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2-Cyclohexen-1-ol, 2-methyl-5-(1-methylethenyl)-, acetate, cis-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedApiezon L150.1317.ter Heide, 1968N2, Embacel; Column length: 2.5 m

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-11321.Raina, Srivastava, et al., 200225. m/0.55 mm/0.25 «mu»m, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryBP-11326.Shawl, Srivastava, et al., 200230. m/0.32 mm/0.25 «mu»m, N2, 5. K/min, 220. C @ 13. min; Tstart: 60. C

Kovats' RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryBP-11322.Dwivedi, Khan, et al., 200425. m/0.25 mm/0.25 «mu»m, N2; Program: 60C => 5C/min => 220C(5min) => 3C/min => 245C(5min)
CapillaryOV-11362.El-Shazly, Dorai, et al., 200230. m/0.25 mm/0.25 «mu»m, He; Program: 44C(4min) => 3C/min => 74C => 6C/min => 134C => 12C/min => 312C
CapillaryDB-51352.Roscigno, 199830. m/0.25 mm/0.25 «mu»m; Program: 50C(5min) => 2C/min => 250C (60min) => 2C/min => 270C => 1C/min => 290C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1365.Benkaci-Ali, Baaliouamer, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 60. C @ 8. min, 2. K/min, 250. C @ 30. min
CapillaryRTX-11342.Muselli, Rossi, et al., 200760. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryDB-51362.Yu, Liao, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 250. C @ 10. min; Tstart: 50. C
CapillaryHP-5MS1381.Chorianopoulos, Kalpoutzakis, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51362.Economakis, Skaltsa, et al., 200230. m/0.25 mm/0.25 «mu»m, 50. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-5MS1362.Skaltsa, Mavrommati, et al., 200130. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryOV-11310.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 «mu»m, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryOV-1011311.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011315.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-Wax1738.Muselli, Rossi, et al., 200760. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 30. min; Tstart: 60. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51367.Monsef-Esfahani, Miri, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 5. min, 3. K/min; Tend: 240. C
CapillaryRTX-11315.Museli, Pau, et al., 200960. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryRTX-11318.Museli, Pau, et al., 200960. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryDB-51363.Jardin, Jham, et al., 200830. m/0.25 mm/0.25 «mu»m, Nitrogen, 60. C @ 1. min, 3. K/min, 240. C @ 9. min
CapillaryHP-51360.Yassa and Akhani, 200830. m/0.25 mm/0.32 «mu»m, Helium, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillarySPB-51366.Raal, Orav, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5 MS1368.Vagionas, Graikou, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51360.Yassa and Akhani, 200730. m/0.25 mm/0.32 «mu»m, He, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryHP-11340.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.33 «mu»m, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryMethyl Silicone1360.Kitchlu, Bakshi, et al., 200625. m/0.25 mm/0.25 «mu»m, He, 90. C @ 2. min, 7. K/min; Tend: 220. C
CapillaryHP-51362.Saeidnia, Gohari, et al., 2005He, 5. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 240. C
CapillaryPE-51322.Singh, Raina, et al., 200530. m/0.32 mm/0.25 «mu»m, H2, 60. C @ 2. min, 5. K/min, 230. C @ 4. min
CapillaryHP-5MS1362.Mimica-Dukic, Bozin, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11366.Palá-Paúl, Velasco-Negueruela, et al., 200450. m/0.25 mm/0.25 «mu»m, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryDB-51395.Edris, Shalaby, et al., 2003He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 220. C
CapillaryHP-51362.Mookdasanit, Tamura, et al., 2003Helium, 2. K/min, 210. C @ 60. min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C
CapillaryCP Sil 5 CB1349.Monfared, Davarani, et al., 2002He, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 220. C
CapillarySE-541364.Silva A.D., Patitucci M.L., et al., 200230. m/0.32 mm/0.25 «mu»m, H2, 5. K/min; Tstart: 40. C; Tend: 240. C
CapillaryHP-51364.Gallori, Flamini, et al., 200130. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51362.Santos-Gomes and Fernandes-Ferreira, 200130. m/0.25 mm/0.25 «mu»m, H2, 3. K/min; Tstart: 60. C; Tend: 285. C
CapillaryOV-1011311.Yang, 2001N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryRTX-11346.Kalemba, 199930. m/0.25 mm/0.25 «mu»m, N2, 4. K/min; Tstart: 60. C; Tend: 300. C
CapillarySPB-51363.Doneanu and Anitescu, 199850. m/0.32 mm/0.25 «mu»m, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C
CapillaryOV-1011311.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011315.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51362.Nezhadali and Parsa, 201030. m/0.20 mm/0.32 «mu»m, Helium; Program: 60 0C (1 min) 3 0C/min -> 140 0C 50 0C/min -> 250 0C (3 min)
CapillaryHP-51362.Riahi, Pourbasheer, et al., 2009Column length: 30. m; Column diameter: 0.32 mm; Program: not specified
CapillaryHP-51338.Qiao, Xie, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium; Program: 40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)
CapillarySE-301351.Vinogradov, 2004Program: not specified
CapillaryOV-1011315.Yang, 2001N2; Column length: 50. m; Column diameter: 0.25 mm; Program: not specified
CapillaryMethyl Silicone1351.Zenkevich, 1999Program: not specified

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-Wax1710.Museli, Pau, et al., 200960. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillarySupelcowax-101731.Raal, Orav, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-20M1727.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.1 «mu»m, He, 2. K/min, 220. C @ 30. min; Tstart: 60. C
CapillaryFFAP1725.Kitchlu, Bakshi, et al., 200620. m/0.25 mm/0.25 «mu»m, He, 6. K/min; Tstart: 90. C; Tend: 250. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-Innowax FSC1782.Suleimenov Y.M., Atazhanova G.A., et al., 200660. m/0.25 mm/0.25 «mu»m, He; Program: 60(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax1782.Baser, Demirci, et al., 200160. m/0.25 mm/0.25 «mu»m, He; Program: 60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

ter Heide, 1968
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Chorianopoulos, N.; Kalpoutzakis, E.; Aligiannis, N.; Mitaku, S.; Nychas, G.-J.; Haroutounian, S.A., Essential oils of Satureja, Origanum, and Thymus species: chemical composition and antibacterial activities against foodborne pathogens, J. Agric. Food Chem., 2004, 52, 26, 8261-8267, https://doi.org/10.1021/jf049113i . [all data]

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Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

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Santos-Gomes, P.C.; Fernandes-Ferreira, M., Organ- and season-dependent variation in the essential oil composition of Salvia officinalis L. cultivated at two different sites, J. Agric. Food Chem., 2001, 49, 6, 2908-2916, https://doi.org/10.1021/jf001102b . [all data]

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Tamura, H.; Yang, R.-H.; Sugisawa, H., Aroma profiles of peel oils of acid citrus, ACS Sym. Ser., 1993, 525, 121-136. [all data]

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Nezhadali, A.; Parsa, M., Study of the volatile compounds in Artemisia Sagebrush from Iran using HS/SPME/GC/MS, Int. J. Environ. Sci. Development, 2010, 1, 3, 287-289, https://doi.org/10.7763/IJESD.2010.V1.56 . [all data]

Riahi, Pourbasheer, et al., 2009
Riahi, S.; Pourbasheer, E.; Ganjali, M.R.; Norouzi, P., Investigation of different linear and non-linear chemometric methods for modeling of retention index of essential oil components: Concerns to support vector mashine, J. Hazard. Mat., 2009, 166, 2-3, 853-859, https://doi.org/10.1016/j.jhazmat.2008.11.097 . [all data]

Qiao, Xie, et al., 2008
Qiao, Y.; Xie, B.J.; Zhang, Y.; Zhang, Y.; FAn, G.; Yao, X.L.; Pan, S.Y., Characterization of aroma active compounds in fruit juice and peel oil of Junchen sweet orange fruit (Citrus sinensis (L.) Osbeck) by GC-MS and GC-O, Molecules, 2008, 13, 6, 1333-1344, https://doi.org/10.3390/molecules13061333 . [all data]

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Zenkevich, I.G., Analytical Parameters of Components of essential Oils for their Gas Chromatographic and Chromato-Mass-Spectral Identification. Acetates of Terpene Alcohols, Rastitelnye Resursy (Plant Resources), 1999, 35, 1, 30-37. [all data]

Suleimenov Y.M., Atazhanova G.A., et al., 2006
Suleimenov Y.M.; Atazhanova G.A.; Ozek T.; Demirci B.; Kulyyasov A.T.; Adekenov S.M.; Baser K.H.C., Essential oil composition of three species of Achillea from Kazakhstan, Chem. Nat. Compd. (Engl. Transl.), 2006, 37, 5, 447-450, https://doi.org/10.1023/A:1014471326724 . [all data]

Baser, Demirci, et al., 2001
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Notes

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