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1-Butanol, 3-methyl-

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m)    25.25.
Carrier gas      
Substrate      
Column diameter (mm)    0.330.33
Phase thickness (mum)      
Temperature (C) 100.60.80.100.120.
I 723.733.721.723.727.
ReferenceTarjan, Nyiredy, et al., 1989Tarjan, Nyiredy, et al., 1989Tarjan, Nyiredy, et al., 1989Haken and Korhonen, 1985Haken and Korhonen, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m) 25.25.25.25.25.
Carrier gas    N2N2
Substrate      
Column diameter (mm) 0.330.330.330.330.33
Phase thickness (mum)      
Temperature (C) 140.60.80.100.120.
I 738.733.721.723.727.
ReferenceHaken and Korhonen, 1985Haken and Korhonen, 1985Haken and Korhonen, 1985Haken, Madden, et al., 1985Haken, Madden, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase SE-30SE-30SE-30SE-30OV-1
Column length (m) 25.25.25.3.2.
Carrier gas N2N2N2Ar 
Substrate    Gas Chrom Q (80-100 mesh)Gas Chrom Q
Column diameter (mm) 0.330.330.33  
Phase thickness (mum)      
Temperature (C) 140.60.80.150.120.
I 738.733.721.720.718.
ReferenceHaken, Madden, et al., 1985Haken, Madden, et al., 1985Haken, Madden, et al., 1985Tiess, 1984Valko, Papp, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SE-30SE-30SE-30SE-30Apiezon L
Column length (m) 2.1.1.1.3.
Carrier gas  ArArArCH4
Substrate Gaschrom QChromosorb W AW DMCS HP (80-100 mesh)Chromosorb W AW DMCS HP (80-100 mesh)Chromosorb W AW DMCS HP (80-100 mesh) 
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 100.100.120.140.100.
I 725.725.719.719.712.
ReferenceWinskowski, 1983Pías and Gascó, 1975Pías and Gascó, 1975Pías and Gascó, 1975Wagaman and Smith, 1971
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m) 2.
Carrier gas  
Substrate Chromosorb W
Column diameter (mm)  
Phase thickness (mum)  
Temperature (C) 100.
I 726.
ReferenceZarazir, Chovin, et al., 1970
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Tarjan, Nyiredy, et al., 1989
Tarjan, G.; Nyiredy, Sz.; Gyor, M.; Lombosi, E.R.; Lombosi, T.S.; Budahegyi, M.V.; Meszaros, S.Y.; Takacs, J.M., Review. Thirtieth Anniversary of the Retention Index According to Kovats in Gas-Liquid Chromatography, J. Chromatogr., 1989, 472, 1-92, https://doi.org/10.1016/S0021-9673(00)94099-8 . [all data]

Haken and Korhonen, 1985
Haken, J.K.; Korhonen, I.O.O., Gas-liquid chromatography of homologous esters. XXIX. Propanoyl and monochlorpropanoyl esters of lower saturated branched-chain and unsaturated alcohols, J. Chromatogr., 1985, 324, 343-353, https://doi.org/10.1016/S0021-9673(01)81333-9 . [all data]

Haken, Madden, et al., 1985
Haken, J.K.; Madden, B.G.; Korhonen, I.O.O., Gas chromatography of homologous esters. XXXI. Butanoyl and monochlorobutanoyl esters of lower saturated branched chain and unsaturated alcohols on SE-30 and OV-351 capillary columns, J. Chromatogr., 1985, 325, 61-73, https://doi.org/10.1016/S0021-9673(00)96008-4 . [all data]

Tiess, 1984
Tiess, D., Gaschromatographische Retentionsindices von 125 leicht- bis mittelflüchtigen organischen Substanzen toxikologisch-analytischer Relevanz auf SE-30, Wiss. Z. Wilhelm-Pieck-Univ. Rostock Math. Naturwiss. Reihe, 1984, 33, 6-9. [all data]

Valko, Papp, et al., 1984
Valko, K.; Papp, O.; Darvas, F., Selection of Gas Chromatographic Stationary Phase Pairs for Characterization of the 1-Octanol-Water Partition Coefficient, J. Chromatogr., 1984, 301, 355-364, https://doi.org/10.1016/S0021-9673(01)89210-4 . [all data]

Winskowski, 1983
Winskowski, J., Gaschromatographische Identifizierung von Stoffen anhand von Indexziffem und unterschiedlichen Detektoren, Chromatographia, 1983, 17, 3, 160-165, https://doi.org/10.1007/BF02271041 . [all data]

Pías and Gascó, 1975
Pías, J.B.; Gascó, L., GC Retention Data of Alcohols and Benzoyl Derivatives of Alcohols, J. Chromatogr. - Chrom. Data, 1975, d14-d16. [all data]

Wagaman and Smith, 1971
Wagaman, K.L.; Smith, T.G., Use of hydrocarbons as carrier gases in GLC, J. Chromatogr. Sci., 1971, 9, 4, 241-244, https://doi.org/10.1093/chromsci/9.4.241 . [all data]

Zarazir, Chovin, et al., 1970
Zarazir, D.; Chovin, P.; Guiochon, G., Identification of hydroxylic compounds and their derivatives by gas chromatography, Chromatographia, 1970, 3, 4, 180-195, https://doi.org/10.1007/BF02269018 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References