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Propene

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxane: CP-Sil 5 CBPetrocol DHUltra-ALLOY-5Ultra-ALLOY-5Ultra-ALLOY-5
Column length (m) 60.100.30.30.30.
Carrier gas HeliumHelium   
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 1.00.500.250.250.25
Tstart (C) 45.20.40.40.40.
Tend (C) 210.220.320.320.320.
Heat rate (K/min) 3.615.20.20.20.
Initial hold (min) 1.4515.2.2.2.
Final hold (min) 2.7230.13.13.13.
I 286.294.295.295.295.
ReferenceBramston-Cook, 2013Supelco, 2012Tsuge, Ohtan, et al., 2011Tsuge, Ohtan, et al., 2011Tsuge, Ohtan, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase Ultra-ALLOY-5Ultra-ALLOY-5OV-101
Column length (m) 30.30.52.
Carrier gas   N2
Substrate    
Column diameter (mm) 0.250.250.26
Phase thickness (mum) 0.250.25 
Tstart (C) 40.40.50.
Tend (C) 320.320.220.
Heat rate (K/min) 20.20.3.
Initial hold (min) 2.2. 
Final hold (min) 13.13. 
I 295.298.290.
ReferenceTsuge, Ohtan, et al., 2011Tsuge, Ohtan, et al., 2011Chupalov and Zenkevich, 1996
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bramston-Cook, 2013
Bramston-Cook, R., Kovats indices for C2-C13 hydrocarbons and selected oxygenated/halocarbons with 100 % dimethylpolysiloxane columns, 2013, retrieved from http://lotusinstruments.com/monographs/List .... [all data]

Supelco, 2012
Supelco, CatalogNo. 24160-U, Petrocol DH Columns. Catalog No. 24160-U, 2012, retrieved from http://www.sigmaaldrich.com/etc/medialib/docs/Supelco/Datasheet/1/w97949.Par.0001.File.tmp/w97949.pdf. [all data]

Tsuge, Ohtan, et al., 2011
Tsuge, S.; Ohtan, H.; Watanabe, C., Pyrolysis - GC/MS Data Book of Synthetic Polymers, Elsevier, 2011, 420. [all data]

Chupalov and Zenkevich, 1996
Chupalov, A.A.; Zenkevich, I.G., Chromatographic Characterization of Structural Transformations of Organic Compounds in Diels-Alder Reaction. Aliphatic Dienes and Dienophyls, Zh. Org. Khim., 1996, 32, 6, 675-684. [all data]


Notes

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