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1-Butanol, 3-methyl-, acetate

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Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-20DB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 25.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.40.40.40.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 1125.1126.1126.1124.1126.
ReferenceShimadzu, 2003Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 30.150.50.50.30.
Carrier gas N2He  N2
Substrate      
Column diameter (mm) 0.250.640.280.280.26
Phase thickness (mum)      
Tstart (C) 60.50.80.80.70.
Tend (C) 200.170.200.200.170.
Heat rate (K/min) 2.1.2.2.3.
Initial hold (min) 10.    
Final hold (min)      
I 1130.1120.1102.1105.1117.
ReferenceUmano, Shoji, et al., 1986Buttery, Seifert, et al., 1982Toda, Yamaguchi, et al., 1982Toda, Yamaguchi, et al., 1982Spencer, Pangborn, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase Carbowax 20MCarbowax 20M
Column length (m) 30.50.
Carrier gas N2He
Substrate   
Column diameter (mm) 0.260.28
Phase thickness (mum)   
Tstart (C) 70.70.
Tend (C) 170.190.
Heat rate (K/min) 3.2.
Initial hold (min)   
Final hold (min)   
I 1121.1126.
ReferenceSpencer, Pangborn, et al., 1978Tressl, Friese, et al., 1978
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Shimadzu, 2003
Shimadzu, Gas chromatography analysis of organic solvents using capillary columns (No. 2), 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

Umano, Shoji, et al., 1986
Umano, K.; Shoji, A.; Hagi, Y.; Shibamoto, T., Volatile constituents of peel of quince fruit, Cydonia oblonga Miller, J. Agric. Food Chem., 1986, 34, 4, 593-596, https://doi.org/10.1021/jf00070a003 . [all data]

Buttery, Seifert, et al., 1982
Buttery, R.G.; Seifert, R.M.; Ling, L.C.; Soderstrom, E.L.; Ogawa, J.M.; Turnbaugh, J.G., Additional aroma components of honeydew melon, J. Agric. Food Chem., 1982, 30, 6, 1208-1211, https://doi.org/10.1021/jf00114a051 . [all data]

Toda, Yamaguchi, et al., 1982
Toda, H.; Yamaguchi, K.; Shibamoto, T., Isolation and identification of banana-like aroma from banana shrub (Michellia figo Spreng), J. Agric. Food Chem., 1982, 30, 1, 81-84, https://doi.org/10.1021/jf00109a017 . [all data]

Spencer, Pangborn, et al., 1978
Spencer, M.D.; Pangborn, R.M.; Jennings, W.G., Gas chromatographic and sensory analysis of volatiles from cling peaches, J. Agric. Food Chem., 1978, 26, 3, 725-732, https://doi.org/10.1021/jf60217a052 . [all data]

Tressl, Friese, et al., 1978
Tressl, R.; Friese, L.; Fendesack, F.; Köppler, H., Gas chromatographic--mass spectrometric investigation of hop aroma constituents in beer, J. Agric. Food Chem., 1978, 26, 6, 1422-1426, https://doi.org/10.1021/jf60220a037 . [all data]


Notes

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