Trifluoperazine
- Formula: C21H24F3N3S
- Molecular weight: 407.496
- IUPAC Standard InChIKey: ZEWQUBUPAILYHI-UHFFFAOYSA-N
- CAS Registry Number: 117-89-5
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 10H-Phenothiazine, 10-[3-(4-methyl-1-piperazinyl)propyl]-2-(trifluoromethyl)-; Phenothiazine, 10-[3-(4-methyl-1-piperazinyl)propyl]-2-(trifluoromethyl)-; RP 7623; Trifluoperazin; Trifluoromethylperazine; Trifluoroperazine; Trifluperazine; Triflurin; Triperazine; 10-(γ-(N'-Methylpiperazino)propyl)-2-trifluoromethylphenothiozine; 10-(3-(4-Methyl-1-piperazinyl)propyl)-2-(trifluoromethyl)phenothiazine; Trifluoperazina; Trifluoromethyl-10-(3'-(1-methyl-4-piperazinyl)propyl)phenothiazine; 10-[3-(4-Methylpiperazin-1-yl)propyl]-2-(trifluoromethyl)-10H-phenothiazine; Trifluroperizine; 2-Trifluoromethyl-10-[3'-(1-methyl-4-piperazinyl)propyl]phenothiazine; Flurazine; NSC 17474; TFP; Triphtazine
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Packed |
---|---|---|---|---|---|
Active phase | SPB-1 | DB-1 | DB-1 | SE-30 | SE-30 |
Column length (m) | 30. | 15. | 15. | 15. | 1.8 |
Carrier gas | He | He | He | He | N2 |
Substrate | Chromosorb W | ||||
Column diameter (mm) | 0.75 | 0.32 | 0.25 | 0.25 | |
Phase thickness (μm) | 1.0 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 160. | 120. | 120. | 100. | 130. |
Tend (C) | 280. | 280. | 280. | 295. | 290. |
Heat rate (K/min) | 10. | 8. | 8. | 5. | 8. |
Initial hold (min) | 2. | ||||
Final hold (min) | 12. | 5. | 5. | 8. | |
I | 2688. | 2662. | 2662. | 2641. | 2685. |
Reference | Christ, Noomano, et al., 1988 | Perrigo, Peel, et al., 1985 | Perrigo, Ballantyne, et al., 1984 | Anderson and Stafford, 1983 | Perrigo and Peel, 1981 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Christ, Noomano, et al., 1988
Christ, D.W.; Noomano, P.; Rosas, M.; Rhone, D.,
Retention indices by wide-bore capillary gas chromatography with nitrogen-phosphorus detection,
J. Anal. Toxicol., 1988, 12, 2, 84-88, https://doi.org/10.1093/jat/12.2.84
. [all data]
Perrigo, Peel, et al., 1985
Perrigo, B.J.; Peel, H.W.; Ballantyne, D.J.,
Use of Dual-Column Fused-Silica Capillary Gas Chromatography in Combination with Detector Response Factors for Analytical Toxicology.,
J. Chromatogr., 1985, 341, 81-88, https://doi.org/10.1016/S0378-4347(00)84011-6
. [all data]
Perrigo, Ballantyne, et al., 1984
Perrigo, B.J.; Ballantyne, D.J.; Peel, H.W.,
Condierations in developing a data base for drugs on a DBI capillary column,
J. Can. Soc. Forensic Sci., 1984, 17, 2, 41-49, https://doi.org/10.1080/00085030.1984.10757360
. [all data]
Anderson and Stafford, 1983
Anderson, W.H.; Stafford, D.T.,
Applications of capillary gas chromatography in routine toxicological analyses,
J. Hi. Res. Chromatogr. Chromatogr. Comm., 1983, 6, 5, 247-254, https://doi.org/10.1002/jhrc.1240060506
. [all data]
Perrigo and Peel, 1981
Perrigo, B.J.; Peel, H.W.,
The use of retention indices and temperature-programmed gas chromatography in analytical toxicology,
J. Chromatogr. Sci., 1981, 19, 5, 219-226, https://doi.org/10.1093/chromsci/19.5.219
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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