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7-Oxabicyclo[4.1.0]heptane, 1-methyl-4-(1-methylethenyl)-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1OV-1DB-5ZB-5
Column length (m) 60.60.30.30.60.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.220.220.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.40.40.
Tend (C) 230.230.250.250.260.
Heat rate (K/min) 2.2.5.5.6.
Initial hold (min)   3.0.54.6
Final hold (min) 5.30.2.2.1.
I 1117.1117.1164.1132.1149.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Dib, Djabou, et al., 2010Hu, Liang, et al., 2010Özel, Gögüs, et al., 2005Jürgens and Dötterl, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase HP-5HP-5 MS
Column length (m) 60.30.
Carrier gas  Helium
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (mum) 0.250.25
Tstart (C) 40.50.
Tend (C) 250.250.
Heat rate (K/min) 5.5.
Initial hold (min) 15.2.
Final hold (min)  5.
I 1133.1116.
ReferenceStashenko, Jaramillo, et al., 2003Shang, Hu, et al., 2001
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

Dib, Djabou, et al., 2010
Dib, M.ElA.; Djabou, N.; Desjobert, L.-M.; Allali, H.; Tabti, B.; Muselli, A.; Costa, J., Characterization of volatile compounds of Daucus crinitus Desf. headspace solid phase microextraction as alternative technique to hydrodistillation, Chem, Centr. J., 2010, 4, 16, 1-15. [all data]

Hu, Liang, et al., 2010
Hu, C.-D.; Liang, Y.-Z.; Guo, F.-Q.; Li, X.-R.; Wang, W.-P., Determination of essential oil composition from Osmanthus fragrans tea by GC-MS combined with a chemometric resolution method, Molecules, 2010, 15, 5, 3683-3693, https://doi.org/10.3390/molecules15053683 . [all data]

Özel, Gögüs, et al., 2005
Özel, M.Z.; Gögüs, F.; Hamilton, J.F.; Lewis, A.C., Analysis of volatile components from Ziziphora taurica subsp. taurica by steam distillation, superheated-water extraction, and direct thermal desorption with GC×GC-TOFMS, Anal. Bioanal. Chem., 2005, 382, 1, 115-119, https://doi.org/10.1007/s00216-005-3156-x . [all data]

Jürgens and Dötterl, 2004
Jürgens, A.; Dötterl, S., Chemical composition of anther volatiles in Ranunculaceae: genera-specific profiles in Aemone, Aquilegia, Caltha, Pulsatilla, Ranunculus, and Trollius species, American Journal of Botany, 2004, 91, 12, 1969-1980, https://doi.org/10.3732/ajb.91.12.1969 . [all data]

Stashenko, Jaramillo, et al., 2003
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparación de la composición química y de la actividad antioxidante in vitro de los metabolitos secundarios volátiles de plantas de la familia verbenaceae, Rev. Acad. Colomb. Cienc. Exactas Fis. Nat., 2003, 27, 105, 579-597. [all data]

Shang, Hu, et al., 2001
Shang, C.; Hu, Y.; Deng, C.; Hu, K., Rapid determination of volatile constituents of Michelia alba flowers by gas chromatography - mass spectrometry with solid-phase microextraction, J. Chromatogr. A, 2001, 942, 1-2, 283-288, https://doi.org/10.1016/S0021-9673(01)01382-6 . [all data]


Notes

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