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Malathion

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryPacked
Active phase SLB-5MSSLB-5MSOV-1OV-1
Column length (m) 30.30.25. 
Carrier gas HeHeH2N2
Substrate    AW-DMCS
Column diameter (mm) 0.250.250.250.53
Phase thickness (mum) 0.250.250.3 
Tstart (C) 70.70.160.80.
Tend (C) 300.300.260.220.
Heat rate (K/min) 2.2.5.2.
Initial hold (min)   1. 
Final hold (min)   2. 
I 1959.1965.1919.1946.
ReferenceMondello, Casilli, et al., 2007Mondello, Casilli, et al., 2007Bicchi, D'Amato, et al., 1996Oyama, Sano, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mondello, Casilli, et al., 2007
Mondello, L.; Casilli, A.; Tranchida, P.Q.; Presti, M.L.; Dugo, P.; Dugo, G., Comprehensive gas chromatography coupled to mass spectrometry for the separation of pesticides in a very complex matrix, Anal. Bioanal. Chem., 2007, 389, 6, 1755-1763, https://doi.org/10.1007/s00216-007-1412-y . [all data]

Bicchi, D'Amato, et al., 1996
Bicchi, C.; D'Amato, A.; Binello, A., Identification of pesticide residues in real matrices by combining retention indices and specific multidetection responses, J. Hi. Res. Chromatogr., 1996, 19, 2, 80-84, https://doi.org/10.1002/jhrc.1240190204 . [all data]

Oyama, Sano, et al., 1987
Oyama, N.; Sano, T.; Syoyama, M.; Maeda, K., Studies on systematic analysis of poisonous compounds in forensic chemistry. II. Application of capillary column gas chromatography to substance identification by means of retention indices, Eisei Kagaku, 1987, 33, 5, 342-348, https://doi.org/10.1248/jhs1956.33.342 . [all data]


Notes

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