
Column diameter (mm) 0.320.310.250.320.2
Phase thickness (μm) 0.52   0.33
Tstart (C) 35.35.60.35.70.
Tend (C) 250.250.240.250.290.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min) 15.3.  8.
Final hold (min) 45.   20.
I 1004.999.982.981.1000.
ReferenceBoylston and Viniyard, 1998Ding, Deng, et al., 1998Lamarque, Maestri, et al., 1998Ong and Acree, 1998Poiana, Sicari, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5DB-5SE-54SE-54
Column length (m) 25.60.60.25.30.
Carrier gas    He 
Substrate      
Column diameter (mm) 0.20.320.320.20.52
Phase thickness (μm)  1.1.0.51.5
Tstart (C) 35.40.40.35.5.
Tend (C) 200.200.200.250.230.
Heat rate (K/min) 5.3.3.5.6.
Initial hold (min) 5.5.5.2. 
Final hold (min)  2.2.  
I 982.1002.1004.1004.1006.
ReferenceQuiroz A. and Niemeyer H.M., 1998Kondjoyan, Viallon, et al., 1997Kondjoyan, Viallon, et al., 1997Bellesia, Pinetti, et al., 1996Milo and Grosch, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1Ultra-2RTX-5OV-101
Column length (m) 12.60.50.30.50.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.320.250.320.520.25
Phase thickness (μm)   0.521.5 
Tstart (C) 35.30.40.5.80.
Tend (C) 225.200.250.230.200.
Heat rate (K/min) 6.4.4.6.2.
Initial hold (min) 3.25.3.  
Final hold (min)  20.30.  
I 975.979.1003.1006.979.
ReferenceRoberts and Acree, 1996Buttery and Ling, 1995King, Matthews, et al., 1995Milo and Grosch, 1995Tamura, Nakamoto, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-1Cross-Linked MethylsiliconeUltra-2
Column length (m) 50.60.60.25.50.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm)  0.250.25 0.52
Tstart (C) 80.70.70.35.40.
Tend (C) 200.270.270.225.250.
Heat rate (K/min) 2.2.52.54.4.
Initial hold (min)  5.5.3.3.
Final hold (min)     30.
I 981.977.977.975.1004.
ReferenceTamura, Nakamoto, et al., 1995Tirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995Bravo and Hotchkiss, 1993King, Hamilton, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5OV-101OV-101
Column length (m) 30.30.30.50.50.
Carrier gas H2H2H2  
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 1.1.1.  
Tstart (C) 40.40.40.80.80.
Tend (C) 220.220.220.200.200.
Heat rate (K/min) 3.3.5.2.2.
Initial hold (min)   5.  
Final hold (min)      
I 1004.1004.1004.980.981.
ReferenceMoio, Dekimpe, et al., 1993Moio, Dekimpe, et al., 1993Moio, Langlois, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeDB-1DB-5HG-5DB-5
Column length (m) 17.60.60.50.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm)  1.21.00.520.25
Tstart (C) 35.30.40.35.40.
Tend (C) 225.240.240.250.250.
Heat rate (K/min) 4.3.3.3.2.
Initial hold (min) 3.10. 15.5.
Final hold (min)    45. 
I 982.983.1004.1004.1002.
ReferenceBravo, Hotchkiss, et al., 1992Ciccioli, Cecinato, et al., 1992Berdague, Denoyer, et al., 1991Drumm and Spanier, 1991Lee, Macku, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101OV-101DB-1DB-1
Column length (m) 60.50.50. 60.
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.250.320.28 0.32
Phase thickness (μm)  0.5   
Tstart (C) 40.50.80.50.50.
Tend (C) 160.250.200.230.230.
Heat rate (K/min) 2.4.2.4.4.
Initial hold (min) 5.    
Final hold (min)    10.10.
I 1005.977.985.979.979.
ReferenceMacku and Shibamoto, 1991Misharina, Golovnya, et al., 1991Anker, Jurs, et al., 1990Binder, Turner, et al., 1990Binder, Turner, et al., 1990, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 50.50.50.50.50.
Carrier gas NitrogenNitrogenN2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)      
Tstart (C) 70.80.80.80.80.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 984.983.981.982.985.
ReferenceSugisawa, Nakamura, et al., 1990Sugisawa, Nakamura, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Sugisawa, Yamamoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-1OV-101OV-101
Column length (m) 50.50.50.50.50.
Carrier gas N2N2   
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm)      
Tstart (C) 80.80.0.40.50.
Tend (C) 200.200.250.225.225.
Heat rate (K/min) 2.2.3.4.4.
Initial hold (min)    0.10.1
Final hold (min)    30.30.
I 979.981.979.980.980.
ReferenceSugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Habu, Flath, et al., 1985Stern, Flath, et al., 1985Stern, Flath, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase OV-101SP 2100SE-30SF-96
Column length (m) 50.40.50.111.
Carrier gas HeHelium Nitrogen
Substrate     
Column diameter (mm) 0.310.200.50.76
Phase thickness (μm)     
Tstart (C) 0.40.40. 
Tend (C) 225.200.170.130.
Heat rate (K/min) 3.10.3.3.
Initial hold (min) 1. 3.8.
Final hold (min)    40.
I 980.979.981.985.
Referencedel Rosario, de Lumen, et al., 1984Labropoulos, Palmer, et al., 1982Heydanek and McGorrin, 1981Donetzhuber, Johansson, et al., 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Castel, Fernandez, et al., 2006
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Choi, 2006
Choi, H.-S., Headspace analyses of fresh leaves and stems of Angelica gigas Nakai, a Korean medicinal herb, Flavour Fragr. J., 2006, 21, 4, 604-608, https://doi.org/10.1002/ffj.1602 . [all data]

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Shafi, Jose, et al., 2006
Shafi, P.M.; Jose, B.; Radhamani, K.T.; Clery, R.A., Influence of pH on essential oil composition of Zanthoxylum rhetsa seeds obtained by steam distillation, Flavour Fragr. J., 2006, 21, 2, 317-318, https://doi.org/10.1002/ffj.1598 . [all data]

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Tzakou, O.; Said, A.; Farag, A.; Rashed, K., Volatile constituents of Ailanthus excelsa Roxb., Flavour Fragr. J., 2006, 21, 6, 899-901, https://doi.org/10.1002/ffj.1739 . [all data]

Yayli, Gülec, et al., 2006
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Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

Chagonda and Chalchat, 2005
Chagonda, L.S.; Chalchat, J.-C., The essential oil of wild and cultivated Hoslundia opposita Vahl. from Zimbabwe, Flavour Fragr. J., 2005, 20, 2, 193-195, https://doi.org/10.1002/ffj.1402 . [all data]

Fakhari A.R., Sonboli A., et al., 2005
Fakhari A.R.; Sonboli A.; Heydari R., Composition of the essential oil of Rhabdosciadium strausii from Iran, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 4, 413-414, https://doi.org/10.1007/s10600-005-0164-1 . [all data]

Holland, Larkov, et al., 2005
Holland, D.; Larkov, O.; Bar-Ya'akov, I.; Bar, E.; Zax, A.; Brandeis, E.; Ravid, U.; Lewinsohn, E., Developmental and varietal differences in volatile ester formation and acetyl-CoA: alcohol acetyl transferase activities in apple (Malus domestica Borkh.) fruit, J. Agric. Food Chem., 2005, 53, 18, 7198-7203, https://doi.org/10.1021/jf050519k . [all data]

Jassbi, Mehrdad, et al., 2005
Jassbi, A.R.; Mehrdad, M.; Soleimani, M.; Mirzaeian, M.; Sonboli, A., Chemical composition of the essential oils of Bunium elegans and Bunium caroides, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 4, 415-417, https://doi.org/10.1007/s10600-005-0165-0 . [all data]

Kalua, Allen, et al., 2005
Kalua, C.M.; Allen, M.S.; Bedgood, D.R., Jr.; Bishop, A.G.; Prenzler, P.D., Discrimination of Olive Oils and Fruits into Cultivars and Maturity Stages Based on Phenolic and Volatile Compounds, J. Agric. Food Chem., 2005, 53, 20, 8054-8062, https://doi.org/10.1021/jf051233i . [all data]

van Loon, Linssen, et al., 2005
van Loon, W.A.M.; Linssen, J.P.H.; Legger, A.; Posthumus, M.A.; Voragen, A.G.J., Identification and olfactometry of French fries flavour extracted at mouth conditions, Food Chem., 2005, 90, 3, 417-425, https://doi.org/10.1016/j.foodchem.2004.05.005 . [all data]

Rohloff and Bones, 2005
Rohloff, J.; Bones, A.M., Volatile profiling of Arabidopsis thaliana - Putative olfactory compounds in plant communication, Phytochemistry, 2005, 66, 16, 1941-1955, https://doi.org/10.1016/j.phytochem.2005.06.021 . [all data]

Senatore, Apostolides Arnold, et al., 2005
Senatore, F.; Apostolides Arnold, N.; Bruno, M., Volatile components of Centaurea eryngioides Lam. and Centaurea liberica Trev. var. hermonis Boiss. Lam., two Asteraceae growing wild in Lebanon, Nat. Prod. Res., 2005, 19, 8, 749-754, https://doi.org/10.1080/14786410412331302136 . [all data]

Tzakou, Bazos, et al., 2005
Tzakou, O.; Bazos, I.; Yannitsaros, A., Essential oils of leaves, inflorescences and infructescences of spontaneous Cotinus coggygria Scop. from Greece, Flavour Fragr. J., 2005, 20, 5, 531-533, https://doi.org/10.1002/ffj.1456 . [all data]

Yayli, Yasar, et al., 2005
Yayli, N.; Yasar, A.; Gülec, C.; Usta, A.; Kolayli, S.; Coskuncelebi, K.; Karaoglu, S., Composition and antimicrobial activity of essential oils from Centaurea sessilis and Centaurea armena, Phytochemistry, 2005, 66, 14, 1741-1745, https://doi.org/10.1016/j.phytochem.2005.04.006 . [all data]

Cavalli, Fernandez, et al., 2004
Cavalli, J.-F.; Fernandez, X.; Lizzani-Cievelier, L.; Loiseau, A.-M., Characterization of volatile compounds of French and Spanish virgin olive oil by HS-SPME: identification of quality-freshness markers, Food Chem., 2004, 88, 1, 151-157, https://doi.org/10.1016/j.foodchem.2004.04.003 . [all data]

Jürgens and Dötterl, 2004
Jürgens, A.; Dötterl, S., Chemical composition of anther volatiles in Ranunculaceae: genera-specific profiles in Aemone, Aquilegia, Caltha, Pulsatilla, Ranunculus, and Trollius species, American Journal of Botany, 2004, 91, 12, 1969-1980, https://doi.org/10.3732/ajb.91.12.1969 . [all data]

Kalvandi, Sefidkon, et al., 2004
Kalvandi, R.; Sefidkon, F.; Atri, M.; Mirza, M., Analysis of the essential oil of Thymus eriocalyx from Iran, Flavour Fragr. J., 2004, 19, 4, 341-343, https://doi.org/10.1002/ffj.1312 . [all data]

Kilic, Hafizoglu, et al., 2004
Kilic, A.; Hafizoglu, H.; Kollmannsberger, H.; Nitz, S., Volatile constituents and key odorants in leaves, buds, flowers, and fruits of Laurus nobilis L., J. Agric. Food Chem., 2004, 52, 6, 1601-1606, https://doi.org/10.1021/jf0306237 . [all data]

Marongiu, Piras, et al., 2004
Marongiu, B.; Piras, A.; Porcedda, S., Comparative analysis of the oil and supercritical CO2 extract of Elettaria cardamomum (L.) maton, J. Agric. Food Chem., 2004, 52, 20, 6278-6282, https://doi.org/10.1021/jf034819i . [all data]

Ramírez, Estévez, et al., 2004
Ramírez, M.R.; Estévez, M.; Morcuende, D.; Cava, R., Effect of the type of frying culinary fat on volatile compounds isolated in fried pork loin chops by using SPME-GC-MS, J. Agric. Food Chem., 2004, 52, 25, 7637-7643, https://doi.org/10.1021/jf049207s . [all data]

Senatore, Napolitano, et al., 2004
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Notes

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