Caryophyllene oxide


Kovats' RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5HP-1DB-5
Column length (m) 30.60.30.60.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.15
Tstart (C) 60.40.60.60.60.
Tend (C) 280.250. 200.220.
Heat rate (K/min) 2.3.3.4.3.
Initial hold (min) 8.1. 5.3.
Final hold (min) 30.20. 25. 
I 1578.1613.1583.1595.1581.
ReferenceHazzit, Baaliouamer, et al., 2006Jalali-Heravi, Zekavat, et al., 2006Lucero, Fredrickson, et al., 2006Meccia G., Rosquete C., et al., 2006Mevy, Bessiere, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1BP-1DB-5DB-5
Column length (m) 25.25.30.30.30.
Carrier gas HeN2N2 He
Substrate      
Column diameter (mm) 0.20.320.320.250.26
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 220.220.220.210.246.
Heat rate (K/min) 3.5.5.2.3.
Initial hold (min) 3.  2. 
Final hold (min)  13.3.33. 
I 1578.1575.1568.1577.1583.
ReferenceMevy, Bessiere, et al., 2006, 2Raina, Verma, et al., 2006Srivastava, Srivastava, et al., 2006Sylvestre, Pichette, et al., 2006Adams, Morris, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSBP-5DB-5MSDB-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.260.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.60.
Tend (C) 246.250.260.240.255.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)  10.2.  
Final hold (min)  5.5.  
I 1581.1589.1590.1581.1582.
ReferenceAdams and Nguyen, 2005Asuming, Beauchamp, et al., 2005Baranauskiene, Venskutonis, et al., 2005Maia, Andrade, et al., 2005Medina, Lucero, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5DB-5MSCP Sil 8 CB
Column length (m) 30.30.30.30.30.
Carrier gas H2HeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.50.
Tend (C) 280.200.260.240.220.
Heat rate (K/min) 4.4.3.3.3.
Initial hold (min)  1.  2.
Final hold (min) 30.15.   
I 1583.1582.1583.1581.1576.
ReferenceAvato, Raffo, et al., 2004Juliani, Zygadlo, et al., 2004Lopes, Strobl, et al., 2004Palmeira, Moura, et al., 2004Schwob, Bessiere, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5HP-5MSHP-5
Column length (m) 50.25.50.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.25 0.250.251.
Tstart (C) 95.40.50.50.40.
Tend (C) 240.280.280.280.250.
Heat rate (K/min) 4.3.5.4.5.
Initial hold (min)  5.2.2.1.
Final hold (min)  5.10.10. 
I 1572.1578.1596.1593.1617.
ReferenceVelasco-Negueruela, Sanz, et al., 2004Amparo Blázquez, Pérez, et al., 2003Baranauskiene, Venskutonis, et al., 2003Baranauskiene, Venskutonis, et al., 2003, 2Bouzouita, Kachouri, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5DB-5CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.15
Tstart (C) 60.60.60.60.50.
Tend (C) 280.280.240.240.230.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)      
Final hold (min)   30.30. 
I 1561.1561.1560.1549.1565.
ReferenceCouladis, Chinou, et al., 2003Gkinis, Tzakou, et al., 2003Marongiu, Piras, et al., 2003Marongiu, Piras, et al., 2003Ogunwande, Olawore, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1BP-1DB-5SPB-1
Column length (m) 30.25.25.30.30.
Carrier gas HeN2N2HeHe
Substrate      
Column diameter (mm) 0.250.320.550.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 280.220.220.250.225.
Heat rate (K/min) 3.5.5.0.52.
Initial hold (min)    5.2.
Final hold (min)  15.15.10.5.
I 1573.1578.1581.1582.1558.
ReferenceÖzcan, Tzakou, et al., 2003Raina, Srivastava, et al., 2003Srivastava, Ahmad, et al., 2003Viña and Murillo, 2003Jayaprakasha, Rao, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5BP-1BP-1HP-5MS
Column length (m) 25.30.60.25.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.20.250.320.550.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.240.220.220.250.
Heat rate (K/min) 3.3.5.5.3.
Initial hold (min)      
Final hold (min)  20. 15. 
I 1581.1581.1578.1566.1583.
ReferenceMevy, Bessiere, et al., 2002Mita, Tsitsimpikou, et al., 2002Raina, Lal, et al., 2002Raina, Srivastava, et al., 2002Salido, Altarejos, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1HP-5DB-1DB-1
Column length (m) 30.25.25.28.50.
Carrier gas N2N2H2HeN2
Substrate      
Column diameter (mm) 0.320.550.320.250.25
Phase thickness (μm) 0.250.250.520.250.25
Tstart (C) 60.60.40.50.80.
Tend (C) 220.220.240.270.225.
Heat rate (K/min) 5.5.4.4.54.
Initial hold (min)    1. 
Final hold (min) 13.15.   
I 1566.1585.1581.1537.1577.
ReferenceShawl, Srivastava, et al., 2002Jain, Srivastava, et al., 2001Kitic, Palic, et al., 2001Nagalakshmi, Thangadurai, et al., 2001Palá-Paúl, Velasco-Negueruela, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1BP-1HP-1DB-1HP-5
Column length (m) 50.25.25.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.550.20.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 100.60.100.40.60.
Tend (C) 250.220.220.260.280.
Heat rate (K/min) 5.5.4.2.3.
Initial hold (min) 7.  5. 
Final hold (min)  15. 20. 
I 1575.1573.1572.1557.1580.
ReferenceRaina, Srivastava, et al., 2001Raina, Srivastava, et al., 2001, 2Rajeswara Rao, 2001Senatore and Rigano, 2001Tzakou and Couladis, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5SE-54DB-5Methyl Silicone
Column length (m) 30.30.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.260.260.260.260.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 246.240.246.246.225.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min)     2.
Final hold (min)     5.
I 1581.1581.1581.1581.1574.
ReferenceAdams, 2000Adams, 2000, 2Adams, 2000, 3Adams, 2000, 4Jayaprakasha, Rao, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30PTE-5HP-5MSDB-5BP-5
Column length (m) 25.60.30.30.25.
Carrier gas HeH2He He
Substrate      
Column diameter (mm) 0.220.320.250.320.25
Phase thickness (μm) 0.250.30.25 0.25
Tstart (C) 70.60.60.50.60.
Tend (C) 220.285.280.250.200.
Heat rate (K/min) 5.4.33.3.3.
Initial hold (min)    5. 
Final hold (min)      
I 1568.1581.1581.1581.1585.
ReferenceKardali, Velasco-Negueruela, et al., 2000Mitic and Dordevic, 2000Roussis, Tsoukatou, et al., 2000Tzakou, Harvala, et al., 2000Weissbecker B., Van Loon J.J.A., et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBOV-101HP-5DB-5
Column length (m) 30.25.25.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.260.250.320.250.25
Phase thickness (μm) 0.25  0.250.33
Tstart (C) 60.60.50.60.40.
Tend (C) 246.280.200.280.260.
Heat rate (K/min) 3.5.5.4.2.
Initial hold (min)     5.
Final hold (min)     20.
I 1581.1570.1576.1579.1567.
ReferenceAdams, 1999Kaul, Gujral, et al., 1999Kuiate, Zollo, et al., 1999Sajjadi and Ghassemi, 1999Senatore and de Feo, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5BP-1BP-1
Column length (m) 30.30.30.50.50.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 250.240.240.260.260.
Heat rate (K/min) 3.3.4.2.2.
Initial hold (min) 5.    
Final hold (min)      
I 1576.1582.1583.1576.1582.
ReferenceSiani, Ramos, et al., 1999da Silva, Andrade, et al., 1999da Silva, Zoghbi, et al., 1999Vera and Chane-Ming, 1999Vera and Chane-Ming, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBMethyl SiliconeDB-5DB-5DB-5
Column length (m) 25.25.30.30.30.
Carrier gas  N2HeHeHe
Substrate      
Column diameter (mm) 0.250.50.250.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 60.60.40.40.60.
Tend (C) 280.220.250.250.240.
Heat rate (K/min) 5.5.2.2.4.
Initial hold (min)   5.5. 
Final hold (min)   20.20. 
I 1572.1575.1567.1567.1579.
ReferenceKaul and Vats, 1998Mallavarapu, Rao, et al., 1998Senatore, Urrunaga Soria, et al., 1998Senatore, 1998Zoghbi, Andrade, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BPX-5SPB-1DB-5OV-101
Column length (m) 30.50.30.30.25.
Carrier gas HeN2HeHeN2
Substrate      
Column diameter (mm) 0.230.220.320.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 200.185.250.240.200.
Heat rate (K/min) 3.2.5.3.5.
Initial hold (min)  10.2.  
Final hold (min)   5.  
I 1599.1580.1565.1582.1575.
ReferenceFiorini, Fourasté, et al., 1997Fournier, Hadjiakhoondi, et al., 1997Jayaprakasha, Jaganmohan Rao, et al., 1997Tellez, Estell, et al., 1997von Poser, Menut, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-5DB-5DB-5OV-101
Column length (m) 25.30.30.30.25.
Carrier gas N2    
Substrate      
Column diameter (mm) 0.2   0.25
Phase thickness (μm)      
Tstart (C) 60.40.40.40.50.
Tend (C) 180.210.210.210.200.
Heat rate (K/min) 3.2.2.2.5.
Initial hold (min) 10.2.2.2. 
Final hold (min) 1.120.120.120. 
I 1574.1575.1577.1576.1578.
ReferenceJantan, Ali, et al., 1995Loayza, Abujder, et al., 1995Loayza, Abujder, et al., 1995Loayza, Abujder, et al., 1995Menut, Lamaty, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase DB-1BP-1
Column length (m) 28.50.
Carrier gas HeH2
Substrate   
Column diameter (mm) 0.250.33
Phase thickness (μm) 0.25 
Tstart (C) 50.65.
Tend (C) 270.220.
Heat rate (K/min) 4.5.
Initial hold (min) 1.2.
Final hold (min)   
I 1537.1587.
ReferenceSaad, El-Sharkawy, et al., 1995Ekundayo, Laakso, et al., 1988
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Vera and Chane-Ming, 1999
Vera, R.R.; Chane-Ming, J., Chemical composition of the essential oil of marjoram (Origanum majorana L.) from Reunion Island, Food Chem., 1999, 66, 2, 143-145, https://doi.org/10.1016/S0308-8146(98)00018-1 . [all data]

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Notes

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