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Malathion

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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxane5 % Phenyl methyl siloxaneHP-5Methyl SiliconeDB-5
Column length (m) 30.30.30.  
Carrier gas HeliumHelium   
Substrate      
Column diameter (mm) 0.250.250.25  
Phase thickness (mum) 0.250.250.25  
Program 50 0C(1 min) 25 0C/min -> 125 0C 10 0C/min -> 300 0C (10 min)50 0C(1 min) 25 0C/min -> 125 0C 10 0C/min -> 300 0C (10 min)50 0C (1 min) 20 0C/min -> 150 0C 10 0C/min -> 280 0Cnot specifiednot specified
I 1963.1965.1962.1928.1965.
ReferenceDepartment of Food Safety and Welfare, 2006Department of Food Safety and Welfare, 2006Kawara, Asada, et al., 2005Zenkevich, Ostroukhova, et al., 2002Soderstrom, White, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m)     30.
Carrier gas      
Substrate      
Column diameter (mm)     0.25
Phase thickness (mum)     0.25
Program not specifiednot specifiednot specifiednot specified50 0C (1 min) 20 0C/min -> 200 0C 10 0C/min -> 280 0C (2 min)
I 1970.1975.1986.1986.1969.
ReferenceSoderstrom, White, et al., 2001Soderstrom, White, et al., 2001Soderstrom, White, et al., 2001Soderstrom, White, et al., 2001Kawata, Mukai, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryOther
Active phase Ultra-1OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.Methyl Silicone
Column length (m)  50. 
Carrier gas  Hydrogen 
Substrate    
Column diameter (mm)  0.32 
Phase thickness (mum)    
Program not specifiednot specifiednot specified
I 1913.1917.1917.
ReferenceTameo and Kiyos, 1991Waggott and Davies, 1984Ardrey and Moffat, 1981
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Department of Food Safety and Welfare, 2006
Department of Food Safety, Ministry of Health; Welfare, Analytical methods for residual compositional substances of agricultural chemicals, feed aadditives, and veterinary drugs in foods, 2006, retrieved from http://www.mhlw.go.jp/english/topics/foodsafety/positivelist060228/de/060526-1a.pdf. [all data]

Kawara, Asada, et al., 2005
Kawara, K.; Asada, T.; Oikawa, K.; Tanabe, A., Multiresidue determination of pesticides in sediments by ultrasonically assisted extraction and gas chromatography/mass spectrometry, J. AOAC International, 2005, 88, 5, 1440-1451. [all data]

Zenkevich, Ostroukhova, et al., 2002
Zenkevich, I.G.; Ostroukhova, O.K.; Dolzhenko, V.I., Optimum analytical parameters for chromatographic characterization of pesticides, J. Anal. Chem. USSR (Engl. Transl.), 2002, 57, 1, 35-39. [all data]

Soderstrom, White, et al., 2001
Soderstrom, M.; White, E.; Abis, L.; Sliwakowski, M., Summary report of the eight meeting of the validation group for the updating of the central OPCW analytical database, 28-29 November 2000, CS-2001-2242, Verification Division S/239/2001, 2001, 14. [all data]

Kawata, Mukai, et al., 1996
Kawata, K.; Mukai, H.; Tanabe, H.; Yasuhara, A., Annual variation of insecticides in precipitation in rural Japan, Bull. Environ. Contam. Toxicol., 1996, 57, 6, 853-858, https://doi.org/10.1007/s001289900268 . [all data]

Tameo and Kiyos, 1991
Tameo, O.; Kiyos, I., Simultaneous determination of pesticides by capillary gas chromatography, Cannot be traslated (in Japan), 1991, 14, 2, 109-122. [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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