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7-Oxabicyclo[4.1.0]heptane, 1-methyl-4-(1-methylethenyl)-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSHP-5HP-5MSPetrocol DH
Column length (m) 30.60.50.30.100.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.20.250.5
Tstart (C) 50.40.35.50.60.
Tend (C) 220.200.250.250.180.
Heat rate (K/min) 5.2.3.5.4.
Initial hold (min) 10. 15.2.8.
Final hold (min)  20.40.5.2.
I 1136.1138.1133.1116.1139.
ReferenceFlamini, Tebano, et al., 2007Seo and Baek, 2005Stashenko, Jaramillo, et al., 2004Shang, Hu, et al., 2002Alonzo, Saiano, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase BP-1
Column length (m) 50.
Carrier gas He
Substrate  
Column diameter (mm) 0.22
Phase thickness (mum) 0.25
Tstart (C) 60.
Tend (C) 220.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 1120.
ReferenceLota, Serra, et al., 2001
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Flamini, Tebano, et al., 2007
Flamini, G.; Tebano, M.; Cioni, P.L., Volatiles emission patterns of different plant organs and pollen of Citrus limon, Anal. Chim. Acta., 2007, 589, 1, 120-124, https://doi.org/10.1016/j.aca.2007.02.053 . [all data]

Seo and Baek, 2005
Seo, W.H.; Baek, H.H., Identification of characteristic aroma-active compounds from water dropword (Oenanthe javanica DC.), J. Agric. Food Chem., 2005, 53, 17, 6766-6770, https://doi.org/10.1021/jf050150z . [all data]

Stashenko, Jaramillo, et al., 2004
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparison of different extraction methods for the analysis of volatile secondary metabolites of Lippia alba (Mill.) N.E. Brown, grown in Colombia, and evaluation of its in vitro antioxidant activity, J. Chromatogr. A, 2004, 1025, 1, 93-103, https://doi.org/10.1016/j.chroma.2003.10.058 . [all data]

Shang, Hu, et al., 2002
Shang, C.; Hu, Y.; Deng, C.; Hu, K., Rapid determination of volatile constituents of Michelia alba flowers by gas chromatography-mass spectrometry with solid-phase microextraction, J. Chromatogr. A, 2002, 942, 1-2, 283-288, https://doi.org/10.1016/S0021-9673(01)01382-6 . [all data]

Alonzo, Saiano, et al., 2001
Alonzo, G.; Saiano, F.; Tusa, N.; del Bosco, S.F., Analysis of volatile compounds released from embryogenic cultures and somatic embryos of sweet oranges by head space SPME, Plant Cell Tissue Organ Cult., 2001, 66, 1, 31-34, https://doi.org/10.1023/A:1010608417457 . [all data]

Lota, Serra, et al., 2001
Lota, M.-L.; Serra, D.R.; Jacquemond, C.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of sour orange, Flavour Fragr. J., 2001, 16, 2, 89-96, https://doi.org/10.1002/1099-1026(200103/04)16:2<89::AID-FFJ950>3.0.CO;2-D . [all data]


Notes

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