2-Naphthalenemethanol, 1,2,3,4,4a,5,6,7-octahydro-α,α,4a,8-tetramethyl-, (2R-cis)-


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSCP-Sil 5 CBHP-5 MSHP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.2520.25
Phase thickness (μm) 0.250.260.250.250.25
Tstart (C) 50.45.30.60.50.
Tend (C) 250.280.250.240.250.
Heat rate (K/min) 7.3.5.3.2.
Initial hold (min) 1. 3.  
Final hold (min) 5.22.10.  
I 1630.1619.1647.1629.1632.
ReferenceZouari, Ayadi, et al., 2012Mothana, Hasson, et al., 2011Zarai, Kadri, et al., 2011Cavar, Maksimovic, et al., 2010Ho, Wang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSZB-5CP-Sil 5 CBDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.70.50.50.50.
Tend (C) 240.290.240.200.250.
Heat rate (K/min) 3.5.3.5.5.
Initial hold (min) 5.   2.
Final hold (min)  10.1.  
I 1623.1640.1621.1649.1632.
ReferenceMonsef-Esfahani, Miri, et al., 2010Radulovic, Blagojevic, et al., 2010Gardini, Beletti, et al., 2009Hnawia, Menut, et al., 2009Ho, Wang, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-15 % Phenyl methyl siloxaneDB-5HP-1
Column length (m) 60.60.60.30.25.
Carrier gas HeliumHeliumHeliumNitrogen 
Substrate      
Column diameter (mm) 0.220.220.250.250.32
Phase thickness (μm) 0.250.250.250.250.17
Tstart (C) 60.60.90.40.50.
Tend (C) 230.230.225.230.260.
Heat rate (K/min) 2.2.3.2.1.
Initial hold (min)     5.
Final hold (min) 30.30.3. 5.
I 1618.1622.1633.1633.1608.
ReferenceMuseli, Pau, et al., 2009Museli, Pau, et al., 2009Retta, Gattuso, et al., 2009Scrivanti, Anton, et al., 2009Wetwiayaklung, Thavanapong, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSUltra 2HP-5HP-5 MSDB-5
Column length (m) 30.50.25.30.50.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.200.250.250.20
Phase thickness (μm) 0.250.110.250.250.32
Tstart (C) 50.60.60.50.60.
Tend (C) 280.230.240.230.220.
Heat rate (K/min) 4.2.4.3.5.
Initial hold (min)  5.2.10.3.
Final hold (min)  30. 10.5.
I 1637.1631.1630.1630.1660.
ReferenceZhao, Zeng, et al., 2009Byun and Shin, 2008Verdian-rizi, 2008Adams, Beauchamp, et al., 2007Amiri, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSHP-5RTX-5 MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeliumHeHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.260.250.25
Tstart (C) 60.50.60.45.60.
Tend (C) 300.280.240.210.300.
Heat rate (K/min) 4.5.4.3.3.
Initial hold (min)  4.2.  
Final hold (min)  10.20.  
I 1620.1631.1635.1632.1599.
ReferenceBaran, von Reuss, et al., 2007Cho, Abd El-Aty, et al., 2007Farsam, Amanlou, et al., 2007Hudaib and Aburjai, 2007Moreno, Lima, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5AT-5BP-1CP Sil 5 CBHP-5MS
Column length (m) 30.60.50.30.30.
Carrier gas  He  He
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.40.50.
Tend (C) 250.200.220.220.280.
Heat rate (K/min) 2.4.2.3.5.
Initial hold (min)     4.
Final hold (min) 33.20.20.3.10.
I 1624.1631.1618.1632.1631.
ReferenceSylvestre, Pichette, et al., 2007Borges, Rojas, et al., 2006Boti, Yao, et al., 2006Hymete, Rohloff, et al., 2006Kim, Abd El-Aty, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1DB-5PE-5HP-5
Column length (m) 30.50.30.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.100.60.
Tend (C) 280.220.260.280.220.
Heat rate (K/min) 5.2.4.3.5.
Initial hold (min) 4. 4.1.10.
Final hold (min) 10.20.   
I 1621.1621.1634.1632.1631.
ReferenceKim, El-Aty, et al., 2006Lesueur, Ban, et al., 2006Morteza-Semnani, Saeedi, et al., 2006Pandey-Rai S., Mallavarapu G.R., et al., 2006Pintore G., Chessa M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5HP-5MSHP-5MSDB-1
Column length (m) 30.25.30.30.60.
Carrier gas HeliumH2 HeHelium
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 250.240.250.243.250.
Heat rate (K/min) 4.3.10.3.5.
Initial hold (min) 2. 5.  
Final hold (min) 20.   10.
I 1630.1637.1645.1625.1624.
ReferencePino, Marquez, et al., 2006Potzernheim, Bizzo, et al., 2006Robinson, 2006Sabulal, Dan, et al., 2006Sonboli, Mirjalili, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5MSHP-5DB-5
Column length (m) 30.30.30.25.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.250.240.240.300.
Heat rate (K/min) 4.10.3.3.3.
Initial hold (min)  2.  3.
Final hold (min)  10. 7. 
I 1631.1646.1630.1626.1625.
ReferenceTrilles, Bombarda, et al., 2006Wang, Yang, et al., 2006Busman, Zoghbi, et al., 2005Duarte, Figueira, et al., 2005Ferraz, Limberger, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-1DB-5HP-5MS
Column length (m) 25.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 50.60.50.60.60.
Tend (C) 250.240.250.230.280.
Heat rate (K/min) 3.3.4.3.4.
Initial hold (min) 3. 5.  
Final hold (min) 10.    
I 1631.1626.1629.1626.1628.
ReferenceGhasemi Y., Faridi P., et al., 2005Khayyat and Karimi, 2005Khajeh, Yamini, et al., 2005Limberger, Sobral, et al., 2005Sajjadi, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PE-5DB-1DB-5MSSPB-5RTX-1
Column length (m) 30.50.30.60.30.
Carrier gas H2N2HeHeN2
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (μm) 0.250.250.251.0.25
Tstart (C) 60.90.80.60.60.
Tend (C) 230.240.250.200.300.
Heat rate (K/min) 5.4.5.4.4.
Initial hold (min) 2. 2.  
Final hold (min) 4. 9.30. 
I 1622.1612.1631.1639.1626.
ReferenceSingh, Raina, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Watanabe Y., Mihara R., et al., 2005Gauvin, Ravaomanarivo, et al., 2004Lis, Boczek, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-5MSHP-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.70.
Tend (C) 240.300.275.280.200.
Heat rate (K/min) 3.3.4.3.10.
Initial hold (min)      
Final hold (min)      
I 1628.1632.1629.1632.1616.
ReferenceTellez, Khan, et al., 2004Tirillini, Pellegrino, et al., 2004Afsharypuor and Jahromy, 2003Couladis, Özcan, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSRSL-200DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 275.280.280.250.275.
Heat rate (K/min) 4.4.6.3.4.
Initial hold (min)   5. 5.
Final hold (min)   5.  
I 1633.1630.1611.1628.1630.
ReferenceGhannadi, Aghazari, et al., 2003Ghasemi, Asghari, et al., 2003Jirovetz, Buchbauer, et al., 2003Limberger, Simões-Pires, et al., 2003Morteza-Semnani and Saeedi, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5DB-5HP-5
Column length (m) 60.60.30.30.30.
Carrier gas He HeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.60.50.50.
Tend (C) 250.250.240.250.250.
Heat rate (K/min) 4.5.3.4.4.
Initial hold (min)  15.  5.
Final hold (min)      
I 1628.1630.1630.1630.1630.
ReferencePourmortazavi, Sefidkon, et al., 2003Stashenko, Jaramillo, et al., 2003Zoghbi, Andrade, et al., 2003Farah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101DB-5DB-1DB-1
Column length (m) 30.25.30.30.50.
Carrier gas H2HeHeHeN2
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.50.60.60.80.
Tend (C) 245.200.250.250.225.
Heat rate (K/min) 3.5.3.4.4.
Initial hold (min) 20.  10. 
Final hold (min)      
I 1624.1607.1626.1615.1602.
ReferenceGancel, Ollé, et al., 2002Kuiate, Bessière, et al., 2002Limberger, Simões-Pires, et al., 2002Norouzi-Arasi, Yavari, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5MSDB-5MSDB-1
Column length (m) 60.50.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm)  0.250.250.25 
Tstart (C) 40.60.60.60.60.
Tend (C) 250.240.270.240.240.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)      
Final hold (min)    30. 
I 1601.1602.1632.1616.1628.5
ReferenceSefidkon, Dabiri, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Zoghbi, Andrade, et al., 2002Marongiu, Porcedda, et al., 2001Santos, Moreira, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSPB-5DB-5CP Sil 5 CBDB-5
Column length (m) 30.50.30.25.30.
Carrier gas HeHeHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.240.240.300.240.
Heat rate (K/min) 3.3.3.6.3.
Initial hold (min)      
Final hold (min)  20.   
I 1638.1631.1631.1605.1631.
ReferenceZoghbi, Andrade, et al., 1999Doneanu and Anitescu, 1998Santos, Andrade, et al., 1998Bos, Woerdenbag, et al., 1997Tellez, Estell, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zouari, Ayadi, et al., 2012
Zouari, N.; Ayadi, I.; Fakhfakh, N.; Rebai, A.; Zouari, S., Variations of chemical composition of essential oils in wild-populations of Thymus algeriensis Boiss et Reut., a North African endemic species, Lipids in Health and Desease, 2012, 11, 1, 28-39, https://doi.org/10.1186/1476-511X-11-28 . [all data]

Mothana, Hasson, et al., 2011
Mothana, R.A.A.; Hasson, S.S.; Schultze, W.; Mowitz, A.; Lindequist, U., Phytochemical composition and in vitro antimicrobial and antioxidant activities of essential oils of three endemic Soqotraen Boswellia species, Food Chem., 2011, 126, 3, 1149-1154, https://doi.org/10.1016/j.foodchem.2010.11.150 . [all data]

Zarai, Kadri, et al., 2011
Zarai, Z.; Kadri, A.; Ben Chobba, I.; Ben Mansour, R.; Bekir, R.; Mejdoub, H.; Gharsallah, N., The in-vitro evaluation of antibacterial, antifungal and cytotoxic properties of Marrubium vulgare L. essential oil grown in Tunisia, Lipids in Health and Disease, 2011, 10, 161, 1-8. [all data]

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Ho, Wang, et al., 2010
Ho, C.-L.; Wang, E.I.-C.; Yu, H.-T.; Yu, H.-M.; Su, Y.-C., Composition amd antioxidant activities of essential oils of different tissues from Cryptomeria japonica D. Don, Quarterly J. Chin. Forestry, 2010, 32, 1, 63-76. [all data]

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Radulovic, Blagojevic, et al., 2010
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Gardini, Beletti, et al., 2009
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Ho, Wang, et al., 2009
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Zhao, Zeng, et al., 2009
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Sylvestre, Pichette, et al., 2007
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Borges, Rojas, et al., 2006
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Hymete, Rohloff, et al., 2006
Hymete, A.; Rohloff, J.; Iversen, T.-H., Essential oil from seeds and husks of Aframomum corrorima from Ethiopia, Flavour Fragr. J., 2006, 21, 4, 642-644, https://doi.org/10.1002/ffj.1634 . [all data]

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Notes

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