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Phosphorothioic acid, O-(1,6-dihydro-6-oxo-1-phenyl-3-pyridazinyl) O,O-diethyl ester


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneHP-5DB-5
Column length (m) 30.30.30.
Carrier gas Helium  
Substrate    
Column diameter (mm) 0.250.250.25
Phase thickness (mum) 0.250.250.25
Program 50 0C(1 min) 25 0C/min -> 125 0C 10 0C/min -> 300 0C (10 min)50 0C (1 min) 20 0C/min -> 150 0C 10 0C/min -> 280 0C50 0C (1 min) 20 0C/min -> 200 0C 10 0C/min -> 280 0C (2 min)
I 2455.2437.2450.
ReferenceDepartment of Food Safety and Welfare, 2006Kawara, Asada, et al., 2005Kawata, Mukai, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Department of Food Safety and Welfare, 2006
Department of Food Safety, Ministry of Health; Welfare, Analytical methods for residual compositional substances of agricultural chemicals, feed aadditives, and veterinary drugs in foods, 2006, retrieved from http://www.mhlw.go.jp/english/topics/foodsafety/positivelist060228/de/060526-1a.pdf. [all data]

Kawara, Asada, et al., 2005
Kawara, K.; Asada, T.; Oikawa, K.; Tanabe, A., Multiresidue determination of pesticides in sediments by ultrasonically assisted extraction and gas chromatography/mass spectrometry, J. AOAC International, 2005, 88, 5, 1440-1451. [all data]

Kawata, Mukai, et al., 1996
Kawata, K.; Mukai, H.; Tanabe, H.; Yasuhara, A., Annual variation of insecticides in precipitation in rural Japan, Bull. Environ. Contam. Toxicol., 1996, 57, 6, 853-858, https://doi.org/10.1007/s001289900268 . [all data]


Notes

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